公开(公告)号：US07019099B2

公开(公告)日：2006-03-28

申请号：US10621380

申请日：2003-07-18

申请人： Yi Yeol Lyu ,  Jin Heong Yim ,  Sang Kook Mah ,  Eun Ju Nah ,  Il Sun Hwang ,  Hyun Dam Jeong ,  Jung Hyung Kim

发明人： Yi Yeol Lyu ,  Jin Heong Yim ,  Sang Kook Mah ,  Eun Ju Nah ,  Il Sun Hwang ,  Hyun Dam Jeong ,  Jung Hyung Kim

IPC分类号： C08G77/18

CPC分类号： H01L21/02126 ,  C08G77/04 ,  C08G77/50 ,  H01B3/46 ,  H01L21/02203 ,  H01L21/02216 ,  H01L21/02282 ,  H01L21/3124 ,  H01L21/31695

摘要： Disclosed herein are siloxane-based resins prepared by hydrolyzing and polycondensing cyclic and/or cage-shape siloxane compounds, optionally with at least one silane compound, in an organic solvent in the presence of a catalyst and water. Also, disclosed herein are methods for forming insulating film between interconnect layers in semiconductor devices by using the siloxane-based resins thus prepared as low dielectric insulating materials.

公开(公告)号：US06623711B2

公开(公告)日：2003-09-23

申请号：US10105723

申请日：2002-03-27

申请人： Yi Yeol Lyu ,  Jin Heong Yim ,  Sang Kook Mah ,  Eun Ju Nah ,  Il Sun Hwang ,  Hyun Dam Jeong ,  Jung Hyung Kim

发明人： Yi Yeol Lyu ,  Jin Heong Yim ,  Sang Kook Mah ,  Eun Ju Nah ,  Il Sun Hwang ,  Hyun Dam Jeong ,  Jung Hyung Kim

IPC分类号： C22B6002

CPC分类号： H01L21/02126 ,  C08G77/04 ,  C08G77/50 ,  H01B3/46 ,  H01L21/02203 ,  H01L21/02216 ,  H01L21/02282 ,  H01L21/3124 ,  H01L21/31695

摘要： Disclosed herein are siloxane-based resins prepared by hydrolyzing and polycondensing cyclic and/or cage-shape siloxane compounds, optionally with at least one silane compound, in an organic solvent in the presence of a catalyst and water. Also, disclosed herein are methods for forming insulating film between interconnect layers in semiconductor devices by using the siloxane-based resins thus prepared as low dielectric insulating materials.

摘要翻译： 本文公开了通过在有机溶剂中在催化剂和水的存在下水解和缩聚环状和/或笼形硅氧烷化合物，任选地与至少一种硅烷化合物制备的硅氧烷基树脂。 此外，本文公开了通过使用如此制备的作为低介电绝缘材料的硅氧烷类树脂在半导体器件中的互连层之间形成绝缘膜的方法。

公开(公告)号：US06660822B2

公开(公告)日：2003-12-09

申请号：US09895158

申请日：2001-07-02

申请人： Yi Yeol Lyu ,  Jin Heong Yim ,  Sang Kook Mah ,  Eun Ju Nah ,  Il Sun Hwang ,  Hyun Dam Jeong ,  Jin Gyu Lee

发明人： Yi Yeol Lyu ,  Jin Heong Yim ,  Sang Kook Mah ,  Eun Ju Nah ,  Il Sun Hwang ,  Hyun Dam Jeong ,  Jin Gyu Lee

IPC分类号： C08G7718

CPC分类号： H01L21/02126 ,  C08G77/50 ,  C09D183/14 ,  H01L21/02216 ,  H01L21/02282 ,  H01L21/3122

摘要： The present invention provides a method for forming insulating film between interconnect layers in microelectronic devices, said method comprising the steps of: preparing siloxane-based resins by hydrolyzing and polycondensing the compound represented by the following formula (1), with or without the compound represented by the following formula (2), in an organic solvent in the presence of a catalyst and water; coating a silicon substrate with the siloxane-based resins dissolved in an organic solvent; and heat-curing the resulting coating film:  RSiX1X2X3  [2] in which, R is hydrogen atom, C1˜C3 alkyl group, C3˜C10 cycloalkyl group, or C6˜C15 aryl group; X1, X2 and X3 are independently C1˜C3 alkyl group, C1˜C10 alkoxy group, or halogen atom; n is an integer ranging from 3 to 8; and m is an integer ranging from 1 to 10.

