公开(公告)号：US20070209093A1

公开(公告)日：2007-09-06

申请号：US11547199

申请日：2005-03-31

申请人： Kazuyuki Tohji ,  Yashinori Satoh ,  Hirohisa Kikuyama ,  Masahide Waki ,  Shiniji Hashiguchi ,  Yasutaka Tashiro

发明人： Kazuyuki Tohji ,  Yashinori Satoh ,  Hirohisa Kikuyama ,  Masahide Waki ,  Shiniji Hashiguchi ,  Yasutaka Tashiro

IPC分类号： C01B31/02 ,  C01B31/00

CPC分类号： H01M4/96 ,  A61L27/08 ,  A61L2400/12 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/168 ,  C01B32/17 ,  C01B2202/06 ,  C04B35/83 ,  C04B2235/445 ,  C04B2235/5288 ,  C04B2235/6562 ,  C04B2235/6567 ,  C04B2235/666 ,  C04B2235/77 ,  C04B2235/96 ,  H01M4/587

摘要： Disclosed are a carbon nanotube aggregate and a method for forming a carbon nanotube aggregate. An aggregate can be obtained by fluorinating the surfaces of carbon nanotubes. The method for forming a carbon nanotube aggregate is characterized by comprising a step for firing a plurality of fluorinated carbon nanotubes.

摘要翻译： 公开了一种碳纳米管集合体和形成碳纳米管集合体的方法。 可以通过氟化碳纳米管的表面获得聚集体。 形成碳纳米管集合体的方法的特征在于包括烧制多个氟化碳纳米管的步骤。

公开(公告)号：US07740825B2

公开(公告)日：2010-06-22

申请号：US11547199

申请日：2005-03-31

申请人： Kazuyuki Tohji ,  Yoshinori Satoh ,  Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Yasutaka Tashiro

发明人： Kazuyuki Tohji ,  Yoshinori Satoh ,  Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Yasutaka Tashiro

IPC分类号： D01F9/12

CPC分类号： H01M4/96 ,  A61L27/08 ,  A61L2400/12 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/168 ,  C01B32/17 ,  C01B2202/06 ,  C04B35/83 ,  C04B2235/445 ,  C04B2235/5288 ,  C04B2235/6562 ,  C04B2235/6567 ,  C04B2235/666 ,  C04B2235/77 ,  C04B2235/96 ,  H01M4/587

摘要： A carbon nanotube aggregate and a method for forming a carbon nanotube aggregate are provided. The carbon nanotube aggregate can be formed by treating carbon nanotubes with fluorine gas and sintering the resulting fluorinated carbon nanotubes. A carbon nanotube aggregate can be formed which does not contain a binder or resin matrix.

摘要翻译： 提供碳纳米管集合体和形成碳纳米管集合体的方法。 可以通过用氟气处理碳纳米管并烧结所得氟化碳纳米管来形成碳纳米管集合体。 可以形成不含粘合剂或树脂基体的碳纳米管集合体。

公开(公告)号：US07268256B2

公开(公告)日：2007-09-11

申请号：US10514192

申请日：2003-04-17

申请人： Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Tetsuo Nishida ,  Yasutaka Tashiro ,  Kenji Aoki

发明人： Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Tetsuo Nishida ,  Yasutaka Tashiro ,  Kenji Aoki

IPC分类号： C07C211/62 ,  C07C209/84

CPC分类号： H01G9/038 ,  C07C209/84 ,  H01G11/62 ,  H01M6/166 ,  H01M10/0568 ,  H01M2300/0025 ,  Y02E60/13 ,  C07C211/63

摘要： Provided is a method for purifying a quaternary alkyl ammonium salt enabling the obtainment of a particulate quaternary alkyl ammonium salt having a low water content at a high yield which is suitably used as an electrolyte in an electrolytic solution.The method for the purification of a quaternary alkyl ammonium salt comprises dispersing a quaternary alkyl ammonium salt to be purified into an organic solvent to allow it to form a suspension there. The alkyl groups constituting the quaternary alkyl ammonium salt have 1 to 5 carbon atoms each. The quaternary alkyl ammonium salt to be purified is dispersed into the organic solvent to make a suspension, and then the particles are washed with an alcohol solvent.

