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    METHOD FOR PRODUCING ESTERS OF MULTIBASIC ACIDS
    92.
    发明申请
    METHOD FOR PRODUCING ESTERS OF MULTIBASIC ACIDS 审中-公开
    用于生产酯多元酸

    公开(公告)号：WO02038531A1

    公开(公告)日：2002-05-16

    申请号：PCT/EP2001/013131

    申请日：2001-11-13

    IPC: C07B61/00 ,  C07C67/08 ,  C07C67/54 ,  C07C69/44 ,  C07C69/80 ,  C08G63/78

    CPC classification number: C07C67/08 ,  C07C67/54 ,  C07C69/44 ,  C07C69/80

    Abstract: The invention relates to a method for producing esters of an acid component chosen from the multibasic C4-C10-carboxylic acids and an alcohol component chosen from C3-C12-alkanols or -alkanediols whose alkyl chain can be interrupted by 1 to 3 oxygen atoms. Sad method comprises the following steps: a) a mixture consisting essentially of the acid component or an anhydride thereof and the alcohol component is heated to boiling in a reaction zone in the presence of an esterification catalyst; b) the vapours containing alcohol and water are separated into a fragment that is rich in alcohol and a fragment that is rich in water by rectification; and c) the alcohol-rich fraction is fed back into the reaction zone, while the water-rich fraction is extracted from the process. The inventive method is simple to carry out and allows the rapid adjustment of an essentially quantitative conversion.

    Abstract translation: 公开了一种用于酯的化合物的制备由多元C4-C10羧酸选择的，所述酸成分和化合物从C3-C12链烷醇或链烷二醇的醇组分，其烷基链可以被中断中选择的工艺（1）至（3）氧原子，其中 a）以基本上由酸组分或其Anhyobid和由在酯化催化剂至沸腾的存在下，醇组分混合物的反应区中加热，b）精馏分离在富含醇的级分和富水馏分中的醇和含有水蒸汽，以及c） 所述富含醇的馏分再循环到反应区和拒绝他们，从工艺的富水馏分。 这个过程是简单地进行，并允许基本上定量转化的快速调整。

    PHTHALIC DIESTER DERIVATIVES AND ELECTRON DONORS
    94.
    发明申请
    PHTHALIC DIESTER DERIVATIVES AND ELECTRON DONORS 审中-公开
    PHELALIC DIESTER衍生物和电子助剂

    公开(公告)号：WO01081292A1

    公开(公告)日：2001-11-01

    申请号：PCT/JP2001/003460

    申请日：2001-04-23

    IPC: C07C69/80 ,  C08F4/649 ,  C08F4/654 ,  C08F10/00 ,  C08F110/06

    CPC classification number: C07C69/80 ,  C08F10/00 ,  C08F110/06 ,  C08F4/651 ,  C08F2500/12

    Abstract: Phthalic diester derivatives of the following general formula (I) and electron donors which contain the derivatives as the active ingredient and are to be used as solid catalysts for the polymerization of olefins can not only give highly stereoregular polymers with an extremely high activity or yield but also exhibit a high response to hydrogen: wherein R is C1-8 alkyl or halogeno; R and R may be the same or different from each other and are each C1-12 alkyl; and n represents the number of R (s) and is 1 or 2, with the proviso that when n is 2, R s may be the same or different from each other.

    Abstract translation: 以通式（I）表示的邻苯二甲酸二酯衍生物和含有该衍生物作为活性成分并用作烯烃聚合的固体催化剂的电子给体不仅能够产生具有非常高的活性或产率的高立体规则聚合物， 也表现出对氢的高响应：其中R 1是C 1-8烷基或卤代; R 2和R 3可以彼此相同或不同，并且各自为C 1-12烷基; 并且n表示R 1（s）的数目，并且为1或2，条件是当n为2时，R 1彼此可以相同或不同。

    METHOD FOR CARRYING OUT A BALANCED REACTION
    95.
    发明申请
    METHOD FOR CARRYING OUT A BALANCED REACTION 审中-公开
    方法用于进行平衡反应

    公开(公告)号：WO99047484A1

    公开(公告)日：1999-09-23

    申请号：PCT/EP1999/001451

    申请日：1999-03-06

    IPC: C07C41/50 ,  C07C67/08 ,  C07C43/303 ,  C07C43/305 ,  C07C69/36 ,  C07C69/60 ,  C07C69/675 ,  C07C69/70 ,  C07C69/704 ,  C07C69/708 ,  C07C69/716 ,  C07C69/72 ,  C07C69/80

    CPC classification number: C07C67/08 ,  C07B2200/07 ,  C07C41/56 ,  C07C2601/14 ,  C07C43/303 ,  C07C43/305

