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    Blue luminescing glasses
    121.
    发明授权
    Blue luminescing glasses 失效
    蓝色发光眼镜

    公开(公告)号：US4946622A

    公开(公告)日：1990-08-07

    申请号：US307231

    申请日：1989-02-06

    申请人： Akos Kiss ,  Peter Kleinschmit ,  Werner Volker ,  Gunter Halbritter

    发明人： Akos Kiss ,  Peter Kleinschmit ,  Werner Volker ,  Gunter Halbritter

    IPC分类号： C03C3/07 ,  C03C3/072 ,  C03C3/102 ,  C03C3/105 ,  C03C3/108 ,  C03C4/12 ,  C03C8/10 ,  C09K11/08

    CPC分类号： C03C3/108 ,  C03C3/072 ,  C03C3/102 ,  C03C8/10 ,  C09K11/0805

    摘要： There are described blue luminescent glasses having the following compositions(a) 0 to 90 mole % alkali metal oxide (sodium oxide, potassium oxide, lithium oxide), individually or several together, 0 to 90 mole % alkaline earth metal oxide (magnesium oxide, calcium oxide, strontium oxide, barium oxide), individually or several together, with the proviso that the magnesium oxide and/or calcium oxide can only be present in an amount of up to 25 mole % and at least 2 mole % of alkali metal oxide and/or alkaline earth metal oxide must be present(b)7 to 95 mole % silica0 to 70 mole % boron oxide (B.sub.2 O.sub.3)0 to 85 mole % aluminum oxide(c) 0.01 to 40 mole % lead oxide (PbO).

    摘要翻译： 描述了具有以下组成的蓝色发光玻璃：（a）0至90摩尔％的碱金属氧化物（氧化钠，氧化钾，氧化锂），单独或几个，0至90摩尔％的碱土金属氧化物（氧化镁， 氧化钙，氧化锶，氧化钡），条件是氧化镁和/或氧化钙的存在量最多只能为25摩尔％，至少2摩尔％的碱金属氧化物 和/或碱土金属氧化物必须存在（b）7〜95摩尔％二氧化硅0〜70摩尔％氧化硼（B 2 O 3）0〜85摩尔％氧化铝（c）0.01〜40摩尔％氧化铅（PbO）。

    Mixtures of sulfurous triazine compounds
    123.
    发明授权
    Mixtures of sulfurous triazine compounds 失效
    亚硫酸三嗪化合物的混合物

    公开(公告)号：US4837322A

    公开(公告)日：1989-06-06

    申请号：US89895

    申请日：1987-08-27

    申请人： Ulrich Deschler ,  Georg Hellwig ,  Rudolf Michel ,  Peter Kleinschmit ,  Siegfried Wolff

    发明人： Ulrich Deschler ,  Georg Hellwig ,  Rudolf Michel ,  Peter Kleinschmit ,  Siegfried Wolff

    IPC分类号： C07D251/52 ,  C08K5/34 ,  C08K5/378 ,  C08L21/00

    CPC分类号： C07D251/52 ,  C08K5/378

    摘要： Mixtures of sulfurous triazine compounds and methods of preparing these compounds with the general formula ##STR1## in which R.sup.1, R.sup.2 =H,R.sup.2 =benzyl,R.sup.2, R.sup.3, R.sup.4 =C.sub.1 -C.sub.8 -alkyl, allyl, C.sub.3 -C.sub.8 cycloalkyl, the latter unsubstituted or substituted with 1-3 methyl groups, 2-hydroxyethyl, 3-hydroxypropyl, 2-hydroxypropyl orR.sup.3 and R.sup.4 (together): C.sub.4 -C.sub.6 -alkylene, --(CH.sub.2 --CHX).sub.2 Y withX=H, CH.sub.3, Y=O,S,S.sub.a : Polysulfide chain with 2-10 S atoms (i.e. 2.ltoreq.a.ltoreq.10), in which the individual polysulfides are present in such concentrations that the statistical average value of "a" is a whole or fractional numerical value in the range from 2 to 5., characterized in that a triazine compound of the general formula ##STR2## in which R.sup.1, R.sup.2, R.sup.3, R.sup.4 have the meanings indicated above is reacted with an ammonium polysulfide or alkali polysulfide and dissolved in a protic polar solvent, especially water, at a temperature of 80.degree. to 140.degree. C.

