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    Method for purifying polyethylene glycol having one amino group
    91.
    发明授权
    Method for purifying polyethylene glycol having one amino group 有权
    一种具有一个氨基的聚乙二醇的纯化方法

    公开(公告)号：US09458292B2

    公开(公告)日：2016-10-04

    申请号：US14780310

    申请日：2014-03-24

    申请人： NOF CORPORATION

    发明人： Hiroki Yoshioka ,  Shingo Kimura ,  Midori Hirai

    IPC分类号： C08G65/34 ,  C08G65/30 ,  C08G65/333

    CPC分类号： C08G65/34 ,  C08G65/30 ,  C08G65/333

    摘要： A method for purifying a polyethylene glycol compound having one amino group, which includes (A) preparing an aqueous solution of the compound having a pH of 1 to 5, (B) an extracting step of mixing the aqueous solution with a mixed organic solvent to cause layer separation into organic and aqueous layers, wherein a ratio of an organic solvent I is 25 to 65% by mass and a ratio of an organic solvent II is 75 to 35% by mass, the organic solvent I is selected from an aromatic hydrocarbon and an ester, the organic solvent II is a halogenated hydrocarbon, and a mixing ratio Y of I to II, temperature T (° C.) at mixing, and molecular weight M of the compound satisfy the following relationship: 1.9×10−6M+0.09≦Y−0.015T≦−1.4×10−6M+0.44 and (C) recovering the compound from the aqueous layer.

    Process for preparing polyether polyols
    94.
    发明授权
    Process for preparing polyether polyols 有权
    制备聚醚多元醇的方法

    公开(公告)号：US09006499B2

    公开(公告)日：2015-04-14

    申请号：US14178517

    申请日：2014-02-12

    申请人： Bayer MaterialScience AG

    发明人： Klaus Lorenz ,  Marcus Eichmann

    IPC分类号： C08G65/34 ,  C08G65/00 ,  C08G65/30

    CPC分类号： C08G65/34 ,  C08G65/00 ,  C08G65/2609 ,  C08G65/30

    摘要： The present invention relates to a process for preparing polyether polyols by base-catalyzed addition of alkylene oxides (epoxides) onto starter compounds which are solid at room temperature and have Zerevitinov-active hydrogen atoms, a particular feature of which is that visually clear and/or homogeneous products are obtained even in the absence of solvents.

    摘要翻译： 本发明涉及一种制备聚醚多元醇的方法，该方法是通过在环氧化物（环氧化物）上加成在室温下为固体的起始化合物进行碱催化加成，并具有齐维伏诺 - 活性氢原子，其特征在于目视清楚和/ 或即使在没有溶剂的情况下也可获得均匀的产物。

    HIGHLY PURE POLOXAMERS AND PURIFICATION METHOD THEREOF
    96.
    发明申请
    HIGHLY PURE POLOXAMERS AND PURIFICATION METHOD THEREOF 审中-公开
    高纯度POLOXAMERS及其纯化方法

    公开(公告)号：US20130274421A1

    公开(公告)日：2013-10-17

    申请号：US13976228

    申请日：2011-12-22

    申请人： Bong Oh Kim ,  Min Hyo Seo

    发明人： Bong Oh Kim ,  Min Hyo Seo

    IPC分类号： C08G65/30

    CPC分类号： C08G65/30 ,  B01D15/02 ,  C08G2650/58

    摘要： Disclosed are a method for purifying poloxamers, comprising dissolving poloxamers in an organic solvent to prepare a polymer solution, and removing organometals or water from the polymer solution by at least one physical method selected from mixing of activated carbon with the polymer solution and centrifugation of the polymer solution, and poloxamers purified by the method.