摘要翻译： 本发明提供了一种在微电子器件中在互连层之间形成绝缘膜的方法，所述方法包括以下步骤：通过将下式（1）表示的化合物水解和缩聚来制备硅氧烷基树脂，所述化合物或不含有化合物 通过下式（2）在有机溶剂中在催化剂和水的存在下反应; 用溶解在有机溶剂中的硅氧烷基树脂涂覆硅衬底; 对所得涂膜进行热固化，其中R为氢原子，C1〜C3烷基，C3〜C10环烷基或C6〜C15芳基; X1，X2和X3独立为C1〜C3烷基，C1 〜C10烷氧基或卤原子; n为3〜8的整数， andm为1〜10的整数。

公开(公告)号：US06632748B2

公开(公告)日：2003-10-14

申请号：US09961449

申请日：2001-09-25

申请人： Jin Heong Yim ,  Yi Yeol Lyu ,  Sang Kook Mah ,  Eun Ju Nah ,  Il Sun Hwang ,  Keun Byoung Yoon

发明人： Jin Heong Yim ,  Yi Yeol Lyu ,  Sang Kook Mah ,  Eun Ju Nah ,  Il Sun Hwang ,  Keun Byoung Yoon

IPC分类号： H01L2131

CPC分类号： H01L21/31695 ,  C08L5/16 ,  H01L21/02126 ,  H01L21/02203 ,  H01L21/02216 ,  H01L21/02282 ,  H01L21/3124 ,  C08L2666/02

摘要： The present invention provides a composition for preparing substances having nano-pores, said composition comprising cyclodextrin derivative, thermo-stable organic or inorganic matrix precursor, and solvent for dissolving said two solid components. There is also provided an interlayer insulating film having evenly distributed nano-pores with a diameter less than 50 Å, which is required for semiconductor devices.

摘要翻译： 本发明提供一种用于制备具有纳米孔的物质的组合物，所述组合物包含环糊精衍生物，热稳定性有机或无机基质前体，以及用于溶解所述两种固体组分的溶剂。 还提供了具有均匀分布的纳米孔的层间绝缘膜，其直径小于等于半导体器件所需的纳米孔。

公开(公告)号：US08389196B2

公开(公告)日：2013-03-05

申请号：US12678489

申请日：2008-09-19

申请人： Woo Young Yang ,  Keon Il Kim ,  Dae Il Hwang ,  Il Hyuk Kim ,  Jae Bum Park ,  Il Sun Hwang ,  Jae Kwang Hwang ,  Dae Woong Choi ,  Dong Won Kim ,  Duck Kyun Ahn

发明人： Woo Young Yang ,  Keon Il Kim ,  Dae Il Hwang ,  Il Hyuk Kim ,  Jae Bum Park ,  Il Sun Hwang ,  Jae Kwang Hwang ,  Dae Woong Choi ,  Dong Won Kim ,  Duck Kyun Ahn

IPC分类号： G03G9/08

CPC分类号： G03G9/0806 ,  G03G9/0819 ,  G03G9/0827

摘要： Provided is a method of preparing a toner, the method including: preparing a solvent emulsion by stirring a medium including a polar medium, an organic solvent, and a surfactant; adding toner components including a resin and a pigment to the solvent emulsion; removing the organic solvent from the solvent emulsion including the toner components; and collecting a toner particle from the solvent emulsion from which the organic solvent is removed.

