公开(公告)号：US20190211186A1

公开(公告)日：2019-07-11

申请号：US16356942

申请日：2019-03-18

申请人： 3M INNOVATIVE PROPERTIES COMPANY

发明人： Mark F. Schulz ,  Michael S. Wendland

IPC分类号： C08K5/47 ,  C09B29/08 ,  G01N21/78 ,  C09B29/033 ,  C08K9/04 ,  C08K7/20 ,  C09C3/08 ,  C09C1/00 ,  C09C1/28 ,  C09C1/02 ,  C09B69/00

CPC分类号： C08K5/47 ,  C08K7/20 ,  C08K9/04 ,  C09B29/0088 ,  C09B29/0801 ,  C09B29/0813 ,  C09B29/0827 ,  C09B29/0829 ,  C09B69/008 ,  C09C1/00 ,  C09C1/021 ,  C09C1/28 ,  C09C3/08 ,  G01N21/78

摘要： A compound represented by formula: and a treated filler having the compound on at least a portion of its surface. R is hydrogen or alkyl. X is alkylene, arylalkylene, or alkylarylene, each optionally interrupted by at least one of an ether, thioether, amine, amide, ester, thioester, carbonate, thiocarbonate, carbamate, thiocarbamate, urea, or thiourea, with alkylene optionally interrupted by arylene. W is hydroxyl, a sulfonic acid group, a phosphonic acid group, carboxylic acid group, —NHR1, epoxy, or —Si(Y)x(Z)3-x. Y is alkyl, aryl, arylalkylenyl, or alkylarylenyl. Z is halide, hydroxyl, alkoxy, aryloxy, acyloxy, polyalkyleneoxy, —O— covalently bonded to the surface of the filler, or —O bonded to another silicon atom, and x is 0 or 1. A composition including the treated filler, a method of making the treated filler, and a method of determining the degree of cure of a curable polymeric resin are also disclosed.

公开(公告)号：US09068290B2

公开(公告)日：2015-06-30

申请号：US14517926

申请日：2014-10-20

申请人： FUJIFILM CORPORATION

发明人： Kazunari Yagi ,  Yasuhiro Ishiwata ,  Yutaro Norizuki

IPC分类号： D06P3/24 ,  B41J2/01 ,  B41M5/00 ,  C09D11/00 ,  C09D11/328 ,  D06P1/08 ,  D06P5/30 ,  D06P3/26 ,  C09B29/036 ,  C09B29/08 ,  C09B43/11 ,  D06P1/18

CPC分类号： D06P3/24 ,  B41J2/01 ,  B41M5/00 ,  C09B29/0051 ,  C09B29/0801 ,  C09B29/0809 ,  C09B43/11 ,  C09D11/00 ,  C09D11/328 ,  D06P1/08 ,  D06P1/18 ,  D06P3/26 ,  D06P5/30 ,  Y10T428/2481

摘要： A coloring composition for inkjet textile printing, containing water and a dye represented by Formula (I) [R1 represents H, halogen, alkyl, aralkyl, aryl, heteroaryl, alkoxy, or cyano; R2 represents H, halogen, cyano, —COOR6, —COR7, —CONR8R9, or an ionic hydrophilic group; R3 represents alkyl, aralkyl, alkenyl, alkynyl, aryl, or heteroaryl; each of R4 and R5 independently represents H, alkyl, cycloalkyl, aralkyl, alkenyl, alkynyl, aryl, or heteroaryl; R15 represents H or a substituent; X represents alkyl, cycloalkyl, aralkyl, aryl, heteroaryl, —COR12, or —CONR13R14; R6 represents alkyl, aryl, or heteroaryl; each of R7 to R14 independently represents H, alkyl, aryl, or heteroaryl; and a number of ionic hydrophilic groups in one molecule is from 1 to 5].

摘要翻译： 用于喷墨织物印花的着色组合物，含有水和由式（I）表示的染料[R1表示H，卤素，烷基，芳烷基，芳基，杂芳基，烷氧基或氰基; R 2表示H，卤素，氰基，-COOR 6，-COR 7，-CONR 8 R 9或离子性亲水基团; R 3表示烷基，芳烷基，烯基，炔基，芳基或杂芳基; R 4和R 5各自独立地表示H，烷基，环烷基，芳烷基，烯基，炔基，芳基或杂芳基; R 15表示H或取代基; X表示烷基，环烷基，芳烷基，芳基，杂芳基，-COR 12或-CONR 13 R 14; R6表示烷基，芳基或杂芳基; R 7至R 14各自独立地表示H，烷基，芳基或杂芳基; 并且一个分子中的多个离子亲水基团为1〜5]。

