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1.发明授权Basic zinc compound flake-like crystalline particle and method for preparation thereof 失效碱性锌化合物片状结晶粒子及其制备方法
公开(公告)号：US4261965A
公开(公告)日：1981-04-14
申请号：US48462
申请日：1979-06-14
CPC分类号： C01G9/06
摘要： Basic zinc compound flake-like crystalline material suited for use in crystal-oriented electronic devices and method for preparation thereof comprising the steps of preparing a solution including at least zinc ions and sulfate ions, and causing precipitation of zinc sulfate crystals by causing a reaction of components of said solution with alkali when said solution is at a temperature in the range 50.degree. to 100.degree. C. and has a pH value of in the range 4 to 6.5.
摘要翻译： 适用于结晶取向电子器件的碱性锌化合物片状结晶材料及其制备方法，包括以下步骤：制备至少包含锌离子和硫酸根离子的溶液，并通过引起硫酸锌晶体的沉淀 当所述溶液在50℃至100℃的温度范围内时，所述溶液与碱的组分，其pH值在4至6.5范围内。
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2.发明授权
公开(公告)号：US4272397A
公开(公告)日：1981-06-09
申请号：US44102
申请日：1979-05-31
CPC分类号： C09K11/565
摘要： Flake-like ceramic particles of zinc sulfide phosphor and method of preparing the same including the steps of preparing flake-like particles of basic zinc sulfate crystal doped with activator, sulfurizing in the particles carbon disulfide, and heating the sulfurized particles in hydrogen sulfide. Particularly by steeping said particles in a solution of alkaline earth metal salt prior to or after sulfurizing, grain growth in ceramic particles can be improved.
摘要翻译： 硫化锌荧光粉片状陶瓷颗粒及其制备方法，包括制备掺杂有活化剂的碱式硫酸锌晶体的片状颗粒，二硫化碳中硫化，硫化氢中加硫硫化颗粒的步骤。 特别是通过在硫化之前或之后将所述颗粒浸入碱土金属盐溶液中，可以提高陶瓷颗粒中的晶粒生长。
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公开(公告)号：US4303913A
公开(公告)日：1981-12-01
申请号：US63701
申请日：1979-08-06
申请人： Takao Tohda , Tsuneharu Nitta , Yoji Fukuda , Tomizo Matsuoka , Ziro Terada
发明人： Takao Tohda , Tsuneharu Nitta , Yoji Fukuda , Tomizo Matsuoka , Ziro Terada
CPC分类号： C09K11/7729 , H01J29/20 , H01J31/15
摘要： A fluorescent display device comprising at least one phosphor screen composed of a mixture of a SnO.sub.2 :Eu phosphor with at least one of the cathodoluminescent phosphors having emission spectra and exitation properties different from SnO.sub.2 :Eu phosphor. This fluorescent display device emits light of different colors when driven at different voltages and at pulse voltages of different duty cycles. A display apparatus comprises such a fluorescent display device and a driving device with variable output voltage.
摘要翻译： 一种荧光显示装置，包括至少一个由SnO 2：Eu荧光粉与至少一种阴极发光荧光体的混合物构成的荧光屏，其具有不同于SnO 2：Eu荧光体的发射光谱和引发性质。 当在不同的电压和不同占空比的脉冲电压下驱动时，该荧光显示装置发射不同颜色的光。 显示装置包括这种荧光显示装置和具有可变输出电压的驱动装置。
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公开(公告)号：US4314178A
公开(公告)日：1982-02-02
申请号：US225323
申请日：1981-01-15
CPC分类号： H01J31/15 , C09K11/7729 , H01J63/06
摘要： A red emission fluorescent display device employing improved SnO.sub.2 :Eu phosphor as a low-energy-electron excitation phosphor. The phosphor is manufactured by the following steps:To a starting material selected from the group consisting of at least one of metallic tin, stannous and stannic halide and stannous sulfate, europium oxide is added in the amount of 5.times.10.sup.-2 to 10 atomic % europium to tin. The mixture is heated and stirred with nitric acid until it becomes dry due to evaporation of the solvent water and unreacted nitric acid, thereby forming a mixed powder of metastannic acid and europium. Then the powder is subjected to heat treatment, causing the metastannic acid to thermally decompose and the europium to diffuse into the stannic oxide matrix.The device exhibts remarkably high luminescence intensity and it is possible to achieve the intensity of 26f.L or more under the E.sub.b of 10 V and the I.sub.b of 1.5 mA/cm.sup.2.