摘要翻译： 提供一种调色剂的制备方法，该方法包括：通过搅拌包含极性介质，有机溶剂和表面活性剂的介质来制备溶剂乳液; 向所述溶剂乳液中添加包括树脂和颜料的调色剂组分; 从包括调色剂组分的溶剂乳液中除去有机溶剂; 并从除去有机溶剂的溶剂乳液中收集调色剂颗粒。

公开(公告)号：US20100232837A1

公开(公告)日：2010-09-16

申请号：US12739706

申请日：2008-10-22

申请人： Dae Il Hwang ,  Woo Young Yang ,  Keon Il Kim ,  Il Hyuk Kim ,  Jae Bum Park ,  Il Sun Hwang ,  Jae Kwang Hwang ,  Dae Woong Choi ,  Dong Won Kim ,  Duck Kyun Ahn

发明人： Dae Il Hwang ,  Woo Young Yang ,  Keon Il Kim ,  Il Hyuk Kim ,  Jae Bum Park ,  Il Sun Hwang ,  Jae Kwang Hwang ,  Dae Woong Choi ,  Dong Won Kim ,  Duck Kyun Ahn

IPC分类号： G03G15/08 ,  G03G9/08 ,  G03G9/097 ,  G03G9/09 ,  G03G9/093

CPC分类号： G03G9/09392 ,  G03G9/09328 ,  G03G9/09342 ,  G03G9/09371 ,  G03G9/09378 ,  G03G9/09385

摘要： A toner has a core-shell structure including a toner core portion having a resin with an active hydrogenactive hydrogen containing group, a colorant and at least one additive, and a toner shell portion surrounding the toner core portion, wherein the toner shell portion includes a cross-linked resin prepared by reaction of at least a portion of the active hydrogen containing group and the cross-linking agent.

摘要翻译： 调色剂具有芯壳结构，其包括具有含活性氢活性氢基团的树脂的调色剂核心部分，着色剂和至少一种添加剂，以及包围调色剂核心部分的调色剂壳体部分，其中调色剂壳体部分包括 通过至少一部分含活性氢的基团与交联剂的反应制备的交联树脂。

公开(公告)号：US08389188B2

公开(公告)日：2013-03-05

申请号：US12739699

申请日：2008-10-22

申请人： Dong Won Kim ,  Woo Young Yang ,  Keon Il Kim ,  Dae Il Hwang ,  Il Hyuk Kim ,  Jae Bum Park ,  Il Sun Hwang ,  Jae Kwang Hwang ,  Dae Woong Choi ,  Duck Kyun Ahn

发明人： Dong Won Kim ,  Woo Young Yang ,  Keon Il Kim ,  Dae Il Hwang ,  Il Hyuk Kim ,  Jae Bum Park ,  Il Sun Hwang ,  Jae Kwang Hwang ,  Dae Woong Choi ,  Duck Kyun Ahn

IPC分类号： G03G9/087

CPC分类号： G03G9/08793 ,  G03G9/0804 ,  G03G9/0825

摘要： Provided are a toner using a resin having an active hydrogen-containing group, and a method of preparing the toner. The toner using a resin having an active hydrogen-containing group includes a binder resin (A), a cross-linked resin including a THF insoluble content of 99-100 weight %, a colorant, and at least one additive. The cross-linked resin is arranged in the form of a plurality of islands in each particle of the toner.

摘要翻译： 提供使用具有含活性氢基团的树脂的调色剂和调色剂的制备方法。 使用具有含活性氢基团的树脂的调色剂包括粘合剂树脂（A），包含不饱和THF含量为99-100重量％的交联树脂，着色剂和至少一种添加剂。 交联树脂以调色剂的每个颗粒中的多个岛的形式布置。

公开(公告)号：US20120288793A1

公开(公告)日：2012-11-15

申请号：US13574698

申请日：2011-02-01

申请人： Dong Won Kim ,  Sung Yul Kim ,  Bo Young Kim ,  Il Sun Hwang ,  Sung Soon Kim

发明人： Dong Won Kim ,  Sung Yul Kim ,  Bo Young Kim ,  Il Sun Hwang ,  Sung Soon Kim

IPC分类号： G03G9/08

CPC分类号： G03G9/08795 ,  G03G9/0806 ,  G03G9/08755 ,  G03G9/08797

摘要： Disclosed is a method for producing toner. The method for producing toner by emulsion aggregation according to the present invention, comprises adjusting viscosity at a homogenization stage, to thereby obtain toner particles having a dense particle size distribution via a simple process.