    摘要翻译： 亚硫基三嗪化合物的混合物和制备这些具有通式Ⅰ的化合物的方法，其中R1，R2 = H，R2 =苄基，R2，R3，R4 = C1-C8-烷基，烯丙基，C3-C8环烷基， 未取代或被1-3个甲基取代的后者，2-羟基乙基，3-羟丙基，2-羟基丙基或R 3和R 4（一起）：C 4 -C 6亚烷基， - （CH 2 -CHX）2 Y，X = CH 3，Y = O，S，Sa：具有2-10个S原子的多硫链（即2

    Silicate-bound zeolite granulates, process for their production and use
    126.
    发明授权
    Silicate-bound zeolite granulates, process for their production and use 失效
    硅酸盐沸石颗粒，其生产和使用过程

    公开(公告)号：US4714690A

    公开(公告)日：1987-12-22

    申请号：US791032

    申请日：1985-10-24

    申请人： Hans Strack ,  Peter Kleinschmit

    发明人： Hans Strack ,  Peter Kleinschmit

    IPC分类号： C01B39/00 ,  B01J20/18 ,  C01B39/14 ,  C01B39/22 ,  C01B39/24 ,  C01B39/26 ,  C01B39/36 ,  B01J29/06

    CPC分类号： B01J20/183

    摘要： Silicate-bound zeolite granulates are disclosed wherein the zeolite contains a cation which is not present in the binder, and where the zeolite can also contain the binder cation. The granulates are produced by placing powdered zeolite in a mixer, adding sodium silicate solution, mixing until zeolite granulates with a grain size of at least 0.1 mm are obtained, optionally after-rolling the zeolite granulates. The moist zeolite granulates can be initially dried at temperatures of 20 degrees to 39 degrees C., where the carbon dioxide content of the drying air is adjusted to less than 200 ppm. Thereafter, a second drying step can be carried out at temperatures of 40 degrees to 120 degrees C. as well as a third drying stage at 121 degrees to 200 degrees C. under otherwise identical conditions. The products may be activated at temperatures of 600 degrees C. maximum. The zeolite granulates thus obtained are then treated with a first aqueous metal salt solution, washed and then optionally treated with a second aqueous metal salt solution, washed and dried again at 40 degrees to 200 degrees C., preferably 100 degrees to 120 degrees C., and then optionally calcined to 300 degrees to 650 degrees C.

    摘要翻译： 公开了硅酸盐结合的沸石颗粒，其中沸石含有不存在于粘合剂中的阳离子，并且其中沸石还可以含有粘合剂阳离子。 通过将粉末状沸石置于混合器中，加入硅酸钠溶液，混合直到得到粒度至少为0.1mm的沸石颗粒，任选地后滚沸石颗粒来制备颗粒。 湿沸石颗粒可以首先在20摄氏度至39摄氏度的温度下干燥，其中干燥空气的二氧化碳含量调节至小于200ppm。 此后，在其它相同的条件下，第二干燥步骤可以在温度为40摄氏度至120摄氏度的温度下进行，第二干燥步骤也可在121度至200摄氏度的第三干燥阶段进行。 产品可能在最高600摄氏度的温度下被激活。 然后将由此获得的沸石颗粒用第一金属盐水溶液处理，洗涤，然后任选地用第二种金属盐溶液处理，再次在40摄氏度至200摄氏度，优选100度至120摄氏度下洗涤和干燥。 ，然后任意煅烧至300度至650度。

    Phenylene group-containing organosilanes and processes for the preparation thereof
    127.
    发明授权
    Phenylene group-containing organosilanes and processes for the preparation thereof 失效
    含亚苯基的有机硅烷及其制备方法

    公开(公告)号：US4647682A

    公开(公告)日：1987-03-03

    申请号：US865486

    申请日：1986-05-21

    申请人： Peter Panster ,  Peter Kleinschmit

    发明人： Peter Panster ,  Peter Kleinschmit

    IPC分类号： C07F7/14 ,  C07F7/12 ,  C07F7/18 ,  C08G77/52 ,  C07F7/08

    CPC分类号： C07F7/12 ,  C07F7/1836 ,  C08G77/52

    摘要： Phenylene group-containing organosilanes represented by the formula: ##STR1## where in each case all three possible isomers in relation to the position of the R.sub.3 Si-R.sup.1 substituents can be present concurrently, R.sup.1 represents --CH.sub.2 --CH.sub.2 -- or CH.sub.3 CH>, and R.sup.2 represents chloride or an alkoxy group. Processes for the production of the organosilanes and the use of these substances for the production of the corresponding organopolysiloxanes are also disclosed.