摘要翻译： 本发明提供一种纯化季铵烷基铵盐的方法，其能够以高收率获得低水含量的季铵烷基铵盐，其适合用作电解液中的电解质。 纯化季烷基铵盐的方法包括将要纯化的季烷基铵盐分散在有机溶剂中以使其在那里形成悬浮液。 构成季烷基铵盐的烷基各有1〜5个碳原子。 将要纯化的季烷基铵盐分散在有机溶剂中以制成悬浮液，然后用醇溶剂洗涤颗粒。

公开(公告)号：US20060020147A1

公开(公告)日：2006-01-26

申请号：US10514192

申请日：2003-04-17

申请人： Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Tetsuo Nishida ,  Yasutaka Tashiro ,  Kenji Aoki

发明人： Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Tetsuo Nishida ,  Yasutaka Tashiro ,  Kenji Aoki

IPC分类号： C07C209/84

CPC分类号： H01G9/038 ,  C07C209/84 ,  H01G11/62 ,  H01M6/166 ,  H01M10/0568 ,  H01M2300/0025 ,  Y02E60/13 ,  C07C211/63

摘要： Provided is a method for purifying a quaternary alkyl ammonium salt enabling the obtainment of a particulate quaternary alkyl ammonium salt having a low water content at a high yield which is suitably used as an electrolyte in an electrolytic solution. The method for the purification of a quaternary alkyl ammonium salt comprises dispersing a quaternary alkyl ammonium salt to be purified into an organic solvent to allow it to form a suspension there. The alkyl groups constituting the quaternary alkyl ammonium salt have 1 to 5 carbon atoms each. The quaternary alkyl ammonium salt to be purified is dispersed into the organic solvent to make a suspension, and then the particles are washed with an alcohol solvent.

摘要翻译： 本发明提供一种纯化季铵烷基铵盐的方法，其能够以高收率获得低水含量的季铵烷基铵盐，其适合用作电解液中的电解质。 纯化季烷基铵盐的方法包括将要纯化的季烷基铵盐分散在有机溶剂中以使其在那里形成悬浮液。 构成季烷基铵盐的烷基各有1〜5个碳原子。 将要纯化的季烷基铵盐分散在有机溶剂中以制成悬浮液，然后用醇溶剂洗涤颗粒。

公开(公告)号：US20080029487A1

公开(公告)日：2008-02-07

申请号：US11722120

申请日：2005-12-19

申请人： Hirohisa Kikuyama ,  Masahide Waki ,  Kanenori Ito ,  Takanobu Kujime ,  Keiichi Nii ,  Rui Hasebe ,  Hitoshi Tsurumaru ,  Hideki Nakashima

发明人： Hirohisa Kikuyama ,  Masahide Waki ,  Kanenori Ito ,  Takanobu Kujime ,  Keiichi Nii ,  Rui Hasebe ,  Hitoshi Tsurumaru ,  Hideki Nakashima

IPC分类号： H01L21/306 ,  C23F1/26

CPC分类号： H01L21/32134 ,  C23F1/26 ,  H01L27/124

摘要： A fine treatment agent according to the present invention is a fine treatment agent for the fine treatment of a multilayer film, including a tungsten film and a silicon oxide film comprising at least one from among hydrogen fluoride, nitric acid, ammonium fluoride and ammonium chloride. Thus, a fine treatment agent which makes fine treatment on a multilayer film, including a tungsten film and a silicon oxide film, possible by controlling the etching rate and a fine treatment method using the same can be provided.