摘要翻译： 公开了一种生产调色剂的方法。 根据本发明的通过乳液聚集制造调色剂的方法包括在均质阶段调节粘度，从而通过简单的方法获得具有致密粒度分布的调色剂颗粒。

公开(公告)号：US20110159424A1

公开(公告)日：2011-06-30

申请号：US12996365

申请日：2009-06-04

申请人： Dae Woong Choi ,  Woo Young Yang ,  Keon Il Kim ,  Dae Il Hwang ,  Il Hyuk Kim ,  Jae Bum Park ,  Il Sun Hwang ,  Jae Kwang Hwang ,  Dong Won Kim ,  Duck Kyun Ahn

发明人： Dae Woong Choi ,  Woo Young Yang ,  Keon Il Kim ,  Dae Il Hwang ,  Il Hyuk Kim ,  Jae Bum Park ,  Il Sun Hwang ,  Jae Kwang Hwang ,  Dong Won Kim ,  Duck Kyun Ahn

IPC分类号： G03G13/06 ,  G03G9/08

CPC分类号： G03G9/0906 ,  G03G9/0821 ,  G03G9/0908 ,  G03G9/0924 ,  G03G9/0926 ,  G03G9/09392

摘要： Provided are a method of forming a toner image and an electrophotographic image forming apparatus including a toner. The method of forming a toner image is performed using a first toner having a yellow color and color coordinate values of a lightness (L) ranging from 91 to 94, a redness (a) ranging from −11 to −9, and a yellowness (b) ranging from 77 to 82; a second toner having a magenta color and color coordinate values of a lightness (L) ranging from 56 to 61, a redness (a) ranging from 56 to 61, and a yellowness (b) ranging from −7 to −5; and a third toner having a cyan color and color coordinate values of a lightness (L) ranging from 58 to 62, a redness (a) ranging from −33 to −30, and a yellowness (b) ranging from −42 to −37.

摘要翻译： 提供了形成调色剂图像的方法和包括调色剂的电子照相图像形成装置。 形成调色剂图像的方法是使用具有黄色的第一调色剂和亮度（L）为91至94，红度（a）为-11至-9，以及黄度（ b）从77到82; 具有品红色的第二调色剂和亮度（L）为56至61，红度（a）为56至61，黄度（b）为-7至-5的色坐标值; 并且具有青色的第三调色剂和亮度（L）为58至62，红度（a）为-33至-30，和黄度（b）范围为-42至-37的色坐标值 。

公开(公告)号：US20110028643A1

公开(公告)日：2011-02-03

申请号：US12936513

申请日：2009-03-30

申请人： Dae Il Hwang ,  Il Sun Hwang ,  Duck Kyun Ahn ,  Woo Young Yang

发明人： Dae Il Hwang ,  Il Sun Hwang ,  Duck Kyun Ahn ,  Woo Young Yang

IPC分类号： C08L67/00 ,  C08G63/91

CPC分类号： C08L67/00 ,  C08G63/20 ,  C08L25/14 ,  C08L67/02 ,  C08L91/06 ,  C08L2666/02

摘要： A wax-resin compatibilizer, a wax-resin dispersion, and methods of preparing the wax-resin dispersion. The wax-resin dispersion includes a wax, the wax-resin compatibilizer, and a second resin. The wax-resin dispersion may have a high wax content and excellent storage stability.

摘要翻译： 蜡 - 树脂增容剂，蜡 - 树脂分散体和蜡 - 树脂分散体的制备方法。 蜡树脂分散体包括蜡，蜡 - 树脂增容剂和第二树脂。 蜡 - 树脂分散体可具有高蜡含量和优异的储存稳定性。