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    Method of precipitation of metal ions
    3.
    发明授权
    Method of precipitation of metal ions 有权
    金属离子析出方法

    公开(公告)号：US08808660B2

    公开(公告)日：2014-08-19

    申请号：US13145632

    申请日：2010-02-09

    申请人： Xiaowei Huang ,  Zhiqi Long ,  Hongwei Li ,  Dali Cui ,  Xinlin Peng ,  Guilin Yang ,  Yongke Hou ,  Chunmei Wang ,  Shunli Zhang

    发明人： Xiaowei Huang ,  Zhiqi Long ,  Hongwei Li ,  Dali Cui ,  Xinlin Peng ,  Guilin Yang ,  Yongke Hou ,  Chunmei Wang ,  Shunli Zhang

    IPC分类号： C01B31/24

    CPC分类号： C22B3/44 ,  C04B22/064 ,  C04B22/066 ,  C22B59/00 ,  Y02P10/234

    摘要： The present invention relates to a method of precipitation of metal ions. Mineral(s), oxide(s), hydroxide(s) of magnesium and/or calcium are adopted as raw materials, and the raw material(s) is processed through at least one step of calcination, slaking, or carbonization to produce aqueous solution(s) of magnesium bicarbonate and/or calcium bicarbonate, and then the solution(s) is used as precipitant(s) to deposit rare earth, such as nickel, cobalt, iron, aluminum, gallium, indium, manganese, cadmium, zirconium, hafnium, strontium, barium, copper and zinc ions. And at least one of metal carbonates, hydroxides or basic carbonates is obtained, or furthermore the obtained products are calcined to produce metal oxides. The invention takes the cheap calcium and/or magnesium minerals or their oxides, hydroxides with low purity as raw materials to instead common precipitants such as ammonium bicarbonate and sodium carbonate etc. The calcium, magnesium, carbon dioxide etc are efficiently and circularly used, and the environment pollution by ammonium-nitrogen wastewater, high concentration salts wastewater is avoided, and both of the discharge of greenhouse gas carbon dioxide and the production cost of metal are decreased.

    摘要翻译： 本发明涉及一种沉淀金属离子的方法。 采用矿物，氧化物，镁和/或钙的氢氧化物作为原料，通过至少一个煅烧，去渣或碳化步骤处理原料以产生水溶液 碳酸氢钙和/或碳酸氢钙的溶液，然后使用该溶液作为沉淀剂沉积稀土，例如镍，钴，铁，铝，镓，铟，锰，镉， 锆，铪，锶，钡，铜和锌离子。 并且获得金属碳酸盐，氢氧化物或碱性碳酸盐中的至少一种，或者进一步将所得产物煅烧以产生金属氧化物。 本发明以廉价的钙和/或镁矿物或其氧化物，低纯度的氢氧化物为原料，代替普通的沉淀剂如碳酸氢铵和碳酸钠等。钙，镁，二氧化碳等有效和循环使用， 避免了氮铵废水，高浓度盐水等环境污染，温室气体二氧化碳的排放和金属的生产成本均下降。

    METHOD OF PRECIPITATION OF METAL IONS
    4.
    发明申请
    METHOD OF PRECIPITATION OF METAL IONS 有权
    降低金属离子的方法

    公开(公告)号：US20110280778A1

    公开(公告)日：2011-11-17

    申请号：US13145632

    申请日：2010-02-09

    申请人： Xiaowei Huang ,  Zhiqi Long ,  Hongwei Li ,  Dali Cui ,  Xinlin Peng ,  Guilin Yang ,  Yongke Hou ,  Chunmei Wang ,  Shunli Zhang

    发明人： Xiaowei Huang ,  Zhiqi Long ,  Hongwei Li ,  Dali Cui ,  Xinlin Peng ,  Guilin Yang ,  Yongke Hou ,  Chunmei Wang ,  Shunli Zhang

    IPC分类号： C01F17/00 ,  C01G49/02 ,  C01F7/34 ,  C01G51/06 ,  C01G53/06 ,  C01G27/00 ,  C01G45/00 ,  C01G15/00 ,  C01G3/00 ,  C01G9/00 ,  C01G11/00 ,  C01G45/02 ,  C01F11/02 ,  C01G3/02 ,  C01G9/02 ,  C01F5/24 ,  C01F11/18