    摘要翻译： 公开了一种用于纯化泊洛沙姆的方法，包括将泊洛沙姆溶解在有机溶剂中以制备聚合物溶液，并通过至少一种选自活性炭与聚合物溶液的混合的物理方法从聚合物溶液中除去有机金属或水，并将 聚合物溶液和通过该方法纯化的泊洛沙姆。

    PROCESS FOR PURIFICATION OF WATER SOLUBLE POLYMERS
    97.
    发明申请
    PROCESS FOR PURIFICATION OF WATER SOLUBLE POLYMERS 有权
    水溶性聚合物的纯化方法

    公开(公告)号：US20100323452A1

    公开(公告)日：2010-12-23

    申请号：US12528304

    申请日：2007-02-22

    申请人： James F. Monthony ,  LI Yang ,  Kurt E. Kershaw ,  Christopher D. Winslow ,  John G. Riley

    发明人： James F. Monthony ,  LI Yang ,  Kurt E. Kershaw ,  Christopher D. Winslow ,  John G. Riley

    IPC分类号： C08G65/30 ,  G01N33/44 ,  C08G65/04

    CPC分类号： C08F8/44 ,  B01D15/361 ,  B01J47/12 ,  C08F6/003 ,  C08G65/30 ,  C08G65/3326 ,  C08G65/3346 ,  G01N30/02 ,  Y10T436/255

    摘要： A process for purification of water soluble polymers is provided. A polymer of interest can be separated from a mixture of polymers, provided the polymer of interest differs from other polymers in the mixture in the number of reactive terminal groups. The process involves derivatizing polymers at the reactive terminal groups with a derivatizing molecule, bearing either (i) two or three cationic or anionic ionizable groups, and a group capable of covalent bonding to the reactive terminal groups or (ii) three or four ionizable groups, at least one of which is capable of covalent bonding to the reactive terminal groups; followed by ion exchange. The process allows removal of PEG from MPEG, and can be used for polymers having an average size greater than 9,000 Da Derivatization may be reversible in order to allow re-use of recovered contaminant polymers.

    摘要翻译： 提供了一种纯化水溶性聚合物的方法。 感兴趣的聚合物可以从聚合物的混合物中分离出来，只要目的聚合物与反应性末端基团数目的混合物中的其它聚合物不同。 该方法包括用衍生化分子衍生化反应性末端基团的聚合物，该衍生化分子带有（i）两个或三个阳离子或阴离子可离子基团，以及能够与反应性末端基团共价连接的基团，或（ii）三个或四个可离子化基团 ，其中至少一个能够与反应性末端基团共价结合; 然后进行离子交换。 该方法允许从MPEG去除PEG，并且可以用于平均尺寸大于9,000Da的聚合物。衍生化可以是可逆的，以便允许再利用回收的污染物聚合物。

    Production of polyether alcohols by usig dmc catalysis
    98.
    发明申请
    Production of polyether alcohols by usig dmc catalysis 审中-公开
    通过使用催化剂生产聚醚醇

    公开(公告)号：US20060167209A1

    公开(公告)日：2006-07-27

    申请号：US10559073

    申请日：2004-06-03

    申请人： Thomas Ostrowski ,  Raimund Ruppel ,  Eva Baun ,  Kathrin Harre

    发明人： Thomas Ostrowski ,  Raimund Ruppel ,  Eva Baun ,  Kathrin Harre

    IPC分类号： C08G18/32 ,  C08G65/30 ,  B32B27/40

    CPC分类号： C08G65/30 ,  C08G65/2663

    摘要： The present invention relates to polyetherols are prepared by a process comprising the reaction of at least one alkylene oxide with at least one initiator compound in the presence of at least one double metal cyanide compound to give a polyetherol and the treatment of the resulting polyetherol with steam or with an inert gas and steam, and the polyetherols obtainable by such a process as well as the use thereof for the synthesis of polyurethanes.

    摘要翻译： 本发明涉及通过包括至少一种烯化氧与至少一种引发剂化合物在至少一种双金属氰化物化合物的存在下反应以产生聚乙烯醇并用蒸汽处理得到的聚乙烯醇的方法制备的聚醚 或惰性气体和蒸汽，以及可通过这种方法获得的聚醚，以及其用于合成聚氨酯的用途。

    Purified polyoxypropylene/polyoxyethylene copolymers and method of preparing the same
    99.
    发明申请
    Purified polyoxypropylene/polyoxyethylene copolymers and method of preparing the same 审中-公开
    纯化聚氧丙烯/聚氧乙烯共聚物及其制备方法

