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    Dispersion, alignment and deposition of nanotubes
    1.
    发明授权
    Dispersion, alignment and deposition of nanotubes 有权
    纳米管的分散，对准和沉积

    公开(公告)号：US08197888B2

    公开(公告)日：2012-06-12

    申请号：US12112675

    申请日：2008-04-30

    申请人： Hung-Jue Sue ,  Xing Cheng ,  Dazhi Sun ,  Huifeng Li ,  Chien-Chia Chu

    发明人： Hung-Jue Sue ,  Xing Cheng ,  Dazhi Sun ,  Huifeng Li ,  Chien-Chia Chu

    IPC分类号： B05D5/12 ,  B05D1/32

    CPC分类号： B82Y30/00 ,  C08K3/041 ,  C08K3/22 ,  C08K3/346 ,  C09D7/70 ,  C08L63/00

    摘要： A dispersible nanocomposite comprising nanotubes associated with nanoplatelets. A method for creating an exfoliated nanotubes solution, aligning nanotubes and depositing them on a substrate or in matrix. In one embodiment, the method includes a nanocomposite of at least one nanotube electrostatically associated with at least one nanoplatelet. The nanoplatelets may be removed from the suspension by altering the ionic strength to create an exfoliated nanotube solution. The exfoliated nanotube solution for injection into microchannel templates and aligned deposition.

    摘要翻译： 包含与纳米片相关的纳米管的可分散的纳米复合材料。 一种用于产生剥离的纳米管溶液的方法，将纳米管排列并将其沉积在基底或基质上。 在一个实施方案中，该方法包括与至少一个纳米血小板静电相关的至少一个纳米管的纳米复合物。 可以通过改变离子强度从悬浮液中除去纳米片，以产生剥离的纳米管溶液。 用于注入微通道模板和对准沉积的剥离的纳米管溶液。

    Intercalation agent free compositions useful to make nanocomposite polymers
    2.
    发明授权
    Intercalation agent free compositions useful to make nanocomposite polymers 有权
    可用于制备纳米复合材料聚合物的嵌入剂自由组合物

    公开(公告)号：US08114925B2

    公开(公告)日：2012-02-14

    申请号：US12515692

    申请日：2007-11-16

    申请人： Luyi Sun ,  Woong Jae Boo ,  Hung-Jue Sue ,  Maurice J. Marks ,  Richard F. Fibiger ,  Michael S. Paquette

    发明人： Luyi Sun ,  Woong Jae Boo ,  Hung-Jue Sue ,  Maurice J. Marks ,  Richard F. Fibiger ,  Michael S. Paquette

    IPC分类号： C08L63/00 ,  C08K9/00 ,  C08K3/00 ,  C08K3/34

    CPC分类号： C08J3/2053 ,  B82Y30/00 ,  C08J5/005 ,  C08J2363/00 ,  Y10S977/778 ,  Y10S977/779 ,  Y10S977/783 ,  Y10S977/785 ,  Y10S977/786 ,  Y10S977/787

    摘要： A method for preparing a filler composition useful for preparing a nanocomposite polymer is provided. The method includes a first step of dispersing a water dispersible filler material in a liquid comprising water to form a dispersion and a second step of replacing at least a portion of the water of the liquid with an organic solvent. The resulting filler composition features a water concentration of the liquid of less than six percent by weight, and the average size of at least one dimension of the filler material is less than two hundred nanometers upon examination by transmission electron microscopy of a representative freeze dried sample of the dispersion of the first step. A nanocomposite polymer, particularly and epoxy resin composition, can be prepared by mixing the above-made filler composition with one or more polymer, polymer component, monomer or prepolymer.