摘要翻译： 一种使用改进的SnO 2：Eu荧光体作为低能量电子激发荧光体的红色发射荧光显示装置。 荧光体通过以下步骤制造：向选自金属锡，亚锡和锡卤化物和硫酸锡中的至少一种的原料中加入氧化铕，量为5×10 -2至10原子％的铕 锡。 将混合物与硝酸一起加热并搅拌直至由于溶剂水和未反应的硝酸的蒸发而变干，从而形成偏亚氨酸和铕的混合粉末。 然后对粉末进行热处理，导致偏钛酸热分解，铕扩散到锡氧化物基质中。 该器件具有显着高的发光强度，并且可以在10V的Eb和1.5mA / cm 2的Ib下实现26f.L或更高的强度。
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公开(公告)号：US4314177A
公开(公告)日：1982-02-02
申请号：US225322
申请日：1981-01-15
CPC分类号： H01J31/15 , C09K11/7729 , H01J63/06
摘要： A red emission fluorescent display device employing improved SnO.sub.2 :Eu phosphor as a low-energy-electron excitation phosphor. The phosphor is manufactured by the following steps:An aqueous solution of a mixture of europium and at least one material selected from stannous halides and stannous sulfate is prepared. The amount of europium ion is adjusted so that the ratio thereof to tin ions ranges between 5.times.10.sup.-2 and 10 atomic %. The solution is poured into and mixed with a hot aqueous solution including oxalic ions, while the mixed solution is being stirred, to form oxalate coprecipitates of tin and europium. After being dryed the coprecipitate is heated so as to be thermally decomposed and then is subjected to heat treatment at the temperature above that for the thermal decomposition, whereby europium ions are diffused into the stannic oxide matrix.The device exhibits remarkably high luminescence intensity which is satisfactory for practical use.
摘要翻译： 使用改进的SnO 2：Eu荧光体作为低能量电子激发荧光体的红色发射荧光显示装置。 通过以下步骤制造荧光体：制备铕与选自亚锡卤化物和硫酸亚锡的至少一种材料的混合物的水溶液。 调整铕离子的量使得其与锡离子的比例在5×10 -2至10原子％之间。 将溶液倒入含有草酸离子的热水溶液中混合，同时搅拌混合溶液，形成锡和铕的草酸盐共沉淀物。 干燥后，将共沉淀物加热分解，然后在高于热分解的温度下进行热处理，由此铕离子扩散到锡氧化物基质中。 该装置显示出非常高的发光强度，这对于实际使用是令人满意的。
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公开(公告)号：US4668582A
公开(公告)日：1987-05-26
申请号：US713597
申请日：1985-03-19
CPC分类号： C23C14/08 , C23C28/00 , H05B33/22 , Y10S428/917
摘要： New black color insulator thin films comprising Pr oxide, composite oxides of Pr-Mn, Pr-Ni, Pr-Co or Mn oxide are used to constitute at least one part or all parts of interface film between a phosphor film and a back electrode film of an AC thin film EL panel; and the panel with such a high contrast as 5:1 even at an illumination of 400 lux has been obtained.