    公开(公告)号：US20050095221A1

    公开(公告)日：2005-05-05

    申请号：US10934169

    申请日：2004-09-03

    申请人： Mannarsamy Balasubramanian ,  R. Emanuele

    发明人： Mannarsamy Balasubramanian ,  R. Emanuele

    IPC分类号： A61K31/765 ,  A61K31/785 ,  C08G20060101 ,  C08G59/14 ,  C08G65/26 ,  C08G65/28 ,  C08G65/30

    CPC分类号： C08G65/30 ,  C08G65/2624

    摘要： The present invention comprises novel preparations of polyoxypropylene/polyoxyethylene octablock copolymers which retain the growth-promoting and immunity-enhancing activity of commercially-available preparations, but are free from the undesirable effects which are inherent in the prior art preparations. Because the polyoxypropylene/polyoxyethylene copolymers which comprise the present invention have a more homogenous population of molecules with fewer low molecular weight species than prior art preparations, the biological activity of the copolymer is better defined and more predictable. Moreover, the polyoxypropylene/polyoxyethylene copolymer of the present invention substantially reduces any risk to human health through the consumption of food animals since the copolymer hereof is not absorbed into the animal's edible tissue. Methods for preparation of the polyoxypropylene/polyoxyethylene copolymer of the present invention are also provided.

    摘要翻译： 本发明包括保留生物促进和免疫增强活性的聚氧丙烯/聚氧乙烯八嵌段共聚物的新型制剂，但是没有现有技术制剂固有的不良作用。 由于包含本发明的聚氧丙烯/聚氧乙烯共聚物具有比现有技术制剂更少的低分子量物质的更均匀的分子群，所以共聚物的生物活性被更好地定义并且更可预测。 此外，本发明的聚氧丙烯/聚氧乙烯共聚物通过食用动物的大量降低对人类健康的任何风险，因为其共聚物不被吸收到动物的食用组织中。 还提供了制备本发明聚氧丙烯/聚氧乙烯共聚物的方法。

    Perfluoropolyethers
    100.
    发明申请
    Perfluoropolyethers 失效
    全氟聚醚

    公开(公告)号：US20050074686A1

    公开(公告)日：2005-04-07

    申请号：US10953768

    申请日：2004-09-30

    申请人： Mattia Bassi ,  Pier Guarda

    发明人： Mattia Bassi ,  Pier Guarda

    IPC分类号： G03F7/20 ,  C07C43/12 ,  C08G65/00 ,  C08G65/04 ,  C08G65/30 ,  C08G65/32 ,  G02B1/04 ,  G02B5/00 ,  G03C3/00 ,  G03F7/004 ,  H01L21/027

    CPC分类号： C08G65/32 ,  C08G65/007 ,  C08G65/30 ,  G02B1/04 ,  G03F7/2041 ,  C08L71/00

    摘要： Use in optical systems as liquids to transmit light at wave lengths lower than 250 nm, in particular at 157 nm, of perfluoropolyethers having the following formula: X1—O(CF2O)n(CF2CF2O)m(CF2CF2CF2O)p (CF2CF2CF2CF2O)q—X2  (I) wherein: the repeating units —CF2O—, —CF2CF2O—, —CF2CF2CF2O—, —CF2CF2CF2CF2O— are statistically distributed along the chain; —X1 and —X2 are perfluoroalkyl chain end groups equal to or different from each other, having formula —(CF2)zCF3 wherein z is 0 or an integer from 1 to 3; n, m, p, q are 0 or integers comprised between 1 and 100, with the proviso that: at least one among n, m, p and q is different from zero; the ratio between the oxygen atoms and the carbon atoms (O/C) is higher than 0.33; wherein the chlorine atoms, determined by 19F-NMR are substantially absent.

    摘要翻译： 在光学系统中作为液体使用波长低于250nm（特别是157nm）的具有下式的全氟聚醚的光：X1-O（CF2O）n（CF2CF2O）m（CF2CF2CF2O）p（CF2CF2CF2CF2O）q- X2（I）其中：重复单元-CF2O-，-CF2CF2O-，-CF2CF2CF2O-，-CF2CF2CF2CF2O-沿着链统计分布; -X1和-X2是彼此等于或不同的全氟烷基链端基，其具有式 - （CF 2）z CF 3，其中z为0或1至3的整数; n，m，p，q是0或包含在1和100之间的整数，条件是：n，m，p和q中的至少一个不同于零; 氧原子和碳原子之间的比例（O / C）高于0.33; 其中通过19 F-NMR确定的氯原子基本上不存在。