    摘要翻译： 提供了制备用于制备纳米复合材料聚合物的填料组合物的方法。 该方法包括将水分散性填料分散在包含水的液体中以形成分散体的第一步骤和用有机溶剂代替液体的至少一部分水的第二步骤。 所得填料组合物的特征在于液体的水浓度小于6重量％，并且通过代表性冷冻干燥样品的透射电子显微镜检查，填充材料的至少一个维度的平均尺寸小于二百纳米 的第一步的分散。 可以通过将上述填充剂组合物与一种或多种聚合物，聚合物组分，单体或预聚物混合来制备纳米复合材料聚合物，特别是环氧树脂组合物。

    Water-soluble nanoparticles with controlled aggregate sizes
    3.
    发明授权
    Water-soluble nanoparticles with controlled aggregate sizes 有权
    具有可控骨料尺寸的水溶性纳米颗粒

    公开(公告)号：US08101838B2

    公开(公告)日：2012-01-24

    申请号：US12238052

    申请日：2008-09-25

    申请人： Dazhi Sun ,  William Neil Everett ,  Hung-Jue Sue ,  Nobuo Miyatake

    发明人： Dazhi Sun ,  William Neil Everett ,  Hung-Jue Sue ,  Nobuo Miyatake

    IPC分类号： C08F226/10

    CPC分类号： C08F226/10 ,  Y10S977/774 ,  Y10S977/811

    摘要： A method of forming dispersed water-soluble quantum dots and tuning water-soluble quantum dot aggregate size by providing a plurality of water-soluble quantum dots in a dispersion, the plurality of water-soluble quantum dots are modified with an amphiphilic polymer, and by adding an amount of the amphiphilic polymer to the dispersion such that the ratio of the amphiphilic polymer units to quantum dots is maintained higher to obtain dispersions of smaller quantum dot aggregates and kept lower to obtain dispersions of larger quantum dot aggregates.

    摘要翻译： 通过在分散体中提供多个水溶性量子点，形成分散的水溶性量子点和调节水溶性量子点聚集体尺寸的方法，多个水溶性量子点用两亲性聚合物改性，并通过 向分散体中加入一定量的两亲聚合物，使得两亲性聚合物单元与量子点的比例保持较高，以获得较小量子点聚集体的分散体并保持较低以获得较大量子点聚集体的分散体。

    ZINC OXIDE POLYMER NANOCOMPOSITES AND METHODS OF PRODUCING ZINC OXIDE POLYMER NANOCOMPOSITES
    4.
    发明申请
    ZINC OXIDE POLYMER NANOCOMPOSITES AND METHODS OF PRODUCING ZINC OXIDE POLYMER NANOCOMPOSITES 审中-公开
    氧化锌聚合物纳米复合材料和生产氧化锌聚合物纳米复合材料的方法

    公开(公告)号：US20070004840A1

    公开(公告)日：2007-01-04

    申请号：US11427936

    申请日：2006-06-30

    申请人： Nobuo Miyatake ,  Yuntao Li ,  Hung-Jue Sue ,  Katsumi Yamaguchi

    发明人： Nobuo Miyatake ,  Yuntao Li ,  Hung-Jue Sue ,  Katsumi Yamaguchi

    IPC分类号： C08K3/22

    CPC分类号： C08J3/14 ,  B82Y30/00 ,  C01B13/32 ,  C01G9/02 ,  C01P2004/64 ,  C08K3/22

    摘要： A zinc oxide polymer nanocomposite composed of zinc oxide nanoparticles. The zinc oxide nanoparticles of the nanocomposite have an average particle size of about 1 nanometer to about 20 nanometers. Suitable polymers of the nanocomposites have less than about 500 ppm alkali metal. A process is provided for preparing the zinc oxide polymer nanocomposites comprising a) preparing a first combination comprising zinc oxide nanoparticles and a polymer; b) preparing a second combination comprising the first combination and an organic solvent; and c) precipitating the zinc oxide nanoparticles and the polymer out of the second combination. The zinc oxide nanoparticles of the first combination have an average particle size of between about 1 nanometer and about 20 nanometers.

    摘要翻译： 由氧化锌纳米粒子组成的氧化锌聚合物纳米复合材料。 纳米复合材料的氧化锌纳米粒子具有约1纳米至约20纳米的平均粒度。 纳米复合材料的合适聚合物具有小于约500ppm的碱金属。 提供了一种制备氧化锌聚合物纳米复合材料的方法，包括：a）制备包含氧化锌纳米颗粒和聚合物的第一组合; b）制备包含第一组合和有机溶剂的第二组合; 和c）使所述氧化锌纳米颗粒和所述聚合物从所述第二组合中沉淀出来。 第一组合物的氧化锌纳米颗粒的平均粒度为约1纳米至约20纳米。