摘要翻译： 包括Pr氧化物，Pr-Mn，Pr-Ni，Pr-Co或Mn氧化物的复合氧化物的新型黑色绝缘体薄膜用于构成荧光体膜和背面电极膜之间的界面膜的至少一部分或全部部分 的AC薄膜EL面板; 并且已经获得了即使在400勒克司的照明下具有5:1的如此高的对比度的面板。
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7.发明授权Electroluminescence display device containing a zinc sulfide emission layer with rare earth elements and/or halides thereof and phosphorus 失效含有稀土元素和/或其卤化物和磷的硫化锌发射层的电致发光显示装置
公开(公告)号：US4733128A
公开(公告)日：1988-03-22
申请号：US673557
申请日：1984-10-05
申请人： Takao Tohda , Yosuke Fujita , Masahiro Nishikawa , Tomizo Matsuoka , Atsushi Abe , Tsuneharu Nitta
发明人： Takao Tohda , Yosuke Fujita , Masahiro Nishikawa , Tomizo Matsuoka , Atsushi Abe , Tsuneharu Nitta
IPC分类号： C09K11/00 , C09K11/08 , C09K11/56 , G09F9/30 , G09F9/33 , H05B33/10 , H05B33/12 , H05B33/14 , H05B33/18
CPC分类号： H05B33/14 , C09K11/565 , H05B33/10 , H05B33/18
摘要： An electroluminescense display device having a emission layer comprising zinc sulfide characterized in that at least one member selected from the group consisting of rare earth elements, manganese, copper, silver, magnesium, aluminum and their halides is contained as an activator, as well as at least one member selected from the group consisting of nitrogen, phosphorus, arsenic and antimony is contained as a coactivator. Said emission layer is formed by sputtering by using, as a target, zinc sulfide containing said activator and coactivator. Said sputtering is conducted in an atmosphere comprising a rare gas or rare gas containing a sulfide gas. The electroluminescence display device of the present invention has a higher brightness than conventional device with a good repeatability.
摘要翻译： PCT No.PCT / JP84 / 00036 Sec。 371日期1984年10月5日 102（e）日期1984年10月5日PCT提交1984年2月9日PCT公布。 第WO84 / 03099号公报 日本1984年8月16日。一种具有包含硫化锌的发射层的电致发光显示装置，其特征在于，含有选自稀土元素，锰，铜，银，镁，铝及其卤化物中的至少一种成分被包含为 含有活化剂，以及选自氮，磷，砷和锑中的至少一种作为共激活剂。 通过使用含有所述活化剂和共激活剂的硫化锌作为目标，通过溅射形成所述发射层。 所述溅射是在包含含有硫化物气体的稀有气体或稀有气体的气氛中进行的。 本发明的电致发光显示装置具有比具有良好重复性的常规装置更高的亮度。
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公开(公告)号：US4547703A
公开(公告)日：1985-10-15
申请号：US576394
申请日：1984-01-26
申请人： Yosuke Fujita , Takao Tohda , Tomizo Matsuoka , Atsushi Abe , Tsuneharu Nitta
发明人： Yosuke Fujita , Takao Tohda , Tomizo Matsuoka , Atsushi Abe , Tsuneharu Nitta
CPC分类号： H05B33/22 , H01B3/12 , Y10S428/917
摘要： In a thin film electroluminescent element comprising a phosphor thin film, a dielectric thin film disposed on at least one of the surfaces of the phosphor thin film and electrodes for applying a voltage across the thin films, the aforementioned dielectric thin film is formed of a dielectric material expressed by a general formula of AB.sub.2 O.sub.6 (where A represents a divalent metal element and B represents a pentavalent metal element). By employing the dielectric material, the voltage for driving a thin film electroluminescent element can be lowered without decreasing the brightness of the element. Further, by using a composite dielectric thin film in which the dielectric thin film expressed by the aforementioned general formula AB.sub.2 O.sub.6 is laminated with a dielectric thin film which is not susceptible to dielectric breakdown of self-healing type, the composite dielectric thin film is made susceptible to the dielectric breakdown of self-healing type. Additionally, the value of product of the dielectric breakdown field intensity and dielectric constant is increased to obtain a thin film electroluminescent element having excellent characteristics.