    CPC分类号： C22B3/44 ,  C04B22/064 ,  C04B22/066 ,  C22B59/00 ,  Y02P10/234

    摘要： The present invention relates to a method of precipitation of metal ions. Mineral(s), oxide(s), hydroxide(s) of magnesium and/or calcium are adopted as raw materials, and the raw material(s) is processed through at least one step of calcination, slaking, or carbonization to produce aqueous solution(s) of magnesium bicarbonate and/or calcium bicarbonate, and then the solution(s) is used as precipitant(s) to deposit rare earth, such as nickel, cobalt, iron, aluminum, gallium, indium, manganese, cadmium, zirconium, hafnium, strontium, barium, copper and zinc ions. And at least one of metal carbonates, hydroxides or basic carbonates is obtained, or furthermore the obtained products are calcined to produce metal oxides. The invention takes the cheap calcium and/or magnesium minerals or their oxides, hydroxides with low purity as raw materials to instead common precipitants such as ammonium bicarbonate and sodium carbonate etc. The calcium, magnesium, carbon dioxide etc are efficiently and circularly used, and the environment pollution by ammonium-nitrogen wastewater, high concentration salts wastewater is avoided, and both of the discharge of greenhouse gas carbon dioxide and the production cost of metal are decreased.

    摘要翻译： 本发明涉及一种沉淀金属离子的方法。 采用矿物，氧化物，镁和/或钙的氢氧化物作为原料，通过至少一个煅烧，去渣或碳化步骤处理原料以产生水溶液 碳酸氢钙和/或碳酸氢钙的溶液，然后使用该溶液作为沉淀剂沉积稀土，例如镍，钴，铁，铝，镓，铟，锰，镉， 锆，铪，锶，钡，铜和锌离子。 并且获得金属碳酸盐，氢氧化物或碱性碳酸盐中的至少一种，或者进一步将所得产物煅烧以产生金属氧化物。 本发明以廉价的钙和/或镁矿物或其氧化物，低纯度的氢氧化物为原料，代替普通的沉淀剂如碳酸氢铵和碳酸钠等。钙，镁，二氧化碳等有效和循环使用， 避免了氮铵废水，高浓度盐水等环境污染，温室气体二氧化碳的排放和金属的生产成本均下降。

    PROCESS FOR PRETREATING ORGANIC EXTRACTANTS AND ITS PRODUCT AND APPLICATION
    5.
    发明申请
    PROCESS FOR PRETREATING ORGANIC EXTRACTANTS AND ITS PRODUCT AND APPLICATION 审中-公开
    预处理有机提取物及其产品和应用的方法

    公开(公告)号：US20100003176A1

    公开(公告)日：2010-01-07

    申请号：US12526436

    申请日：2008-02-02

    申请人： Xiaowei Huang ,  Hongwei Li ,  Zhiqi Long ,  Xinlin Peng ,  Dali Cui ,  Guilin Yang ,  Xinghua Luo ,  Na Zhao ,  Yongqi Zhang

    发明人： Xiaowei Huang ,  Hongwei Li ,  Zhiqi Long ,  Xinlin Peng ,  Dali Cui ,  Guilin Yang ,  Xinghua Luo ,  Na Zhao ,  Yongqi Zhang

    IPC分类号： C01F17/00

    CPC分类号： C22B3/0067 ,  B01D11/0288 ,  B01D11/0492 ,  C01F17/0006 ,  C22B3/0005 ,  C22B3/0044 ,  C22B59/00 ,  Y02P10/234

    摘要： A process for pretreating organic extractants and its product and application in SX separation of rare earth. The pretreating method is that extractant and rare earth solution are mixed with powder or slurry of alkaline earth metal compound containing magnesium and/or calcium to realize pre-extraction, or the organic extractant are mixed with rare earth carbonate slurry to realize pre-extraction. When rare earth ion in aqueous phase is extracted into organic phase, the exchanged hydrogen ions enter into aqueous phase and dissolve the alkaline earth metal compound or the rare earth carbonate which helps to keep the acidity equilibrium of the system. The obtained organic extractant loaded with rare earth is used for unsaponificated SX separation of rare earth.With this method, there is no need to saponificate organic extractant with liquid ammonia or alkali, and there is no ammonia-nitrogen wastewater produced. So separation cost decrease at a large scale and a lot of the cost to treat the three wastes is cut. This method is applicable to SX separation for all rare earth elements in chloride, sulphate and nitrate system and has advantages of low investment and high profit.