公开(公告)号：US06489452B1

公开(公告)日：2002-12-03

申请号：US09813036

申请日：2001-03-21

申请人： Keiichi Tateishi ,  Toshiki Fujiwara ,  Makoto Yamada

发明人： Keiichi Tateishi ,  Toshiki Fujiwara ,  Makoto Yamada

IPC分类号： C09B29036

CPC分类号： C09D11/328 ,  C09B29/0051 ,  C09B29/0801 ,  C09B29/0809 ,  C09B43/11 ,  C09B43/16

摘要： An azo dye represented by the following general formula (1) and a process for making the azo dye is disclosed. The process comprises a step in which a diazonium salt is formed by the reaction between an aminopyrazole represented by the general formula (3) and an diazotizing agent, a step in which a compound represented by the general formula (5) is formed by the reaction between the diazonium salt and an aromatic coupling agent represented by the general formula (4), and a step in which an azo dye represented by the general formula (6) is formed by the reaction between the compound represented by the general formula (5) and an arylating agent or a heterylating agent in the presence of a base.

摘要翻译： 公开了由以下通式（1）表示的偶氮染料和制备偶氮染料的方法。 该方法包括通过由通式（3）表示的氨基吡唑与重氮化剂之间的反应形成重氮盐的步骤，其中通过反应形成由通式（5）表示的化合物的步骤 在由通式（4）表示的重氮盐和芳族偶联剂之间，通过通式（5）表示的化合物之间的反应形成由通式（6）表示的偶氮染料， 和芳基化剂或异构化剂在碱的存在下反应。

公开(公告)号：US20150037546A1

公开(公告)日：2015-02-05

申请号：US14517926

申请日：2014-10-20

申请人： FUJIFILM CORPORATION

发明人： Kazunari YAGI ,  Yasuhiro ISHIWATA ,  Yutaro NORIZUKI

IPC分类号： D06P3/24 ,  D06P5/30 ,  D06P1/08

CPC分类号： D06P3/24 ,  B41J2/01 ,  B41M5/00 ,  C09B29/0051 ,  C09B29/0801 ,  C09B29/0809 ,  C09B43/11 ,  C09D11/00 ,  C09D11/328 ,  D06P1/08 ,  D06P1/18 ,  D06P3/26 ,  D06P5/30 ,  Y10T428/2481

摘要： A coloring composition for inkjet textile printing, containing water and a dye represented by Formula (I) [R1 represents H, halogen, alkyl, aralkyl, aryl, heteroaryl, alkoxy, or cyano; R2 represents H, halogen, cyano, —COOR6, —COR7, —CONR8R9, or an ionic hydrophilic group; R3 represents alkyl, aralkyl, alkenyl, alkynyl, aryl, or heteroaryl; each of R4 and R5 independently represents H, alkyl, cycloalkyl, aralkyl, alkenyl, alkynyl, aryl, or heteroaryl; R15 represents H or a substituent; X represents alkyl, cycloalkyl, aralkyl, aryl, heteroaryl, —COR12, or —CONR13R14; R6 represents alkyl, aryl, or heteroaryl; each of R7 to R14 independently represents H, alkyl, aryl, or heteroaryl; and a number of ionic hydrophilic groups in one molecule is from 1 to 5].

摘要翻译： 用于喷墨织物印花的着色组合物，含有水和由式（I）表示的染料[R1表示H，卤素，烷基，芳烷基，芳基，杂芳基，烷氧基或氰基; R 2表示H，卤素，氰基，-COOR 6，-COR 7，-CONR 8 R 9或离子性亲水基团; R 3表示烷基，芳烷基，烯基，炔基，芳基或杂芳基; R 4和R 5各自独立地表示H，烷基，环烷基，芳烷基，烯基，炔基，芳基或杂芳基; R 15表示H或取代基; X表示烷基，环烷基，芳烷基，芳基，杂芳基，-COR 12或-CONR 13 R 14; R6表示烷基，芳基或杂芳基; R 7至R 14各自独立地表示H，烷基，芳基或杂芳基; 并且一个分子中的多个离子亲水基团为1〜5]。

