PROCESS FOR PRODUCING HIGH PURITY NICKEL SULFATE

    公开(公告)号:US20240317604A1

    公开(公告)日:2024-09-26

    申请号:US18578923

    申请日:2022-07-07

    CPC classification number: C01G53/10 C01D5/02 C01D5/16

    Abstract: The present invention is to provide a process for removing magnesium contained as an impurity from nickel sulfate and producing high-purity nickel sulfate.
    The process for producing an aqueous nickel sulfate solution from which magnesium is removed from nickel sulfate, comprises the following steps (1) to (3):



    (1) a carbonation step obtaining a slurry comprising nickel carbonate as a solid content by mixing a nickel sulfate aqueous solution and lithium carbonate,
    (2) a solid-liquid separation step of separating the slurry obtained in the carbonation step into a solid content and liquid component, and
    (3) a dissolution step dissolving the solid content obtained in said solid-liquid separation step with a solution containing sulfuric acid.

    SOFT MAGNETIC MATERIAL, POWDER MAGNETIC CORE AND METHOD OF MANUFACTURING SOFT MAGNETIC MATERIAL
    7.
    发明申请
    SOFT MAGNETIC MATERIAL, POWDER MAGNETIC CORE AND METHOD OF MANUFACTURING SOFT MAGNETIC MATERIAL 有权
    软磁材料,粉末磁芯和制造软磁材料的方法

    公开(公告)号:US20100255188A1

    公开(公告)日:2010-10-07

    申请号:US12816833

    申请日:2010-06-16

    Abstract: A soft magnetic material is a soft magnetic material including a composite magnetic particle (30) having a metal magnetic particle (10) mainly composed of Fe and an insulating coating (20) covering metal magnetic particle (10), and insulating coating (20) contains an iron phosphate compound and an aluminum phosphate compound. The atomic ratio of Fe contained in a contact surface of insulating coating (20) in contact with metal magnetic particle (10) is larger than the atomic ratio of Fe contained in the surface of insulating coating (20). The atomic ratio of Al contained in the contact surface of insulating coating (20) in contact with metal magnetic particle (10) is smaller than the atomic ratio of Al contained in the surface of insulating coating (20). Thus, iron loss can be reduced.

    Abstract translation: 软磁性材料是包括具有主要由Fe构成的金属磁性粒子(10)和覆盖金属磁性粒子(10)的绝缘涂层(20)的复合磁性体(30)和绝缘涂层(20)的软磁性材料, 含有磷酸铁化合物和磷酸铝化合物。 包含在与金属磁性颗粒(10)接触的绝缘涂层(20)的接触表面中的Fe的原子比大于绝缘涂层(20)表面中所含的Fe的原子比。 绝缘涂层(20)与金属磁性颗粒(10)接触的接触表面中所含的Al的原子比小于绝缘涂层(20)表面中的Al的原子比。 因此,可以减少铁损。

    Process for producing acicular geothite particles and acicular magnetic
iron oxide particles
    10.
    发明授权
    Process for producing acicular geothite particles and acicular magnetic iron oxide particles 失效
    生产针状地质颗粒和针状磁性氧化铁颗粒的方法

    公开(公告)号:US5378380A

    公开(公告)日:1995-01-03

    申请号:US22847

    申请日:1993-02-25

    Abstract: Disclosed herein are a process for producing acicular goethite particles comprising the step of: blowing an oxygen-containing gas into a ferrous salt reaction solution containing colloidal ferrous hydroxide or iron-containing colloidal precipitates which is obtained by reacting an aqueous ferrous salt solution with less than one equivalent of an aqueous alkali hydroxide solution, an aqueous alkali carbonate solution, or an aqueous alkali hydroxide and alkali carbonate solution based on Fe.sup.2+ in said aqueous ferrous salt solution, in the presence of ascorbic acid or a salt thereof so as to oxidize said colloidal ferrous hydroxide or iron-containing colloidal precipitates and to produce acicular goethite particles throught green rust; and a process for producing acicular magnetic iron oxide particles by reducing the acicular goethite particles obtained in the above process to produce acicular magnetite particles, and if necessary, oxidizing the acicular magnetite particles to obtain acicular maghemite particles, and if necessary, modifying the acicular magnetite or maghemite particles with Co or Co and Fe.sup.2+.

    Abstract translation: 本文公开了一种制备针状针铁矿颗粒的方法,包括以下步骤:将含氧气体吹入含有胶态氢氧化亚铁或含铁胶体沉淀物的亚铁盐反应溶液中,该溶液通过使亚铁盐水溶液与小于 一种碱金属氢氧化物水溶液,碱金属碳酸盐水溶液或碱金属氢氧化物和碱金属碳酸盐水溶液中,在所述含水亚铁盐水溶液中,在抗坏血酸或其盐的存在下,氧化所述胶体 含氢氧化铁或含铁胶体沉淀物,并通过绿锈生成针状针铁矿颗粒; 以及通过将上述方法中得到的针状针铁矿粒子还原而制造针状磁性氧化铁粒子的方法,制造针状磁铁矿粒子,根据需要,根据需要氧化针状磁铁矿粒子,得到针状磁赤铁矿粒子,根据需要,对针状磁铁矿 或具有Co或Co和Fe2 +的磁赤铁矿颗粒。

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