摘要翻译： PCT No.PCT / JP83 / 00164 Sec。 371日期1984年1月26日 102（e）日期1984年1月26日PCT提交1983年5月26日PCT公布。 出版物WO83 / 04339 日本1983年12月8日。在包括荧光体薄膜的薄膜电致发光元件中，设置在荧光体薄膜的至少一个表面上的电介质薄膜和用于在薄膜上施加电压的电极，上述电介质 由通式AB 2 O 6（其中A表示二价金属元素，B表示五价金属元素）表示的电介质材料形成薄膜。 通过使用介电材料，可以降低用于驱动薄膜电致发光元件的电压而不降低元件的亮度。 此外，通过使用其中由上述通式AB 2 O 6表示的电介质薄膜与不易受自愈型电介质击穿的电介质薄膜层压的复合电介质薄膜，使复合电介质薄膜变得易受影响 对自愈型的介电击穿。 此外，提高介电击穿场强和介电常数的乘积值以获得具有优异特性的薄膜电致发光元件。
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公开(公告)号：US4814668A
公开(公告)日：1989-03-21
申请号：US140867
申请日：1987-12-23
申请人： Takao Tohda , Tomizo Matsuoka , Yosuke Fujita , Atsushi Abe , Tsuneharu Nitta
发明人： Takao Tohda , Tomizo Matsuoka , Yosuke Fujita , Atsushi Abe , Tsuneharu Nitta
摘要： An electroluminescent display device comprising an electroluminescent emitting layer including zinc oxide containing a luminescent active material, an insulating layer formed on one surface of the electroluminescent emitting layer and a pair of energizing means for applying signal voltages corresponding to an information to be displayed to a multilayer assembly including the said two layers, characterized in that a plurality of semiconductor layers each containing at least one chemical compound selected from the group consisting of chemical compounds of the II-VI groups and tin oxide are arranged as one of the energizing means arranged on the side of the electroluminescent emitting layer or between the energizing means arranged on the side of the electroluminescent emitting layer and the electroluminescent emitting layer. This device features that it requires only a reduced drive voltage for image displaying purposes and ensures an increased luminescent brightness.
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公开(公告)号：US4664985A
公开(公告)日：1987-05-12
申请号：US654841
申请日：1984-09-25
申请人： Tomizo Matsuoka , Yosuke Fujita , Jun Kuwata , Atsushi Abe , Tsuneharu Nitta
发明人： Tomizo Matsuoka , Yosuke Fujita , Jun Kuwata , Atsushi Abe , Tsuneharu Nitta
IPC分类号： H05B33/14 , G09F9/30 , H01B3/12 , H05B33/12 , H05B33/22 , B32B9/00 , B32B19/00 , H01J1/62 , H01J63/04
CPC分类号： H01B3/12 , H05B33/22 , Y10S428/917
摘要： An electroluminescent element, especially a thin-film electroluminescent element in which the dielectric film layer provided on at least one side of an electroluminor layer is essentially composed of the materials represented by the following compositional formula:x(Ti.sub.1-s A.sub.s O.sub.2) and y(Sr.sub.1-t B.sub.t O)wherein A is at least one member selected from the group consisting of Zr, Hf and Sn, and B is at least one member selected from the group consisting of Mg, Ba and Ca. In the above formula, x+y=100 mol %, 0.ltoreq.s
摘要翻译： 电致发光元件，特别是薄膜电致发光元件，其中设置在电致发光层的至少一侧的电介质膜层基本上由以下组成式表示的材料组成：x（Ti1-sAsO2）和y（Sr1 tBtO），其中A是选自Zr，Hf和Sn中的至少一种，B是选自Mg，Ba和Ca中的至少一种。 在上式中，x + y = 100摩尔％，0≤s≤1,0
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