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    Separation reagent of platinum group metal, method for separating and recovering platinum group metal, and amide-containing tertiary amine compound
    2.
    发明授权
    Separation reagent of platinum group metal, method for separating and recovering platinum group metal, and amide-containing tertiary amine compound 有权
    铂族金属的分离试剂，铂族金属的分离回收方法和含酰胺的叔胺化合物

    公开(公告)号：US08609898B2

    公开(公告)日：2013-12-17

    申请号：US13013490

    申请日：2011-01-25

    申请人： Hirokazu Narita ,  Mikiya Tanaka ,  Kazuko Morisaku

    发明人： Hirokazu Narita ,  Mikiya Tanaka ,  Kazuko Morisaku

    IPC分类号： C07C233/05 ,  C22B61/00

    CPC分类号： C22B11/04 ,  C22B3/001 ,  C22B3/0032 ,  C22B3/10 ,  C22B11/06 ,  Y02P10/234

    摘要： The present invention provides a novel separation reagent capable of obtaining a high extraction % of rhodium in a chlorine-based acid solution, which has never existed heretofore, and a method for separating and recovering a platinum group metal using the same. An organic phase composed of an amide-containing tertiary amine separation reagent represented by the structural formula shown below is brought into contact with an acid solution containing a platinum group metal, thereby extracting rhodium, platinum and palladium with the organic phase. Among the metals extracted with the organic phase, rhodium is selectively back-extracted with a highly-concentrated hydrochloric acid solution, while palladium and platinum are back-extracted with a highly-concentrated nitric acid solution: wherein at least one of R1, R2 and R3 represents an amide group represented by: R1 to R3 other than the amide group and R4 to R6 represent a group selected from an optionally branched chain hydrocarbon group of 1 to 18 carbon atoms, an alicyclic hydrocarbon group of 1 to 10 carbon atoms, and an aromatic hydrocarbon group of 1 to 14 carbon atoms.

    摘要翻译： 本发明提供了一种能够在迄今为止从未存在的氯系酸溶液中获得高提取率的铑的新型分离试剂，以及使用该分离试剂的铂族金属的分离和回收方法。 将由下述结构式表示的含酰胺的叔胺分离试剂构成的有机相与含有铂族金属的酸溶液接触，由有机相萃取铑，铂和钯。 在有机相提取的金属中，用高度浓缩的盐酸溶液选择性地反萃取铑，钯和铂用高浓度硝酸溶液反萃取：其中R1，R2和 R3表示由除酰胺基以外的R1〜R3表示的酰胺基，R4〜R6表示选自1〜18个任意支链的烃基，1〜10个碳原子的脂环族烃基， 1〜14个碳原子的芳香族烃基。

    SEPARATION REAGENT OF PLATINUM GROUP METAL, METHOD FOR SEPARATING AND RECOVERING PLATINUM GROUP METAL, AND AMIDE-CONTAINING TERTIARY AMINE COMPOUND
    3.
    发明申请
    SEPARATION REAGENT OF PLATINUM GROUP METAL, METHOD FOR SEPARATING AND RECOVERING PLATINUM GROUP METAL, AND AMIDE-CONTAINING TERTIARY AMINE COMPOUND 有权
    铂族金属的分离试剂，分离和回收铂族金属的方法，以及含胺的仲胺化合物

    公开(公告)号：US20110113927A1

    公开(公告)日：2011-05-19

    申请号：US13013490

    申请日：2011-01-25

    申请人： Hirokazu NARITA ,  Mikiya TANAKA ,  Kazuko MORISAKU

    发明人： Hirokazu NARITA ,  Mikiya TANAKA ,  Kazuko MORISAKU

    IPC分类号： C22B61/00

    CPC分类号： C22B11/04 ,  C22B3/001 ,  C22B3/0032 ,  C22B3/10 ,  C22B11/06 ,  Y02P10/234

    摘要： The present invention provides a novel separation reagent capable of obtaining a high extraction % of rhodium in a chlorine-based acid solution, which has never existed heretofore, and a method for separating and recovering a platinum group metal using the same. An organic phase composed of an amide-containing tertiary amine separation reagent represented by the structural formula shown below is brought into contact with an acid solution containing a platinum group metal, thereby extracting rhodium, platinum and palladium with the organic phase. Among the metals extracted with the organic phase, rhodium is selectively back-extracted with a highly-concentrated hydrochloric acid solution, while palladium and platinum are back-extracted with a highly-concentrated nitric acid solution: wherein at least one of R1, R2 and R3 represents an amide group represented by: R1 to R3 other than the amide group and R4 to R6 represent a group selected from an optionally branched chain hydrocarbon group of 1 to 18 carbon atoms, an alicyclic hydrocarbon group of 1 to 10 carbon atoms, and an aromatic hydrocarbon group of 1 to 14 carbon atoms.