    Abstract: The invention relates to a method for carrying out a balanced reaction, comprising the following steps: a) a low-boiling educt (E2) which is gaseous in the reaction conditions is guided through a separate, liquid, higher-boiling educt (E1) in a bubble reactor and b) unreacted educt (E2) is conveyed to a membrane module together with the product to be separated (P1), which is also in gaseous form, as feed. Said membrane module is located outside of the reactor and is suitable for vapour permeation. In said membrane module, P1 is separated off as permeate whilst E2 is recovered as retentate and returned to the reactor in a circuit until the desired quantity of educt (E1) has been converted into the target product. The method is characterised in that carbonyl compounds of formula (I) R -(CO)n1-(B)m-(CO)n2-R are used as (E1), B representing an optionally hydroxy- and/or carboxy-substituted alk(en)yl radical with 1 to 12 carbon atoms which is also optionally interrupted by an ether oxygen, a phenyl radical or a carbonyl group, R and R representing hydrogen or a hydroxyl or alkyl radical with 1 to 12 carbon atoms independently of each other or forming a saturated or unsaturated aliphatic C5 or C6 ring together with at least one carbonyl group, said ring being optionally substituted with C1-C4 alkyl and/or hydroxy and the sum of n1 and n2 being either 1 or 2 and m being 0 or 1, and in that aliphatic alcohols with 2 to 8 carbon atoms are used as (E2).

    Abstract translation: 执行Gleichegwichtsreaktion，其中（a）的低沸点，通过液体分离vorliegendes较重沸点离析物（E2）开始在鼓泡式反应器（E2）材料的反应条件下是气态的vorliegendes导出，（b）中提出的未反应的起始材料的方法（ E2）（连同也气态本分离的产品P1）供给作为进料的介质适合位于反应器膜组件，其中，（P1）被分离为渗透物，而（E2的外部气相渗透）回收作为渗余物，并且只要在反应器中的循环 返回到起始原料（E1）已被转移到目标产物的期望部分，其特征在于，作为（E1）羰基的式（I）化合物：R t <1> - （CO）N 1（B ）间 - （CO）N 2-R <2>：其中B为任选羟基 - 和/或羧基以及任选被醚氧取代unterbro rupted烷（烯）ylenrest具有1至12个碳原子，一个苯基或一个羰基，R <1>和R <2>独立地是氢，具有1至12个碳原子，或具有至少一个羰基一起羟基或烷基 形成饱和或不饱和的，任选C1-C4烷基和/或羟基取代的脂族C5-或C6-环，n1和n2为1或2，m是0或1，和具有E2的脂族醇的总和 从2至8个碳原子的使用。

    PROCESS FOR PRODUCING ESTERS
    96.
    发明申请
    PROCESS FOR PRODUCING ESTERS 审中-公开
    生产过程的过程

    公开(公告)号：WO99041226A1

    公开(公告)日：1999-08-19

    申请号：PCT/JP1999/000591

    申请日：1999-02-12

    IPC: B01J31/12 ,  C07B61/00 ,  C07C67/08 ,  C07C69/80 ,  C07C69/82

    CPC classification number: C07C67/08 ,  C07C69/80

    Abstract: A process for producing esters from organic carboxylic acids and/or anhydrides thereof and C4-18 alcohols wherein the reaction time is shortened by elevating the reaction rate at the initial stage of the reaction and the energy cost is reduced thereby bringing about an economical advantage. The above process is characterized in that the reaction is effected under a pressure of 0.02 to 5 kg/cm and the feedstock alcohol is supplied within a temperature range from a temperature lower by 20 DEG C than the boiling p oint of the alcohol under the pressure in the reactor to the boiling point thereof.

    Abstract translation: 由有机羧酸和/或其酸酐生产酯的方法和通过提高反应初始阶段的反应速率并降低能量成本而缩短反应时间的C4-18醇，从而带来经济上的优势。 上述方法的特征在于反应在0.02-5kg / cm 2的压力下进行，原料醇在比醇的沸点低20℃的温度范围内供应 在反应器的压力下至其沸点。

    MONOESTERS AND MACROCYCLIC DIESTER OF PHTHALIC ACID AND SYNTHESIS THEREOF
    97.
    发明申请
    MONOESTERS AND MACROCYCLIC DIESTER OF PHTHALIC ACID AND SYNTHESIS THEREOF 审中-公开
    单酸酯和大分子油酸酯及其合成

    公开(公告)号：WO99014257A1

    公开(公告)日：1999-03-25

    申请号：PCT/US1998/017141

    申请日：1998-08-19

    IPC: C07C69/76 ,  C07C69/80 ,  C07D321/00 ,  C08G63/08 ,  C08G63/181 ,  C08G63/78 ,  C08G63/85

    CPC classification number: C07C69/76 ,  C07C69/80 ,  C07D321/00 ,  C08G63/181 ,  C08G63/78 ,  C08G63/85 ,  Y10S526/915

    Abstract: Monoesters and macrocyclic diesters of 2,2,4-trimethyl-1,3-pentanediol and phthalic acid or a derivative thereof are described. Methods by which such monoesters and diesters may be prepared are also described. The mono- and diesters according to the invention are useful in the preparation of clear, hard thermoplastic polymers. The thermoplastic polymers are useful in coatings, inks, reinforced plastics and packaging materials.

    Abstract translation: 描述了2,2,4-三甲基-1,3-戊二醇和邻苯二甲酸或其衍生物的单酯和大环二酯。 还描述了可以制备这种单酯和二酯的方法。 根据本发明的单酯和二酯可用于制备透明硬的热塑性聚合物。 热塑性聚合物可用于涂料，油墨，增强塑料和包装材料。

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