公开(公告)号：US4243584A

公开(公告)日：1981-01-06

申请号：US919482

申请日：1978-06-27

申请人： Richard Sommer ,  Gerhard Wolfrum ,  Gerhard Buttner

发明人： Richard Sommer ,  Gerhard Wolfrum ,  Gerhard Buttner

IPC分类号： C09B29/01 ,  C09B29/08 ,  C09B29/36 ,  C09B29/38 ,  D06P3/26

CPC分类号： C09B29/0801 ,  C09B29/08 ,  C09B29/36

摘要： Monoazo dyestuffs of the formula ##STR1## wherein R.sub.1 represents an aromatic radical, an aliphatic radical with 1-4 C atoms or a dialkylamino radical, in which the alkyl groups contain 1-C atoms, R.sub.2 represents hydrogen, halogen, alkyl with 1-C atoms, alkoxy with 1-4 C atoms or trifluoromethyl, R.sub.3 represents hydrogen, halogen, alkyl with 1-4 C atoms, alkoxy with 1-4 C atoms or trifluoromethyl and K represents the radical of a coupling component K-H of the formulae (II), (III) and (IV) ##STR2## wherein R.sub.4 represents alkyl with 1-4 C atoms or aryl,R.sub.5 represents hydrogen or unsubstituted alkyl with 1-4 C atoms,R.sub.6 represents hydrogen, nitrile, halogen, alkyl with 1-4 C atoms or alkoxy with 1-4 C atoms,R.sub.7 represents hydrogen, alkyl with 1-4 C atoms, aryl, a carboxylic acid ester group or a carboxylic acid amide group,R.sub.8 represents hydrogen, alkyl, cycloalkyl, aryl or the radical of a heterocyclic compound,R.sub.9 represents hydrogen, halogen, alkyl with 1-4 C atoms, alkoxy with 1-4 C atoms or acylamino,R.sub.10 represents hydrogen, halogen, alkyl with 1-4 C atoms, alkoxy with 1-4 C atoms or aryloxy,R.sub.11 represents hydrogen or alkyl,R.sub.12 represents hydrogen or alkyl and m represents 0 or 1,are suitable for the dyeing of synthetic fibre materials, especially those from polyamides. Level yellow, red and ruby shades are obtained with good dyeing yield and fastness.

摘要翻译： 其中R 1表示芳族基团，具有1-4个碳原子的脂族基团或二烷基氨基，其中烷基含有1-C原子，R 2表示氢，卤素，具有1- C原子，具有1-4个C原子的烷氧基或三氟甲基，R 3表示氢，卤素，具有1-4个C原子的烷基，具有1-4个C原子的烷氧基或三氟甲基，K表示式（I）的偶合组分KH的基团 II），（III）和（IV）其中R 4表示具有1-4个C原子的烷基或芳基，R 5表示氢或具有1-4个C原子的未取代的烷基，R 6表示氢，腈，卤素，具有1个 -4个C原子或具有1-4个C原子的烷氧基，R7代表氢，具有1-4个C原子的烷基，芳基，羧酸酯基或羧酸酰胺基，R8代表氢，烷基，环烷基，芳基或 杂环化合物的基团，R 9表示氢，卤素，具有1-4个C原子的烷基，具有1-4个C原子的烷氧基或a 氨基，R 10表示氢，卤素，具有1-4个C原子的烷基，具有1-4个C原子的烷氧基或芳氧基，R 11表示氢或烷基，R 12表示氢或烷基，m表示0或1，适于染色 合成纤维材料，特别是聚酰胺。 获得具有良好的染色产率和坚牢度的黄色，红色和红宝石色调。

公开(公告)号：US20030040608A1

公开(公告)日：2003-02-27

申请号：US10176764

申请日：2002-06-24

发明人： Keiichi Tateishi ,  Toshiki Fujiwara ,  Makoto Yamada

IPC分类号： C09B031/047

CPC分类号： C09D11/328 ,  C09B29/0051 ,  C09B29/0801 ,  C09B29/0809 ,  C09B43/11 ,  C09B43/16

摘要： An azo dye represented by the following general formulae (10) and (12): 1 (wherein the variables are as defined herein) and a process for making the azo dye is disclosed. The process comprises a step in which a diazonium salt is formed by the reaction between an aminopyrazole represented by the general formula (3) and an diazotizing agent, a step in which a compound represented by the general formula (5) is formed by the reaction between the diazonium salt and an aromatic coupling agent represented by the general formula (4), and a step in which an azo dye represented by the general formula (6) is formed by the reaction between the compound represented by the general formula (5) and an arylating agent or a heterylating agent in the presence of a base.

摘要翻译： 由以下通式（10）和（12）表示的偶氮染料（其中变量如本文所定义）和制备偶氮染料的方法。 该方法包括通过由通式（3）表示的氨基吡唑与重氮化剂之间的反应形成重氮盐的步骤，其中通过反应形成由通式（5）表示的化合物的步骤 在由通式（4）表示的重氮盐和芳族偶联剂之间，通过通式（5）表示的化合物之间的反应形成由通式（6）表示的偶氮染料， 和芳基化剂或异构化剂在碱的存在下反应。

公开(公告)号：US4234483A

公开(公告)日：1980-11-18

申请号：US713619

申请日：1976-08-11

申请人： Raouf Botros ,  Ivan E. Riggle

发明人： Raouf Botros ,  Ivan E. Riggle

IPC分类号： C09B29/08 ,  D06P3/04 ,  D06P3/24 ,  D06P3/52

CPC分类号： C09B29/0847 ,  C09B29/0801

摘要： Azo compounds of the formula: ##STR1## are provided where A is a diazotizable aromatic hydrocarbon and X is hydrogen or lower alkyl. The compounds dye synthetic fibers, particularly nylon and polyester, and wool in strong yellow to red hues of outstanding brightness and build-up. The dyeings have excellent fastness properties.