    摘要翻译： 一种用于预处理有机萃取剂及其产品和在稀土SX分离中的应用的方法。 预处理方法是将萃取剂和稀土溶液与含有镁和/或钙的碱土金属化合物的粉末或浆料混合以实现预萃取，或者将有机萃取剂与稀土碳酸盐浆料混合以实现预萃取。 当水相中的稀土离子萃取到有机相中时，交换的氢离子进入水相并溶解碱土金属化合物或稀土碳酸盐，有助于保持体系的酸度平衡。 将所得到的装有稀土的有机萃取剂用于稀土的未分配的SX分离。 通过这种方法，不需要用液体氨或碱对有机萃取剂进行皂化，不产生氨氮废水。 因此，分离成本大幅度地下降，处理三种废物的成本大幅度下降。 该方法适用于氯化物，硫酸盐和硝酸盐体系中所有稀土元素的SX分离，具有投资低，利润高的优点。

    ALUMINATE PHOSPHOR CONTAINING BIVALENCE METAL ELEMENTS, ITS PREPARATION AND THE LIGHT EMITTING DEVICES INCORPORATING THE SAME
    6.
    发明申请
    ALUMINATE PHOSPHOR CONTAINING BIVALENCE METAL ELEMENTS, ITS PREPARATION AND THE LIGHT EMITTING DEVICES INCORPORATING THE SAME 有权
    含有金属元素的铝酸钠，其制备方法和同时发光的发光装置

    公开(公告)号：US20090218585A1

    公开(公告)日：2009-09-03

    申请号：US12465381

    申请日：2009-05-13

    申请人： Weidong ZHUANG ,  Yunsheng Hu ,  Zhen Long ,  Chusheng Zhang ,  Xiaowei Huang ,  Hongwei Li

    发明人： Weidong ZHUANG ,  Yunsheng Hu ,  Zhen Long ,  Chusheng Zhang ,  Xiaowei Huang ,  Hongwei Li

    IPC分类号： H01L33/00 ,  C09K11/85

    CPC分类号： C09K11/7774 ,  C09K11/778

    摘要： A phosphor can be excited by UV, purple or blue light LED, its production and the light emitting devices. The general formula of the phosphor is LnaMb(O,F)12:(R3+, M′2+)x, wherein, Ln is at least one metal element selected from a group consisting of Sc, Y, La, Pr, Nd, Gd, Ho, Yb and Sm, 2.6≦a≦3.4; M is at least one element selected from a group consisting of B, Al and Ga, 4.5≦b≦5.5; R is at least one metal element selected from a group consisting of Ce and Tb; M′ is at least one metal element selected from a group consisting of Ca, Sr, Ba, Mn and Zn, 0.001≦x≦0.4. The phosphor possesses broad emitting range, high efficiency, better uniformity and stability. A light emitting device can be obtained by incorporating this phosphor into a UV, purple or blue light emitting device.

    摘要翻译： 紫外线，紫光或蓝光LED，其生产和发光器件可以激发荧光体。 荧光体的通式为LnaMb（O，F）12：（R3 +，M'2 +）x，其中，Ln为选自Sc，Y，La，Pr，Nd， Gd，Ho，Yb和Sm，2.6 <= a <= 3.4; M是选自B，Al和Ga中的至少一种元素，4.5≤b≤5.5; R是选自Ce和Tb中的至少一种金属元素; M'是选自Ca，Sr，Ba，Mn和Zn中的至少一种金属元素，0.001≤x≤0.4。 荧光粉具有广泛的发光范围，高效率，更好的均匀性和稳定性。 通过将该荧光体掺入UV，紫色或蓝色发光器件中，可以获得发光器件。

    Phosphor, its preparation method and light emitting devices using the same
    7.
    发明授权
    Phosphor, its preparation method and light emitting devices using the same 有权
    荧光体及其制备方法和使用其的发光装置

    公开(公告)号：US07955524B2

    公开(公告)日：2011-06-07

    申请号：US12232604

    申请日：2008-09-19

    申请人： Weidong Zhuang ,  Yunsheng Hu ,  Zhen Long ,  Xiaowei Huang ,  Hongwei Li ,  Shusheng Zhang ,  Huagiang He