    摘要翻译： 由下式表示的含亚苯基的有机硅烷：（1）其中在各种情况下，与R 3 Si-R 1取代基的位置相关的所有三种可能的异构体可以同时存在，R 1表示-CH 2 -CH 2 - 或CH 3 CH 3， ，R2表示氯原子或烷氧基。 还公开了生产有机硅烷的方法和这些物质用于生产相应的有机聚硅氧烷的用途。

    Method for preparation of 3-chloropropyl-trichlorosilane
    129.
    发明授权
    Method for preparation of 3-chloropropyl-trichlorosilane 失效
    3-氯丙基三氯硅烷的制备方法

    公开(公告)号：US4584395A

    公开(公告)日：1986-04-22

    申请号：US699696

    申请日：1985-02-08

    申请人： Peter Panster ,  Rudolf Michel ,  Wolfgang Buder ,  Peter Kleinschmit

    发明人： Peter Panster ,  Rudolf Michel ,  Wolfgang Buder ,  Peter Kleinschmit

    IPC分类号： C07F7/12 ,  B01J31/00 ,  C07B61/00 ,  C07F7/14 ,  C07F7/08

    CPC分类号： C07F7/14

    摘要： A method for the preparation of 3-chloropropyltrichlorosilane is carried out by conversion of trichlorosilane with allylchloride in the presence of a platinum containing polymeric organosiloxane-ammonium compound containing units represented by the structural formula: ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 represent a group of the formula:R.sup.5 --SiO.sub.3/2 (2)wherein R.sup.5 denotes an alkylene group and the free valences of the oxygen atoms are saturated by silicon atoms of further groups of the formula (2), optionally with incorporation of crosslinking agents, R.sup.4 has the same meaning as R.sup.1, R.sup.2 and R.sup.3 or hydrogen, alkyl, cycloalkyl or benzyl, Y.sup.x- represents PtX.sub.4.sup.2- or PtX.sub.6.sup.2- (X is Cl or Br) and can also be an inorganic 1 to 3 functional anion of a protonic acid which yields stable salts with amine bases or the hydroxy group, and x is a number from 1 to 3.

    摘要翻译： 制备3-氯丙基三氯硅烷的方法是通过在含有由下列结构式表示的含有单元的含铂聚合物有机硅氧烷 - 铵化合物存在下，将三氯硅烷与烯丙基氯反应进行的：其中R1，R2和R3 代表式为R5-SiO3 / 2（2）的基团，其中R5表示亚烷基并且氧原子的游离价被另外的式（2）的基团的硅原子饱和，任选地加入交联剂 ，R4与R1，R2和R3或氢，烷基，环烷基或苄基具有相同的含义，Yx-表示PtX42-或PtX62-（X是Cl或Br），也可以是质子的无机1至3官能阴离子 其与胺碱或羟基产生稳定的盐，x为1至3的数。

    Lead activated luminescent material and process for its production
    130.
    发明授权
    Lead activated luminescent material and process for its production 失效
    铅活化发光材料及其生产工艺

    公开(公告)号：US4578212A

    公开(公告)日：1986-03-25

    申请号：US719954

    申请日：1985-04-04

    申请人： Akos Kiss ,  Peter Kleinschmit ,  Werner Volker ,  Gunter Halbritter

    发明人： Akos Kiss ,  Peter Kleinschmit ,  Werner Volker ,  Gunter Halbritter

    IPC分类号： C09K11/08 ,  C09K11/67 ,  C09K11/66

    CPC分类号： C09K11/678

    摘要： There are described luminescent materials activated with lead upon excitation with long wave and short wave ultraviolet rays emit in the blue-green region, have long afterglow times, can be prepared from components which do not have high purity, are not susceptible to pulverizing, and are stable to the customary ceramic glazes. They consist of (or consist essentially of):10 to 89.9 mole % zirconium oxide (ZrO.sub.2)5 to 85 mole % boron oxide (B.sub.2 O.sub.3)5 to 85 mole % silicon dioxide (SiO.sub.2)0.1 to 20 mole % lead oxide (PbO)0 to 15 mole % sodium oxide (Na.sub.2 O)0 to 15 mole % potassium oxide (K.sub.2 O) and0 to 5 mole % aluminum oxide (Al.sub.2 O.sub.3).

    摘要翻译： 描述了在长时间的波长和短波紫外线激发时用铅激发的发光材料在蓝绿色区域发射，具有长的余辉时间，可以由不具有高纯度，不易于粉碎的组分制备，以及 对于习惯的陶瓷釉是稳定的。 它们由（或基本上由...组成）：10至89.9摩尔％氧化锆（ZrO 2）5至85摩尔％氧化硼（B 2 O 3）5至85摩尔％二氧化硅（SiO 2）0.1至20摩尔％氧化铅（PbO） 0〜15摩尔％的氧化钠（Na 2 O）0〜15摩尔％的氧化钾（K 2 O）和0〜5摩尔％的氧化铝（Al 2 O 3）。