    Stabilization of polymers with zinc oxide nanoparticles
    5.
    发明申请
    Stabilization of polymers with zinc oxide nanoparticles 审中-公开
    用氧化锌纳米粒子稳定聚合物

    公开(公告)号：US20060194910A1

    公开(公告)日：2006-08-31

    申请号：US11312043

    申请日：2005-12-20

    申请人： Nobuo Miyatake ,  Hung-Jue Sue ,  Yuntao Li ,  Katsumi Yamaguchi

    发明人： Nobuo Miyatake ,  Hung-Jue Sue ,  Yuntao Li ,  Katsumi Yamaguchi

    IPC分类号： C08K3/22

    CPC分类号： C01B13/32 ,  B82Y30/00 ,  C01G9/02 ,  C01P2004/64

    摘要： A composition and method of making a stabilizer for polymers. The composition has zinc oxide (ZnO) nanoparticles dispersed and having an average size of no more than about 15 nanometers, wherein the ZnO nanoparticles are provided as an additive to a polymeric material, thereby forming a stabilized polymer composite in which the ZnO nanoparticles remain dispersed and have an average size of no more than about 15 nanometers. The stabilized polymer composite is stabilized against heat and ultraviolet light. The polymeric material can be a (meth)acrylic resin, a styrenic resin, a pre-cure epoxy resin, or combinations thereof. In a concentrated form, the composition has ZnO nanoparticles that are typically less than 20% of the stabilized polymer composite. The stabilizer is polymerizable and may include additional additives.

    摘要翻译： 制备聚合物稳定剂的组合物和方法。 该组合物具有分散的平均尺寸不大于约15纳米的氧化锌（ZnO）纳米颗粒，其中ZnO纳米颗粒作为添加剂提供到聚合物材料中，由此形成稳定的聚合物复合材料，其中ZnO纳米颗粒保持分散 并且具有不超过约15纳米的平均尺寸。 稳定的聚合物复合材料耐热和紫外光稳定。 聚合物材料可以是（甲基）丙烯酸树脂，苯乙烯树脂，预固化环氧树脂或其组合。 在浓缩形式中，组合物具有通常小于稳定的聚合物复合材料的20％的ZnO纳米颗粒。 稳定剂是可聚合的并且可以包括另外的添加剂。

    Intercalation agent free compositions useful to make nanocomposite polymers
    6.
    发明授权
    Intercalation agent free compositions useful to make nanocomposite polymers 失效
    可用于制备纳米复合材料聚合物的嵌入剂自由组合物

    公开(公告)号：US08481616B2

    公开(公告)日：2013-07-09

    申请号：US13351004

    申请日：2012-01-16

    申请人： Luyi Sun ,  Jae Woong Boo ,  Hung-jue Sue ,  Maurice J. Marks ,  Richard F. Fibiger ,  Michael S. Paquette

    发明人： Luyi Sun ,  Jae Woong Boo ,  Hung-jue Sue ,  Maurice J. Marks ,  Richard F. Fibiger ,  Michael S. Paquette

    IPC分类号： C08G59/18 ,  C08K9/00 ,  C08K7/00 ,  C08K3/34 ,  B32B27/20 ,  B32B27/38

    CPC分类号： C08J3/2053 ,  B82Y30/00 ,  C08J5/005 ,  C08J2363/00 ,  Y10S977/778 ,  Y10S977/779 ,  Y10S977/783 ,  Y10S977/785 ,  Y10S977/786 ,  Y10S977/787

    摘要： A two step method for preparing a filler composition, the filler composition useful to prepare a nanocomposite polymer and an epoxy nanocomposite coating. First, disperse a water dispersible filler material in a liquid comprising water, but without any added intercalation agent, to form a dispersion. Second, replace at least a portion of the water of the liquid with an organic solvent so that the water concentration of the liquid is less than six percent by weight to form the filler composition, the average size of at least one dimension of the filler material being less than two hundred nanometers upon examination by transmission electron microscopy of a representative freeze dried sample of the dispersion of the first step. A nanocomposite polymer can be prepared by mixing the filler composition with one or more polymer, polymer component, monomer or prepolymer to produce a polymer containing the filler composition.