摘要翻译： 根据本发明的精细处理剂是用于精细处理包括钨膜和包含氟化氢，硝酸，氟化铵和氯化铵中的至少一种的氧化硅膜的多层膜的精细处理剂。 因此，可以提供通过控制蚀刻速率和使用其的精细处理方法对包括钨膜和氧化硅膜在内的多层膜进行精细处理的精细处理剂。

公开(公告)号：US07175823B2

公开(公告)日：2007-02-13

申请号：US10505802

申请日：2003-02-27

申请人： Hirohisa Kikuyama ,  Masahide Waki ,  Hiroto Izumi ,  Hirofumi Yazaki ,  Kenji Aoki ,  Shinji Hashiguchi ,  Masatsugu Kawawaki ,  Yuko Murakami

发明人： Hirohisa Kikuyama ,  Masahide Waki ,  Hiroto Izumi ,  Hirofumi Yazaki ,  Kenji Aoki ,  Shinji Hashiguchi ,  Masatsugu Kawawaki ,  Yuko Murakami

IPC分类号： C01G33/00 ,  C01G35/00

CPC分类号： C01G33/003 ,  C01G33/00 ,  C01G35/00 ,  C01G35/003 ,  C01P2006/80 ,  C22B3/20 ,  C22B3/22 ,  C22B3/44 ,  C22B34/24 ,  Y02P10/234

摘要： The present invention provides a method enabling the high purification of a niobium compound and/or tantalum compound in a simplified manner at a low cost. This is accomplished by providing a method enabling the high purification of a niobium compound and/or tantalum compound comprising the steps of preparing a solution containing niobium and/or tantalum, allowing a precipitate comprising niobium and/or tantalum to develop, separating the precipitate by filtration from the filtrate, converting the precipitate to a liquid melt or taking the filtrate, and separating a niobium compound from a tantalum compound or vice versa by utilizing the difference in solubility to the solvent between the niobium compound and the tantalum compound.

摘要翻译： 本发明提供了一种能够以低成本简便地进行铌化合物和/或钽化合物的高纯化的方法。 这是通过提供一种能够高效纯化铌化合物和/或钽化合物的方法实现的，包括以下步骤：制备含有铌和/或钽的溶液，使包含铌和/或钽的沉淀物显影，分离沉淀物 从滤液过滤，将沉淀物转化为液体熔融物或取出滤液，并通过利用铌化合物和钽化合物之间的溶剂的溶解度差异将钽铌化合物与钽化合物分离，反之亦然。

公开(公告)号：US20070112183A1

公开(公告)日：2007-05-17

申请号：US10555384

申请日：2004-05-06

申请人： Hisao Kitano ,  Hiroshi Shimizu ,  Masakatsu Nozaki ,  Fumio Tanimoto ,  Hirohisa Kikuyama ,  Masahide Waki ,  Kanenori Ito ,  Shinji Hashiguchi

发明人： Hisao Kitano ,  Hiroshi Shimizu ,  Masakatsu Nozaki ,  Fumio Tanimoto ,  Hirohisa Kikuyama ,  Masahide Waki ,  Kanenori Ito ,  Shinji Hashiguchi

IPC分类号： C08B37/08

CPC分类号： C07H5/06 ,  A23K10/20 ,  A23K20/163 ,  A23K20/24 ,  A23K50/80 ,  C08B37/003

摘要： This invention aims to develop a chitin oligomer composition and/or a chitosan oligomer composition wherein the content of an oligomer from a trimer to a decamer is 60% or more, and to develop a process for preparing the above-mentioned oligomer composition. The object of the invention can be achieved by mixing hydrofluoric acid or hydrohalogenated acid other than hydrofluoric acid and hydrofluoric acid with a chitin-based material and/or a chitosan-based material.

摘要翻译： 本发明的目的在于开发几丁质低聚物组合物和/或壳聚糖低聚物组合物，其中从三聚体到十聚体的低聚物的含量为60％以上，并且开发制备上述低聚物组合物的方法。 本发明的目的可以通过将除氢氟酸和氢氟酸之外的氢氟酸或氢卤酸与几丁质基材料和/或壳聚糖基材料混合来实现。