    发明人： Weidong Zhuang ,  Yunsheng Hu ,  Zhen Long ,  Xiaowei Huang ,  Hongwei Li ,  Shusheng Zhang ,  Huagiang He

    IPC分类号： C09K11/08 ,  C09K11/66 ,  C09K11/61

    CPC分类号： C09K11/7792 ,  C09K11/7774 ,  H01L33/502

    摘要： A phosphor can be excited by UV, purple or blue light LED, its preparation method, and light emitting devices incorporating the same. The phosphor contains rare earth, silicon, alkaline-earth metal, halogen, and oxygen, as well as aluminum or gallium. Its General formula of is aLn2O3.MO.bM′2O3.fSiO2.cAXe:dR, wherein Ln is at least one metal element selected from a group consisting of Sc, Y, La, Pr, Nd, Gd, Ho, Yb and Sm; M is at least one metal element selected from a group consisting of Ca, Sr and Ba; M′ is at least one metal element selected from Al and Ga; A is at least one metal element selected from a group consisting of Li, Na, K, Mg, Ca, Sr and Ba; X is at least one element selected from F and Cl; R is at least one metal element selected from a group consisting of Ce, Eu, Tb and Mn; 0.01≦a≦2, 0.35≦b≦4, 0.01≦c≦1, 0.01≦d≦0.3, 0.01≦f≦3, 0.6≦e≦2.4. The phosphor has broad emitting range, high efficiency, better uniformity and stability. A light emitting device is obtained by incorporating the phosphor into a UV, purple or blue light emitting device.

    摘要翻译： 可以通过紫外线，紫色或蓝色光LED，其制备方法和包含该荧光体的发光装置激发荧光体。 荧光体含有稀土，硅，碱土金属，卤素和氧，以及铝或镓。 其通式为aLn2O3.MO.bM'2O3.fSiO2.cAXe：dR，其中Ln是选自Sc，Y，La，Pr，Nd，Gd，Ho，Yb和Sm中的至少一种金属元素 ; M是选自Ca，Sr和Ba中的至少一种金属元素; M'是选自Al和Ga中的至少一种金属元素; A是选自Li，Na，K，Mg，Ca，Sr和Ba中的至少一种金属元素; X是选自F和Cl中的至少一种元素; R是选自Ce，Eu，Tb和Mn中的至少一种金属元素; 0.01＆nlE; a＆nlE; 2,0.35＆nlE; b＆nlE; 4,0.01＆nlE; c＆nlE; 1,0.01＆nlE; d＆nlE; 0.3,0.01＆nlE; f＆nlE; 3,0.6＆ 荧光体具有广泛的发光范围，高效率，更好的均匀性和稳定性。 通过将荧光体掺入UV，紫色或蓝色发光器件中来获得发光器件。

    Aluminate phosphor containing bivalence metal elements, its preparation and the light emitting devices incorporating the same
    8.
    发明授权
    Aluminate phosphor containing bivalence metal elements, its preparation and the light emitting devices incorporating the same 有权
    含有二价金属元素的铝酸盐荧光体及其制备方法及其结合的发光装置

    公开(公告)号：US07850869B2

    公开(公告)日：2010-12-14

    申请号：US12465381

    申请日：2009-05-13

    申请人： Weidong Zhuang ,  Yunsheng Hu ,  Zhen Long ,  Shusheng Zhang ,  Xiaowei Huang ,  Hongwei Li

    发明人： Weidong Zhuang ,  Yunsheng Hu ,  Zhen Long ,  Shusheng Zhang ,  Xiaowei Huang ,  Hongwei Li

    IPC分类号： C09K11/78

    CPC分类号： C09K11/7774 ,  C09K11/778

    摘要： A phosphor can be excited by UV, purple or blue light LED, its production and the light emitting devices. The general formula of the phosphor is LnaMb(O,F)12:(R3+,M′2+)x, wherein, Ln is at least one metal element selected from a group consisting of Sc, Y, La, Pr, Nd, Gd, Ho, Yb and Sm, 2.6≦a≦3.4; M is at least one element selected from a group consisting of B, Al and Ga, 4.5≦b≦5.5; R is at least one metal element selected from a group consisting of Ce and Tb; M′ is at least one metal element selected from a group consisting of Ca, Sr, Ba, Mn and Zn, 0.001≦x≦0.4. The phosphor possesses broad emitting range, high efficiency, better uniformity and stability. A light emitting device can be obtained by incorporating this phosphor into a UV, purple or blue light emitting device.

