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    METHOD OF PREPARING AN ADSORBENT MATERIAL SHAPED IN THE ABSENCE OF BINDER AND METHOD OF EXTRACTING LITHIUM FROM SALINE SOLUTIONS USING SAID MATERIAL
    1.
    发明申请
    METHOD OF PREPARING AN ADSORBENT MATERIAL SHAPED IN THE ABSENCE OF BINDER AND METHOD OF EXTRACTING LITHIUM FROM SALINE SOLUTIONS USING SAID MATERIAL 审中-公开
    制备在粘合剂中形成的吸附材料的方法和使用上述材料从盐溶液中提取锂的方法

    公开(公告)号：US20160317998A1

    公开(公告)日：2016-11-03

    申请号：US15107453

    申请日：2014-12-23

    申请人： ERAMET ,  IFP ENERGIES NOUVELLES

    发明人： Malika BOUALLEG ,  Olivier LAFON ,  Fabien André Pierre BURDET ,  Romain Charles Joseph René SOULAIROL

    IPC分类号： B01J20/08 ,  C02F1/28 ,  C01D15/04 ,  B01D15/36 ,  B01J20/04 ,  B01J20/30

    CPC分类号： B01J20/08 ,  B01D15/36 ,  B01J20/046 ,  B01J20/3007 ,  B01J20/3078 ,  B01J20/3085 ,  B01J2220/58 ,  C01D15/04 ,  C01F7/043 ,  C01P2002/72 ,  C01P2006/12 ,  C02F1/281

    摘要： A method for preparing a crystallized solid material of formula LiCl.2Al(OH)3,nH2O with n being comprised between 0.01 and 10, includes mixing in an aqueous medium, at least one source of alumina and at least one source of lithium in order to obtain a suspension, filtering the resulting suspension obtained for obtaining a slurry, followed by drying the obtained slurry at a temperature between 20 and 80° C. for a period between 1 h and 12 h, then shaping by extrusion the resulting dried slurry, directly after the drying to obtain extrudates, where the shaping was carried out without any binder, and then the drying of the obtained extrudates at a temperature comprised between 20 and 200° C. for a period between 1 hour and 20 hours, in order to obtain the crystallized solid material of formula LiCl.2Al(OH)3,nH2O as extrudates. A method for extracting lithium from saline solutions uses the thereby prepared material.

    摘要翻译： 制备结晶固体物质的方法，其中n包含在0.01至10之间的式LiCl 2 Al（OH）3，nH 2 O，其包括在水性介质中，至少一种氧化铝源和至少一种锂源，按顺序混合 得到悬浮液，过滤获得的悬浮液得到的悬浮液，然后在20〜80℃的温度下干燥所获得的浆料1小时至12小时之间的时间，然后挤出所得干浆料， 在干燥后直接获得挤出物，其中在没有任何粘合剂的情况下进行成型，然后将所得挤出物在20-200℃的温度下干燥1小时至20小时，以便 得到结晶的式LiCl 2 Al（OH）3，nH 2 O的固体物质作为挤出物。 从盐溶液中提取锂的方法使用由此制备的材料。

    Process for the preparation of lithium aluminosilicate or gamma lithium aluminate ceramics having a controlled stoichiometry and microstructure
    2.
    发明授权
    Process for the preparation of lithium aluminosilicate or gamma lithium aluminate ceramics having a controlled stoichiometry and microstructure 失效
    用于制备具有受控化学计量和微结构的铝硅酸锂或γ-铝酸锂陶瓷的方法

