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    Process for production of living (co)polymer and use of the (co)polymer
    3.
    发明专利
    Process for production of living (co)polymer and use of the (co)polymer 审中-公开
    生产（CO）聚合物的方法和（CO）聚合物的使用方法

    公开(公告)号：JP2006183057A

    公开(公告)日：2006-07-13

    申请号：JP2006055130

    申请日：2006-03-01

    申请人： Mitsui Chemicals Inc ,  三井化学株式会社

    发明人： NOBORI TADAHITO ,  FUNAKI KATSUHIKO ,  SHIBAHARA ATSUSHI ,  SUZUKI MAKOTO ,  MIZUTANI KAZUMI ,  SHIROYAMA HIROMI ,  HARA RETSU ,  HAYASHI TAKAOMI ,  KIYONO SHINJI ,  FUJIYOSHI SETSUKO ,  SAKAYAMA HIROYUKI ,  MIZOGUCHI MITSUSACHI ,  MATSUMOTO TAKESHI ,  HIROSE YOSHIHARU

    IPC分类号： C09D201/02 ,  C09D5/03 ,  C09D7/12 ,  C09D163/00

    摘要： PROBLEM TO BE SOLVED: To provide a process for effectively and efficiently producing a living (co)polymer by the catalytic living polymerization of a polar unsaturated compound, when producing the (co)polymer by polymerizing the polar unsaturated compound; and to provide a thermosetting powder coating composition (e.g. an acrylic thermosetting powder coating composition) having storage stability, appearance characteristics, physical characteristics and chemical characteristics. SOLUTION: The thermosetting powder coating composition contains (A) the (co)polymer of the polar unsaturated compound which is the living polymer obtained by polymerizing the unsaturated compound in the presence of a hydroxycarbonyl compound having at least both of an alcoholic hydroxy group and a carbonyl group in one molecule when producing the polymer by (co)polymerizing the polar unsaturated compound by using an organic oxysalt compound as a catalyst, and (B) a component of a curing agent composition capable of curing the (co)polymer. COPYRIGHT: (C)2006,JPO&NCIPI

    摘要翻译： 要解决的问题：为了通过极性不饱和化合物的催化活性聚合提供生产（共）聚合物的方法，当通过聚合极性不饱和化合物制备（共）聚合物时; 并提供具有储存稳定性，外观特性，物理特性和化学特性的热固性粉末涂料组合物（例如丙烯酸类热固性粉末涂料组合物）。 解决方案：热固性粉末涂料组合物含有（A）极性不饱和化合物的（共）聚合物，它是通过在具有至少两个醇羟基的羟基羰基化合物存在下使不饱和化合物聚合而得到的活性聚合物 通过使用有机氧化锡化合物作为催化剂（极）使极性不饱和化合物聚合来制造聚合物时，在一个分子中具有羰基，（B）能够使（共）聚合物固化的固化剂组合物的成分 。 版权所有（C）2006，JPO＆NCIPI

    Method of producing conjugated diene
    4.
    发明专利
    Method of producing conjugated diene 有权
    生产混合二烯的方法

    公开(公告)号：JP2014172883A

    公开(公告)日：2014-09-22

    申请号：JP2013048314

    申请日：2013-03-11

    申请人： Mitsui Chemicals Inc ,  三井化学株式会社

    发明人： HORIUCHI NOBUHIKO ,  IKENAGA YUICHI ,  HAYASHI TAKAOMI

    IPC分类号： C07C1/24 ,  C07B61/00 ,  C07C11/167

    摘要： PROBLEM TO BE SOLVED: To provide a method of improving the results of intramolecular dehydration reactions of vicinal diol and producing conjugated diene in an industrially advantageous manner.SOLUTION: This invention provides a method of producing conjugated diene by the intramolecular dehydration of vicinal diol, in which pyrophosphate as a rare earth element is used as a catalyst.