    摘要翻译： 紫外线，紫光或蓝光LED，其生产和发光器件可以激发荧光体。 荧光体的通式为LnaMb（O，F）12：（R3 +，M'2 +）x，其中，Ln为选自Sc，Y，La，Pr，Nd， Gd，Ho，Yb和Sm，2.6＆nlE; a＆nlE; 3.4; M是选自B，Al和Ga中的至少一种元素，4.5和nlE; b＆nlE; 5.5; R是选自Ce和Tb中的至少一种金属元素; M'是选自由Ca，Sr，Ba，Mn和Zn组成的组中的至少一种金属元素，0.001＆nlE; x＆nlE; 0.4。 荧光粉具有广泛的发光范围，高效率，更好的均匀性和稳定性。 通过将该荧光体掺入UV，紫色或蓝色发光器件中，可以获得发光器件。

    Phosphor, its preparation method and light emitting devices using the same
    9.
    发明申请
    Phosphor, its preparation method and light emitting devices using the same 有权
    荧光体及其制备方法和使用其的发光装置

    公开(公告)号：US20090050918A1

    公开(公告)日：2009-02-26

    申请号：US12232604

    申请日：2008-09-19

    申请人： Weidong Zhuang ,  Yunsheng Hu ,  Zhen Long ,  Xiaowei Huang ,  Hongwei Li ,  Shusheng Zhang ,  Huagiang He

    发明人： Weidong Zhuang ,  Yunsheng Hu ,  Zhen Long ,  Xiaowei Huang ,  Hongwei Li ,  Shusheng Zhang ,  Huagiang He

    IPC分类号： H01L33/00 ,  C09K11/79

    CPC分类号： C09K11/7792 ,  C09K11/7774 ,  H01L33/502

    摘要： A phosphor can be excited by UV, purple or blue light LED, its preparation method, and light emitting devices incorporating the same. The phosphor contains rare earth, silicon, alkaline-earth metal, halogen, and oxygen, as well as aluminum or gallium. Its General formula of is aLn2O3.MO.bM′2O3.fSiO2.cAXe: dR, wherein Ln is at least one metal element selected from a group consisting of Sc, Y, La, Pr, Nd, Gd, Ho, Yb and Sm; M is at least one metal element selected from a group consisting of Ca, Sr and Ba; M′ is at least one metal element selected from Al and Ga; A is at least one metal element selected from a group consisting of Li, Na, K, Mg, Ca, Sr and Ba; X is at least one element selected from F and Cl; R is at least one metal element selected from a group consisting of Ce, Eu, Tb and Mn; 0.01≦a≦2, 0.35≦b≦4, 0.01≦c≦1, 0.01≦d≦0.3, 0.01≦f≦3, 0.6≦e≦2.4. The phosphor has broad emitting range, high efficiency, better uniformity and stability. A light emitting device is obtained by incorporating the phosphor into a UV, purple or blue light emitting device.

    摘要翻译： 可以通过紫外线，紫色或蓝色光LED，其制备方法和包含该荧光体的发光装置激发荧光体。 荧光体含有稀土，硅，碱土金属，卤素和氧，以及铝或镓。 其通式为aLn2O3.MO.bM'2O3.fSiO2.cAXe：dR，其中Ln是选自Sc，Y，La，Pr，Nd，Gd，Ho，Yb和Sm中的至少一种金属元素 ; M是选自Ca，Sr和Ba中的至少一种金属元素; M'是选自Al和Ga中的至少一种金属元素; A是选自Li，Na，K，Mg，Ca，Sr和Ba中的至少一种金属元素; X是选自F和Cl中的至少一种元素; R是选自Ce，Eu，Tb和Mn中的至少一种金属元素; 0.01 <= a <= 2，0.35 <= b <= 4，0.01 <= c <= 1，0.01 <= d <= 0.3,0.01 <= f <= 3，0.6 <= e <= 2.4。 荧光体具有广泛的发光范围，高效率，更好的均匀性和稳定性。 通过将荧光体掺入UV，紫色或蓝色发光器件中来获得发光器件。