    公开(公告)号：US5545427A

    公开(公告)日：1996-08-13

    申请号：US398813

    申请日：1995-03-06

    申请人： Jean-Pierre Boilot ,  Marcel Boncoeur ,  Bernard Rasneur ,  Olivier Renoult

    发明人： Jean-Pierre Boilot ,  Marcel Boncoeur ,  Bernard Rasneur ,  Olivier Renoult

    IPC分类号： C04B38/00 ,  C01F7/04 ,  C04B35/44 ,  G21B1/11 ,  G21B1/17 ,  G21C3/06

    CPC分类号： C04B35/44 ,  C01F7/043

    摘要： This invention relates to a process for the preparation of lithium aluminosilicate or gamma lithium aluminate ceramics having a controlled microstructure and stoichiometry.According to this process, mixing takes place accompanied by stirring in a short chain anhydrous alcohol of an unpolymerized liquid aluminium alkoxide and optionally a silicon alkoxide with a hydrated or unhydrated lithium hydroxide, followed by the addition of water in order to hydrolyze the mixture and obtain, after drying, beta LiAlO.sub.2 powder.This powder can be directly compacted and then sintered at temperatures of 800.degree. to 1150.degree. C. without prior calcination giving a gamma lithium aluminate ceramic with a controlled stoichiometry and microstructure (grains of 0.1 to 10 .mu.m).

    摘要翻译： 本发明涉及一种制备具有受控微结构和化学计量的铝硅酸锂或γ-铝酸锂陶瓷的方法。 根据该方法，在未聚合的液体铝醇盐的短链无水醇和任选的含有水合或未水合氢氧化锂的硅烷醇盐的搅拌下进行混合，然后加入水以水解混合物并获得 ，干燥后，加入β-LiAlO2粉末。 该粉末可以直接压实，然后在800℃至1150℃的温度下烧结，而无需预先煅烧，得到具有受控化学计量和微观结构（0.1至10μm的晶粒）的γ铝酸铝陶瓷。

    Method of preparing a sintered lithium aluminate structure for containing electrolyte
    3.
    发明授权
    Method of preparing a sintered lithium aluminate structure for containing electrolyte 失效
    制备含有电解质的铝酸锂烧结体的方法

    公开(公告)号：US4251600A

    公开(公告)日：1981-02-17

    申请号：US107760

    申请日：1979-12-27

    申请人： James W. Sim ,  Kimio Kinoshita

    发明人： James W. Sim ,  Kimio Kinoshita

    IPC分类号： C01F7/04 ,  C04B35/113 ,  H01M2/16 ,  H01M8/02 ,  H01M8/14 ,  B28B1/26

    CPC分类号： H01M2/1646 ,  C01F7/043 ,  C04B35/113 ,  H01M8/0295 ,  H01M2300/0048

    摘要： A porous sintered tile is formed of lithium aluminate for retaining moltenlectrolyte within a fuel cell. The tile is prepared by reacting lithium hydroxide in aqueous solution with alumina particles to form beta lithium aluminate particles. The slurry is evaporated to dryness and the solids dehydrated to form a beta lithium aluminate powder. The powder is compacted into the desired shape and sintered at a temperature in excess of 1200 K. but less than 1900 K. to form a porous integral structure that is subsequently filled with molten electrolyte. A tile of this type is intended for use in containing molten alkali metal carbonates as electolyte for use in a fuel cell having porous metal or metal oxide electrodes for burning a fuel gas such as hydrogen and/or carbon monoxide with an oxidant gas containing oxygen.

    摘要翻译： 多孔烧结砖由铝酸锂形成，用于将熔融电解质保持在燃料电池内。 通过使氢氧化锂在水溶液中与氧化铝颗粒反应形成β铝酸锂颗粒来制备瓦。 将浆料蒸发至干，固体脱水形成β-铝酸锂粉末。 将粉末压实成所需的形状并在超过1200K但低于1900K的温度下烧结以形成随后用熔融电解质填充的多孔整体结构。 这种瓷砖用于将熔融碱金属碳酸盐作为电解液用于含有多孔金属或金属氧化物电极的燃料电池中，所述多孔金属或金属氧化物电极用含氧气的氧化剂气体燃烧诸如氢气和/或一氧化碳的燃料气体。

    Molten salt synthesis of lithium meta-aluminate powder
    4.
    发明授权
    Molten salt synthesis of lithium meta-aluminate powder 失效
    熔融盐合成偏铝酸锂粉末

