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    METHOD FOR PRODUCING COMPOUND
    2.
    发明专利
    METHOD FOR PRODUCING COMPOUND 审中-公开

    公开(公告)号：JP2013253041A

    公开(公告)日：2013-12-19

    申请号：JP2012129727

    申请日：2012-06-07

    申请人： DAINIPPON INK & CHEMICALS

    发明人： HORIGUCHI MASAHIRO ,  AOKI YOSHIO ,  HAYASHI MASANAO ,  KUSUMOTO TETSUO

    IPC分类号： C07C51/56 ,  A61K8/81 ,  A61K47/32 ,  C07B41/10 ,  C07B41/12 ,  C07B61/00 ,  C07C55/02 ,  C07C67/12 ,  C07C69/92 ,  C07C231/02 ,  C07C237/22 ,  C07C251/88 ,  C07C381/14 ,  C07F7/10

    摘要： PROBLEM TO BE SOLVED: To provide a method for producing a compound having an ester bond and/or amide bond, with a small content of impurities in high yield; and to provide a high purity compound obtained by the method.SOLUTION: There is provided a method for producing a mixed acid anhydride (4) by adding a compound (1) having at least one carboxy group and a base (2) simultaneously without mixing in advance to an acid halide compound (3) to react them. Also a method for producing an ester compound and/or amide compound (6) is provided which comprises: adding a compound (1) having at least one carboxy group and a base (2) simultaneously without mixing in advance to an acid halide compound (3) to react them to produce a mixed acid anhydride (4); and thereafter reacting with a compound (5) having at least one group selected from a hydroxy group, mercapto group and/or amino group.

    Comonomer and a method of manufacturing the same for polycarbonate resin production
    3.
    发明专利
    Comonomer and a method of manufacturing the same for polycarbonate resin production 有权

    公开(公告)号：JP5366453B2

    公开(公告)日：2013-12-11

    申请号：JP2008163387

    申请日：2008-06-23

    申请人： 出光興産株式会社

    发明人： 康弘 石川 ,  浩一 菅 ,  亜起 藤岡

    IPC分类号： C08G64/18 ,  C07B41/12 ,  C07B63/00 ,  C08G65/332

    摘要： PROBLEM TO BE SOLVED: To provide a comonomer for production of polycarbonate resin comprising a high-purity diester diol, and a method for producing the same. SOLUTION: The comonomer for production of a polycarbonate resin is represented by the general formula (I), wherein R 1 and R 2 each independently represents a 1-3C alkyl group, Y represents a 2-15C linear or branched alkylene group, p and q each independently represents an integer of 0-4, respectively, r represents an integer of 2-450, and has a tin content (as an element) of not more than 10 ppm. The present invention is a method for producing a comonomer for production of a polycarbonate resin having a tin content (as an element) of not more than 10 ppm by esterification or transesterfication reaction of hydroxybenzoic acid alkyl esters and polyalkylene ether glycol in the presence of a tin-based catalyst to obtain a reaction mixture containing a compound represented by the general formula (I), followed by a treatment of the reaction mixture with an aqueous phosphoric acid solution or a solid adsorbent. COPYRIGHT: (C)2010,JPO&INPIT