    摘要翻译： 本发明提供了一种能够在迄今为止从未存在的氯系酸溶液中获得高提取率的铑的新型分离试剂，以及使用该分离试剂的铂族金属的分离和回收方法。 将由下述结构式表示的含酰胺的叔胺分离试剂构成的有机相与含有铂族金属的酸溶液接触，由有机相萃取铑，铂和钯。 在有机相提取的金属中，用高度浓缩的盐酸溶液选择性地反萃取铑，钯和铂用高浓度硝酸溶液反萃取：其中R1，R2和 R3表示由除酰胺基以外的R1〜R3表示的酰胺基，R4〜R6表示选自1〜18个任意支链的烃基，1〜10个碳原子的脂环族烃基， 1〜14个碳原子的芳香族烃基。

    Collecting agent comprising ammoniated compounds (primary, secondary, tertiary amines), for use in the process of grinding and/or floating copper, molybdenum, zinc, and other contained mineral ores
    5.
    发明申请
    Collecting agent comprising ammoniated compounds (primary, secondary, tertiary amines), for use in the process of grinding and/or floating copper, molybdenum, zinc, and other contained mineral ores 有权
    包含氨化化合物（一级，二级，叔胺类）的收集剂，用于研磨和/或漂浮铜，钼，锌和其他含矿物矿石的工艺

    公开(公告)号：US20060032800A1

    公开(公告)日：2006-02-16

    申请号：US10999754

    申请日：2004-11-29

    申请人： Hector Correa-Castillo ,  German Rodriguez-Buendia

    发明人： Hector Correa-Castillo ,  German Rodriguez-Buendia

    IPC分类号： E03F5/06

    CPC分类号： C22B1/00 ,  B03D1/0043 ,  B03D1/008 ,  B03D1/01 ,  B03D2201/02 ,  B03D2203/04 ,  C02F1/24 ,  C02F1/5236 ,  C02F1/56 ,  C02F2101/20 ,  C02F2103/16 ,  C22B3/001 ,  Y02P10/234

    摘要： The present invention provides a ammoniated collector (amine, azepine, etc.) alone or in combination with other thiol-type collecting reactants, as well as sodium, iron, magnesium, and/or manganese sulfates, sulfurs, oxides, and hydroxides, acrylic acid polymers and copolymers or other spreading agents, in the process of grinding and floating mineral ores, in order to allow to set new floating operational conditions in existing mineral ore processing plants; to obtain substantial improvements in metallurgic productivity by improving the kinetics of the floating process, which allows to increase recovery of molybdenum, decrease recovery of iron, increase copper grade in copper concentrate, at least keep or improve copper recovery, among others, through the addition of a collecting reactant implying savings of up to 100% of consumption of modifying agents, such as lime, currently used.

    摘要翻译： 本发明提供单独的或与其它硫醇型收集反应物以及钠，铁，镁和/或硫酸锰，硫酸，氧化物和氢氧化物，丙烯酸类的氨化收集剂（胺，氮杂等） 酸性聚合物和共聚物或其他铺展剂，在研磨和漂浮矿物矿石的过程中，以便在现有的矿石加工厂中设置新的浮选操作条件; 通过改善浮选工艺的动力学来获得冶金生产率的显着提高，这允许增加钼的回收率，降低铁的回收率，提高铜精矿中的铜品位，至少保持或提高铜的回收率等，通过加入 的收集反应物意味着节省高达100％的目前使用的改性剂如石灰的消耗。

    Separation of copper from cobalt
    8.
    发明授权
    Separation of copper from cobalt 失效
    铜与钴的分离

    公开(公告)号：US3887679A

    公开(公告)日：1975-06-03

    申请号：US25839672

    申请日：1972-05-31

    申请人： FALCONBRIDGE NICKEL MINES LTD

    发明人： WIGSTOL EIVIND ,  FROYLAND KJELL ELNAR

    IPC分类号： C22B23/00 ,  C01G3/00 ,  C22B3/00 ,  C22B3/20 ,  C22B3/28 ,  C22B15/00 ,  C01G51/00

    CPC分类号： C22B3/0012 ,  C01G3/00 ,  C01G3/003 ,  C22B3/001 ,  Y02P10/234

    摘要： A solvent extraction process for the improved separation of copper from cobalt in chloride solutions in which an organic solution containing an amine solvent, such as tri-iso-octylamine, is cycled around a closed organic circuit comprising in turn co-extraction of cobalt and copper from the chloride solution, preferential stripping of cobalt from the organic solution into water or dilute chloride solution thereby forming a cobalt eluate, stripping of copper from the organic, and return of the regenerated organic to the co-extraction step. The invention comprises dividing the organic into two streams, coextracting cobalt and copper from the chloride solution into one stream, preferentially extracting copper from the cobalt eluate into the other stream, and combining the two streams for preferential cobalt stripping therefrom, thereby forming a closed preferential cobalt stripping, preferential copper extracting circuit and producing a purified cobalt eluate.

    摘要翻译： 用于在氯化物溶液中改善铜与钴的分离的溶剂萃取方法，其中将含有胺溶剂的有机溶液（例如三异辛基胺）围绕封闭的有机回路循环，所述闭合有机回路包括依次共萃取钴 和来自氯化物溶液的铜，优先将钴从有机溶液中汽提到水或稀氯化物溶液中，由此形成钴洗脱液，从有机物中剥离铜，并将再生有机物返回共萃取步骤。 本发明包括将有机物分成两股，将氯化物溶液中的钴和铜共萃取成一股料流，优先将铜从钴洗脱液中提取到另一股料流中，并将两股料流合并，从而形成优质的钴 封闭的优选钴剥离，优选铜提取回路和生产纯化的钴洗脱液。