    公开(公告)号：US4201760A

    公开(公告)日：1980-05-06

    申请号：US8734

    申请日：1979-02-02

    申请人： Ronald H. Arendt ,  Matthew J. Curran

    发明人： Ronald H. Arendt ,  Matthew J. Curran

    IPC分类号： C01F7/04 ,  H01M8/02

    CPC分类号： C01F7/043 ,  H01M8/0295 ,  Y10S423/12

    摘要： A particulate mixture of an alkali chloride solvent salt, a lithium salt reactant selected from the group consisting of lithium hydroxide, lithium nitrate, lithium carbonate and mixtures thereof, and an aluminum salt reactant selected from the group consisting of aluminum hydroxide, alpha-alumina, gamma-alumina and mixtures thereof is heated to melt the chloride salt solvent in which the lithium and aluminum salt reactants dissolve and react precipitating lithium meta-aluminate.

    摘要翻译： 碱金属氯化物溶剂盐，选自氢氧化锂，硝酸锂，碳酸锂及其混合物的锂盐反应物和选自氢氧化铝，α-氧化铝， 将γ-氧化铝及其混合物加热熔化其中锂盐和铝盐反应物溶解的氯化物盐溶剂并使析出的偏铝酸锂反应。

    Method of preparing electrolyte for use in fuel cells
    5.
    发明授权
    Method of preparing electrolyte for use in fuel cells 失效
    制备用于燃料电池的电解质的方法

    公开(公告)号：US4115632A

    公开(公告)日：1978-09-19

    申请号：US794295

    申请日：1977-05-05

    申请人： Kimio Kinoshita ,  John P. Ackerman

    发明人： Kimio Kinoshita ,  John P. Ackerman

    IPC分类号： C01F7/04 ,  H01M8/02 ,  H01M8/14 ,  H01M8/00

    CPC分类号： H01M8/144 ,  C01F7/043 ,  H01M8/0295 ,  H01M8/142 ,  H01M8/145 ,  Y02E60/526

    摘要： An electrolyte compact for fuel cells includes a particulate support material of lithium aluminate that contains a mixture of alkali metal compounds, such as carbonates or hydroxides, as the active electrolyte material. The porous lithium aluminate support structure is formed by mixing alumina particles with a solution of lithium hydroxide and another alkali metal hydroxide, evaporating the solvent from the solution and heating to a temperature sufficient to react the lithium hydroxide with alumina to form lithium aluminate. Carbonates are formed by reacting the alkali metal hydroxides with carbon dioxide gas in an exothermic reaction which may proceed simultaneously with the formation with the lithium aluminate. The mixture of lithium aluminate and alkali metal in an electrolyte active material is pressed or otherwise processed to form the electrolyte structure for assembly into a fuel cell.

    摘要翻译： 用于燃料电池的电解质压块包括含有碱金属化合物如碳酸盐或氢氧化物的混合物作为活性电解质材料的铝酸锂颗粒载体材料。 通过将氧化铝颗粒与氢氧化锂和另一种碱金属氢氧化物的溶液混合，将溶剂从溶液中蒸发并加热到足以使氢氧化锂与氧化铝反应形成铝酸锂的温度来形成多孔铝酸锂载体结构。 碳酸盐通过使碱金属氢氧化物与二氧化碳气体在放热反应中反应而形成，放热反应可与铝酸锂形成同时进行。 将电解质活性材料中的铝酸锂和碱金属的混合物压制或以其它方式加工以形成用于组装成燃料电池的电解质结构。

    Production of beta-lithium aluminate (LiAlO.sub.2)
    6.
    发明授权
    Production of beta-lithium aluminate (LiAlO.sub.2) 失效
    生产β-铝酸锂（LiAlO {HD 2 {B）