公开(公告)号：US06955795B2

公开(公告)日：2005-10-18

申请号：US10149266

申请日：2000-12-11

申请人： Hirohisa Kikuyama ,  Toshirou Fukudome ,  Masahide Waki ,  Tomoyuki Deguchi

发明人： Hirohisa Kikuyama ,  Toshirou Fukudome ,  Masahide Waki ,  Tomoyuki Deguchi

IPC分类号： C01B25/455 ,  C01D15/00 ,  C01B25/10

CPC分类号： C01D15/005

摘要： In order to provide a method for producing lithium hexafluorophosphate capable of producing lithium hexafluorophosphate of a higher purity than in the related art without the necessity for after-treatment for removal of impurities, a method is characterized by filtering lithium hexafluorophosphate coexisting with a solvent and then carrying out after-filtering drying in a gas atmosphere containing PF5.

摘要翻译： 为了提供能够生产比现有技术更高纯度的六氟磷酸锂的六氟磷酸锂的方法，而不需要后处理除去杂质，一种方法的特征在于过滤与溶剂共存的六氟磷酸锂，然后 在含有PF 5的气体气氛中进行后处理干燥。

公开(公告)号：US20050123459A1

公开(公告)日：2005-06-09

申请号：US10505806

申请日：2003-02-27

申请人： Hirohisa Kikuyama ,  Masahide Waki ,  Hiroto Izumi ,  Hirofumi Yazaki ,  Kenji Aoki ,  Shinji Hashiguchi ,  Masatsugu Kawawaki ,  Yuko Murakami

发明人： Hirohisa Kikuyama ,  Masahide Waki ,  Hiroto Izumi ,  Hirofumi Yazaki ,  Kenji Aoki ,  Shinji Hashiguchi ,  Masatsugu Kawawaki ,  Yuko Murakami

IPC分类号： C01G33/00 ,  C01G35/00 ,  C01G35/02 ,  C22B3/44 ,  C22B34/20 ,  C22B34/24

CPC分类号： C01G35/00 ,  C01G33/00 ,  C01G35/02 ,  C01P2006/80 ,  C22B3/10 ,  C22B3/44 ,  C22B34/20 ,  C22B34/24 ,  Y02P10/234

摘要： The present invention provides a method for purifying a niobium compound and/or tantalum compound in a simplified manner at a low cost. This is accomplished by providing a method for purifying a niobium compound and/or tantalum compound whereby a niobium compound and/or tantalum compound dissolved in a solvent is allowed to precipitate to be isolated.

摘要翻译： 本发明提供了一种以低成本简化的方法纯化铌化合物和/或钽化合物的方法。 这是通过提供一种纯化铌化合物和/或钽化合物的方法来实现的，由此使溶解在溶剂中的铌化合物和/或钽化合物沉淀以分离。

公开(公告)号：US06896866B2

公开(公告)日：2005-05-24

申请号：US10149881

申请日：2000-12-14

申请人： Hirohisa Kikuyama ,  Masahide Waki ,  Kazuyuki Fujimoto ,  Yoshinori Nakagawa

发明人： Hirohisa Kikuyama ,  Masahide Waki ,  Kazuyuki Fujimoto ,  Yoshinori Nakagawa

IPC分类号： C01G41/04

CPC分类号： C01G41/04

摘要： A method for purifying tungsten hexafluoride of high purity, capable of producing tungsten hexafluoride of higher purity than that of the related art, readily and at a low cost. A method for purifying tungsten hexafluoride of high purity, characterized in that tungsten hexafluoride containing molybdenum hexafluoride as an impurity, makes contact with a layer, in which a metal or an alloy is packed, containing at least one of molybdenum, tungsten, copper, nickel, iron, cobalt, zinc, titanium, aluminum, calcium, and magnesium at a temperature ranging from 0° C. to 100° C.

摘要翻译： 能够容易且成本低廉地纯化六氟化钨，能够生产纯度高于现有技术的六氟化钨的方法。 一种净化高纯度六氟化钨的方法，其特征在于含有六氟化钼作为杂质的六氟化钨使其与包含钼，钨，铜，镍中的至少一种的金属或合金的层相接触 ，铁，钴，锌，钛，铝，钙和镁，温度范围为0℃至100℃。