摘要翻译： 提供下式的偶氮化合物：其中A是可重氮化的芳族烃，X是氢或低级烷基。 化合物染色合成纤维，特别是尼龙和聚酯，以及具有强烈的黄色至红色色调的羊毛，具有出色的亮度和积聚性。 染色具有优异的牢度特性。

公开(公告)号：US4159265A

公开(公告)日：1979-06-26

申请号：US899830

申请日：1978-04-25

申请人： Richard Sommer ,  Gerhard Wolfrum ,  Gerhard Buttner

发明人： Richard Sommer ,  Gerhard Wolfrum ,  Gerhard Buttner

IPC分类号： C09B29/08 ,  C09B29/36

CPC分类号： C09B29/0801 ,  C09B29/36

摘要： Monoazo dyestuffs of the formula ##STR1## wherein K represents the radical of a couping component K-H of the formula ##STR2## said dyestuff being suitable for the dyeing of synthetic fibre materials especially those from polyamides.

摘要翻译： 其中K表示式（IMAGE）所示的配合组分K-H的基团，所述染料适用于合成纤维材料的染色，特别是聚酰胺染色。

公开(公告)号：US20160319105A1

公开(公告)日：2016-11-03

申请号：US15109350

申请日：2014-12-19

申请人： 3M INNOVATIVE PROPERTIES COMPANY

发明人： Mark F. Schulz ,  Michael S. Wendland

IPC分类号： C08K5/47 ,  G01N21/78 ,  C08K7/20 ,  C08K9/04 ,  C09B29/08 ,  C09B29/033

CPC分类号： C08K5/47 ,  C08K7/20 ,  C08K9/04 ,  C09B29/0088 ,  C09B29/0801 ,  C09B29/0813 ,  C09B29/0827 ,  C09B29/0829 ,  C09B69/008 ,  C09C1/00 ,  C09C1/021 ,  C09C1/28 ,  C09C3/08 ,  G01N21/78

摘要： A compound represented by formula (I): and a treated filler having the compound on at least a portion of its surface. R is hydrogen or alkyl. X is alkylene, arylalkylene, or alkylarylene, each optionally interrupted by at least one of an ether, thioether, amine, amide, ester, thioester, carbonate, thiocarbonate, carbamate, thiocarbamate, urea, or thiourea, with alkylene optionally interrupted by arylene. W is hydroxyl, a sulfonic acid group, a phosphonic acid group, carboxylic acid group, —NHR1, epoxy, or —Si(Y)x(Z)3-x. Y is alkyl, aryl, arylalkylenyl, or alkylarylenyl. Z is halide, hydroxyl, alkoxy aryloxy, acyloxy, polyalkyleneoxy, —O— covalently bonded to the surface of the filler, or —O bonded to another silicon atom, and x is 0 or 1. A composition including the treated filler, a method of making the treated filler, and a method of determining the degree of cure of a curable polymeric resin are also disclosed.

公开(公告)号：US06613888B2

公开(公告)日：2003-09-02

申请号：US10176764

申请日：2002-06-24

申请人： Keiichi Tateishi ,  Toshiki Fujiwara ,  Makoto Yamada

发明人： Keiichi Tateishi ,  Toshiki Fujiwara ,  Makoto Yamada

IPC分类号： C09B29036

CPC分类号： C09D11/328 ,  C09B29/0051 ,  C09B29/0801 ,  C09B29/0809 ,  C09B43/11 ,  C09B43/16

摘要： An azo dye represented by the following general formulae (10) and (12): (wherein the variables are as defined herein) and a process for making the azo dye is disclosed. The process comprises a step in which a diazonium salt is formed by the reaction between an aminopyrazole represented by the general formula (3) and an diazotizing agent, a step in which a compound represented by the general formula (5) is formed by the reaction between the diazonium salt and an aromatic coupling agent represented by the general formula (4), and a step in which an azo dye represented by the general formula (6) is formed by the reaction between the compound represented by the general formula (5) and an arylating agent or a heterylating agent in the presence of a base.

摘要翻译： 由以下通式（10）和（12）表示的偶氮染料（其中变量如本文所定义）和制备偶氮染料的方法。 该方法包括通过由通式（3）表示的氨基吡唑与重氮化剂之间的反应形成重氮盐的步骤，其中通过反应形成由通式（5）表示的化合物的步骤 在由通式（4）表示的重氮盐和芳族偶联剂之间，通过通式（5）表示的化合物之间的反应形成由通式（6）表示的偶氮染料， 和芳基化剂或异构化剂在碱的存在下反应。