    公开(公告)号：US3998939A

    公开(公告)日：1976-12-21

    申请号：US606060

    申请日：1975-08-20

    申请人： David M. Mason ,  Cornelius J. VanDrunen

    发明人： David M. Mason ,  Cornelius J. VanDrunen

    IPC分类号： C01F7/04 ,  H01M8/02

    CPC分类号： C01F7/043 ,  H01M8/0295 ,  Y02P70/56

    摘要： A low pressure process for the production of beta-lithium aluminate (LiAlO.sub.2) in a two thermal stage reaction of alumina with liquid phase lithium carbonate comprising admixing powdered alumina with a carbonates composition selected from the group consisting of a ternary lithium-potassium-sodium carbonates composition, a binary lithium-potassium carbonates composition and a binary lithium-sodium carbonates composition, heating the admixture at about 480.degree. to 550.degree. C. in a first thermal stage for a period of time to react the alumina with lithium carbonate to form lithium aluminate, and raising the temperature of the lithium aluminate to about 600.degree. to 650.degree. C. in a second thermal stage for a period of time to transform the lithium aluminate (LiAlO.sub.2) to the desired beta-lithium aluminate.

    摘要翻译： 在氧化铝与液相碳酸锂的两个热阶段反应中生产β-锂铝酸锂（LiAlO 2）的低压方法，包括将粉末状氧化铝与选自三元碳酸锂 - 碳酸钠的碳酸盐组合物混合 组合物，二元碳酸氢钾组合物和二元碳酸锂 - 碳酸钠组合物，在约480℃至550℃下在第一热级中加热混合物一段时间以使氧化铝与碳酸锂反应形成锂 铝酸盐，并在第二个热阶段将铝酸锂的温度升高至约600至650℃，持续一段时间以将铝酸锂（LiAlO 2）转化为所需的β-铝酸锂。

    METHOD FOR PRODUCING alpha-LITHIUM ALUMINATE
    7.
    发明申请
    METHOD FOR PRODUCING alpha-LITHIUM ALUMINATE 有权
    生产铝酸铝的方法

    公开(公告)号：US20160347623A1

    公开(公告)日：2016-12-01

    申请号：US15114594

    申请日：2014-02-05

    申请人： NIPPON CHEMICAL INDUSTRIAL CO., LTD.

    发明人： Junya Fukazawa

    IPC分类号： C01F7/04 ,  H01M8/14 ,  H01M8/0295

    CPC分类号： C01F7/043 ,  C01P2002/72 ,  C01P2004/03 ,  C01P2006/12 ,  C01P2006/37 ,  C01P2006/40 ,  H01M8/0295 ,  H01M8/142 ,  H01M2008/147 ,  Y02E60/526

    摘要： The purpose of the present invention is to provide an industrially advantageous method for producing α-lithium aluminate which has physical properties that are suitable for use as an electrolyte holding plate of a MCFC having excellent thermal stability, even if the α-lithium aluminate is a fine material having a BET specific surface area of 10 m2/g or higher in particular. Provided is a method for producing α-lithium aluminate characterized by subjecting a mixture (a), which is obtained by mixing transitional alumina and lithium carbonate at an Al/Li molar ratio of 0.95-1.01, to a first firing reaction so as to obtain a fired product, and subjecting a mixture (b), which is obtained by adding an aluminum compound to the obtained fired product at quantities whereby the molar ratio of aluminum atoms in the aluminum compound relative to lithium atoms in the fired product (Al/Li) is 0.001-0.05, to a second firing reaction.

    摘要翻译： 本发明的目的是提供一种工业上有利的生产α-铝酸锂的方法，其具有适合用作具有优异的热稳定性的MCFC的电解质保持板的物理性能，即使α-铝酸锂是 特别是BET比表面积为10m 2 / g以上的精细材料。 提供一种制造α-铝酸锂的方法，其特征在于将以Al / Li摩尔比为0.95-1.01的过渡氧化铝和碳酸锂混合得到的混合物（a）进行第一次烧成反应，得到 烧成品，对得到的烧成品中加入铝化合物而得到的混合物（b）的量相对于烧成品中的铝化合物中的铝原子摩尔比相对于锂原子的摩尔比（Al / Li ）为0.001-0.05，进行第二次烧制反应。