    摘要翻译： 要解决的问题：提供一种以工业上有利的方式改进连位二醇和共轭二烯的分子内脱水反应结果的方法。本发明提供了一种通过邻二醇的分子内脱水制备共轭二烯的方法， 将作为稀土元素的焦磷酸盐用作催化剂。

    Method of producing olefin
    5.
    发明专利
    Method of producing olefin 有权
    生产烯烃的方法

    公开(公告)号：JP2013234139A

    公开(公告)日：2013-11-21

    申请号：JP2012106828

    申请日：2012-05-08

    申请人： Mitsui Chemicals Inc ,  三井化学株式会社

    发明人： HORIUCHI NOBUHIKO ,  IKENAGA YUICHI ,  HAYASHI TAKAOMI

    IPC分类号： C07C1/24 ,  C07B61/00 ,  C07C11/02 ,  C07C11/113

    摘要： PROBLEM TO BE SOLVED: To provide a method of producing an internal olefin with high selectivity when an olefin is produced by an intramolecular dehydration reaction of a secondary alcohol.SOLUTION: In a method of producing an olefin (B) represented by formula (II) by performing an intramolecular dehydration reaction of a secondary alcohol (A) represented by formula (I) in a gaseous phase condition in the presence of a solid catalyst (C) including an oxide or oxides of one or more elements selected from elements belonging to the periodic table group 1-15, water is supplied along with the secondary alcohol (A) to a reactor. (In the formula, R is a group selected from 1-20C hydrocarbon groups).

    摘要翻译： 要解决的问题：提供当通过仲醇的分子内脱水反应制备烯烃时以高选择性制备内烯烃的方法。溶液：在由式（II）表示的烯烃（B）的制备方法中， 通过在气相条件下，在固体催化剂（C）的存在下进行由式（I）表示的仲醇（A）的分子内脱水反应，所述固体催化剂（C）包括选自以下的元素的一种或多种元素的氧化物或氧化物： 周期表组1-15，将水与仲醇（A）一起供应到反应器。 （式中，R为选自1-20C烃基的基团）。

    PREPARATION OF POLYMER
    7.
    发明专利
    PREPARATION OF POLYMER 失效

    公开(公告)号：JP2000355606A

    公开(公告)日：2000-12-26

    申请号：JP2000112089

    申请日：2000-04-13

    申请人： MITSUI CHEMICALS INC

    发明人： NOBORI TADAHITO ,  SHIBAHARA ATSUSHI ,  KIYONO SHINJI ,  HAYASHI TAKAOMI ,  FUNAKI KATSUHIKO ,  HARA RETSU ,  MIZUTANI KAZUMI ,  TAKAGI USAJI

    IPC分类号： C08G65/10 ,  C08F4/00 ,  C08F8/00 ,  C08F12/14 ,  C08F16/36 ,  C08F20/00 ,  C08F22/40 ,  C08F26/06

    摘要： PROBLEM TO BE SOLVED: To easily obtain a polymer which contains no metal components and has no odor by performing anionic polymerization of a monomer comprising at least a polar unsatd. compd. in the presence of a phosphazenium compd. or the compd. plus an active hydrogen compd., wherein the average mol.wt. and the number of the generated molecules are controlled. SOLUTION: A phosphazenium compd. represented by the formula is used. In the formula, Z- is an anion having a configuration derived by eliminating a proton from an active hydrogen compd.; a-d are each 1 or 0 wherein they are not 0 at the same time; R is a 1-10C hydrocarbon group wherein two R's on the same nitrogen atom may be bonded together to form a ring structure. A polar unsatd. compd. to be used has a polar functional group selected from the group consisting of a CO group, a CN group and a pyridyl group as well as an unsatd. group in one molecule. It is pref. a compd. in which the above two form a conjugation system directly or indirectly. The active hydrogen compd. is pref. HCN, a monovalent carboxylic ester, a multivalent carboxylic ester, water, a monohydric alcohol, or the like.

    PRODUCTION OF 1,2-DIOXYETHANE DERIVATIVE
    8.
    发明专利
    PRODUCTION OF 1,2-DIOXYETHANE DERIVATIVE 失效

    公开(公告)号：JP2000128830A

    公开(公告)日：2000-05-09

    申请号：JP19903799

    申请日：1999-07-13

    申请人： MITSUI CHEMICALS INC

    发明人： NOBORI TADAHITO ,  HAYASHI TAKAOMI ,  HARA RETSU ,  KIYONO SHINJI ,  SHIBAHARA ATSUSHI ,  FUNAKI KATSUHIKO ,  MIZUTANI KAZUMI ,  TAKAGI USAJI