    摘要翻译： 用于制备填料组合物的两步法，用于制备纳米复合聚合物和环氧纳米复合涂层的填料组合物。 首先，将水分散性填料分散在包含水的液体中，但不加任何添加的嵌入剂，以形成分散体。 第二，用有机溶剂代替液体的至少一部分水，使得液体的水浓度小于6重量％以形成填料组合物，填料的至少一个维度的平均尺寸 通过透射电子显微镜检查第一步的分散体的代表性冷冻干燥样品，小于二百纳米。 可以通过将填料组合物与一种或多种聚合物，聚合物组分，单体或预聚物混合以制备含有填料组合物的聚合物来制备纳米复合聚合物。

    Methods of producing zinc oxide polymer nanocomposites
    7.
    发明申请
    Methods of producing zinc oxide polymer nanocomposites 审中-公开
    生产氧化锌聚合物纳米复合材料的方法

    公开(公告)号：US20100249335A1

    公开(公告)日：2010-09-30

    申请号：US12802164

    申请日：2010-06-01

    申请人： Nobuo Miyatake ,  Yuntao Li ,  Hung-Jue Sue ,  Katsumi Yamaguchi

    发明人： Nobuo Miyatake ,  Yuntao Li ,  Hung-Jue Sue ,  Katsumi Yamaguchi

    IPC分类号： C08F8/42

    CPC分类号： C08J3/14 ,  B82Y30/00 ,  C01B13/32 ,  C01G9/02 ,  C01P2004/64 ,  C08K3/22

    摘要： A zinc oxide polymer nanocomposite composed of zinc oxide nanoparticles. The zinc oxide nanoparticles of the nanocomposite have an average particle size of about 1 nanometer to about 20 nanometers. Suitable polymers of the nanocomposites have less than about 500 ppm alkali metal. A process is provided for preparing the zinc oxide polymer nanocomposites comprising a) preparing a first combination comprising zinc oxide nanoparticles and a polymer; b) preparing a second combination comprising the first combination and an organic solvent; and c) precipitating the zinc oxide nanoparticles and the polymer out of the second combination. The zinc oxide nanoparticles of the first combination have an average particle size of between about 1 nanometer and about 20 nanometers.

    摘要翻译： 由氧化锌纳米粒子组成的氧化锌聚合物纳米复合材料。 纳米复合材料的氧化锌纳米粒子具有约1纳米至约20纳米的平均粒度。 纳米复合材料的合适聚合物具有小于约500ppm的碱金属。 提供了一种制备氧化锌聚合物纳米复合材料的方法，包括：a）制备包含氧化锌纳米颗粒和聚合物的第一组合; b）制备包含第一组合和有机溶剂的第二组合; 和c）使所述氧化锌纳米颗粒和所述聚合物从所述第二组合中沉淀出来。 第一组合物的氧化锌纳米颗粒的平均粒度为约1纳米至约20纳米。

    ISOLATED NANOTUBES AND POLYMER NANOCOMPOSITES
    8.
    发明申请
    ISOLATED NANOTUBES AND POLYMER NANOCOMPOSITES 审中-公开
    分离的纳米颗粒和聚合物纳米复合材料

    公开(公告)号：US20100197832A1

    公开(公告)日：2010-08-05

    申请号：US12698602

    申请日：2010-02-02

    申请人： Dazhi SUN ,  Hung-Jue SUE

    发明人： Dazhi SUN ,  Hung-Jue SUE

    IPC分类号： C08L63/00

    CPC分类号： C08L63/00 ,  C08K7/24

    摘要： A method for producing a nanocomposite, the nanocomposite comprises at least one nanofiller, wherein said nanofiller comprises at least one nanotube, and a medium comprising a polymeric matrix. Further, the nanotube comprises at least one exfoliated nanotube. The method comprises agglomerating at least one nanotube from a nanotube and nanoplatelet dispersion in a solvent. Additionally, the method comprises redispersing at least one nanotube in a matrix precursor solution.

    摘要翻译： 一种制备纳米复合材料的方法，所述纳米复合材料包含至少一种纳米填料，其中所述纳米填料包含至少一种纳米管，和包含聚合物基质的介质。 此外，纳米管包括至少一个剥离的纳米管。 该方法包括将来自纳米管的至少一个纳米管和纳米血小板分散体在溶剂中凝聚。 另外，该方法包括在基质前体溶液中再分散至少一种纳米管。