    IPC分类号： B01J31/02 ,  C07B61/00 ,  C07C67/26 ,  C07C69/16 ,  C07C69/96

    摘要： PROBLEM TO BE SOLVED: To obtain a 1,2-dioxyethane derivative in a high yield by using a phosphazenium compound as a catalyst on the reaction of an epoxy compound with a carboxylic acid ester, a carboxylic acid anhydride or a carbonate. SOLUTION: This method for producing a 1,2-dioxyethane compound comprises reacting an epoxy compound with an carboxylic acid ester, a carboxylic acid anhydride or a carbonate in the presence of a phosphazenium compound of the formula (R is a 1-10C hydrocarbon; Z- is a halogen anion, hydroxy anion, an alkoxy anion or the like), thus obtaining the corresponding 1,2-dioxyethane derivative, respectively. For example, phenyl glycidyl ether is dropped and reaction with phenyl acetate in the presence of tetrakis[tris(dimethylamino)phosphoranylidenamino]phosphonium of the formula to obtain 1,3-diphenoxy-2-propyl acetate in a production yield of 98%. The compound of the formula can exhibit an extremely high catalytic activity.

    PRODUCTION FOR ORGANIC COMPOUND
    9.
    发明专利
    PRODUCTION FOR ORGANIC COMPOUND 失效

    公开(公告)号：JP2000080049A

    公开(公告)日：2000-03-21

    申请号：JP10999599

    申请日：1999-04-16

    申请人： MITSUI CHEMICALS INC

    发明人： NOBORI TADAHITO ,  HAYASHI TAKAOMI ,  HARA RETSU ,  KIYONO SHINJI ,  SHIBAHARA ATSUSHI ,  FUNAKI KATSUHIKO ,  URAGAMI TATSUNOBU ,  TAKUMA HIROSUKE ,  TAKAGI USAJI

    IPC分类号： B01J31/02 ,  C07B41/04 ,  C07B61/00 ,  C07C41/03 ,  C07C43/13 ,  C07C43/23 ,  C07C43/295 ,  C07C69/78 ,  C07C319/14 ,  C07C323/10

    摘要： PROBLEM TO BE SOLVED: To effectively obtain an organic compound under a mild condition in high yield by performing an organic reaction in the presence of a specific phosphine oxide compound. SOLUTION: This organic compound is produced by performing an organic reaction in the presence of a phosphine oxide compound of formula I [R1 is H or a 1-10C hydrocarbon; (x) is 0-5.0]. An oxyalkylene derivative is produced preferably in the presence of the compound of formula I by reacting an epoxy compound with an alcohol, etc., of the formula: H-Q (H is an active hydrogen atom; Q is an organic group formed by removal of the active hydrogen atom from the alcohol, etc.), a carboxylic acid ester of formula II, a carboxylic acid anhydride of formula III, a sulfonic acid ester of formula IV (R2 is H or a 1-35C organic group; OZ1 is an organic group formed by removal of the active hydrogen atom from the alcohol, etc.; OZ2 is an organic group formed by removal of the active hydrogen atom from a carboxylic acid) or a carbonate of formula V (R3 is a 1-35C fatty hydrocarbon, etc.).

    PRODUCTION OF POLYALKYLENE OXIDE
    10.
    发明专利
    PRODUCTION OF POLYALKYLENE OXIDE 失效

    公开(公告)号：JPH11302371A

    公开(公告)日：1999-11-02

    申请号：JP10674598

    申请日：1998-04-16

    申请人： MITSUI CHEMICALS INC

    发明人： HAYASHI TAKAOMI ,  FUNAKI KATSUHIKO ,  SHIBAHARA ATSUSHI ,  MIZUTANI KAZUMI ,  HARA RETSU ,  KIYONO SHINJI ,  NOBORI TADAHITO ,  TAKAGI USAJI

    IPC分类号： C08G65/10 ,  C08G65/26

    摘要： PROBLEM TO BE SOLVED: To provide a method for simply and efficiently producing a polyalkylene oxide without containing a metal component at all and without leaving a malodor, using a polymerization initiator without especially causing problems in production or handling, and without the necessity for carrying out a special treatment before initiating the polymerization when polymerizing an alkylene oxide compound and producing the polyalkylene oxide. SOLUTION: An alkylene oxide compound is polymerized in the presence of a phosphine oxide compound represented by the formula [Rs are each the same kind or a different kind and a 1-10C hydrocarbon group; (x) denotes the amount of contained water molecules in terms of molar ratio and is 0-5.0] or the phosphine oxide compound and water or an active hydrogen compound selected from organic compounds each having a partial structural formula OH or NH.