摘要:
This invention provides a process for producing a 5-hydroxy-3-oxopentanoic acid, a useful pharmaceutical intermediate, easily from a readily available, inexpensive starting material without using any extraordinary production equipment such as a very-low-temperature reactor. Thus, this invention provides a process for producing a 5-hydroxy-3-oxopentanoic acid which comprises permitting a lithium amide to act upon a mixture of an acetic acid ester and a 3-hydroxypropionic acid derivative at not below −20° C. Further, this invention also provides a process for producing a 5-hydroxy-3-oxopentanoic acid which comprises treating a mixture of an acetic acid ester and a 3-hydroxypropionic acid derivative with a Grignard reagent to prepare a mixture of a compound and an acetic acid ester of the above formula (I), and permitting a lithium amide to act upon the mixture at a temperature not below −20° C.
摘要:
The invention provides a web transfer belt, having good paper releasability, that can be produced with ease and at a low cost without increasing either its hardness or its weight, and a production process therefor. In one embodiment, the web transfer belt includes a high-molecular weight elastic member formed using a resin material mixed with microcapsules (alternatively, closed bubbles or closed bubbles created by a foaming agent), and having a web-receiving face for receiving a web P thereon to transfer, at whose web-receiving face there are provided a multitude of recesses having cut-openings of the microcapsules, such that a water film W easy to be formed between the web-receiving face and the web P can be broken by a large number of recesses.
摘要:
The present invention has its objects to provide a method for reducing &agr;-aminoketone derivatives under mild conditions with high stereoselectivity. This invention is a method for reducing &agr;-aminoketone which comprises reacting an a-aminoketone derivative of general formula (1) with a compound prepared from an organoaluminum compound of general formula (4), a sulfonic acid derivative of general formula (5), and an alcohol compound of general formula (6) to give an &agr;-aminoalcohol derivative of general formula (7)
摘要:
A display control apparatus having a plurality of different display modes for displaying a plurality of types of image signals corresponding to different resolutions and dot clocks, includes a discrimination circuit for displaying the display mode of the currently displayed image signal, and a selection circuit for selecting on-screen display data to be displayed on the basis of the display mode discriminated by the discrimination circuit. In addition, an input circuit inputs the on-screen display data selected by the selection circuit in place of the currently displayed image data, and an output circuit outputs the on-screen display data input by the input circuit in the display mode of the image signal.
摘要:
The present invention provides a process for reducing carbonyl compounds to hydroxy compounds, in particular stereoselectively reducing .alpha.-aminohaloketone derivatives, under mild conditions in an easy and simple manner, which comprises reacting a carbonyl compound of the general formula (1) with an organoaluminum compound of the general formula (4) to provide the corresponding alcohol compound of the general formula (5). ##STR1##
摘要:
A die for press-molding glass optical elements which can press-mold glass optical elements having high melting points and various shapes repeatedly, which includes a base material having high strength on which a cutting layer having heat resistance and free cutting machinability is formed. After cutting the cutting layer into the desired shape with high accuracy, the die is coated with a surface protective film.
摘要:
This invention relates to a gas refining system wherein a high-temperature and high-pressure reducing gas is introduced into a fixed-bed desulfurizer packed with an adsorbent by which sulfur compounds contained in the high-temperature and high-pressure reducing gas are adsorbed and removed in the form of a sulfide, and the adsorbent having the sulfide adsorbed thereon is regenerated by roasting it with a regenerating gas containing oxygen, characterized in that the gas refining system is equipped with oxygen concentration control means for controlling the oxygen concentration in the regenerating gas introduced into the desulfurizer so as to keep the internal temperature of the desulfurizer during the regeneration reaction within the allowable temperature range of the adsorbent. This invention includes an embodiment in which the exhaust gas obtained after the regeneration reaction gas is brought into contact with a calcium compound-containing slurry to recover gypsum is recycled to the desulfurizer for use as the regenerating gas for the adsorbent. Thus, the adverse effect of the heat of regeneration reaction on the adsorbent used in the fixed-bed desulfurizer can be avoided positively and easily.
摘要:
A 3,4-epoxybutyrate of the formula: ##STR1## wherein R.sup.1 is an alkyl or aralkyl group is efficiently prepared by a process comprising steps of:(a) reacting 3,4-dihydroxybutyronitrile of the formula: ##STR2## with a sulfonyl chloride of the formula: R.sup.2 --SO.sub.2 --Cl wherein R.sup.2 is an alkyl group or a phenyl group which may be substituted in the presence of a base to obtain a compound of the formula: ##STR3## (b) reacting the compound prepared in the step (a) with an alcohol of the formula: R.sup.1 --OH in the presence of an acid to obtain a compound of the formula: ##STR4## and (c) reacting the compound prepared in the step (b) with a base to obtain the 3,4-epoxybutyrate.
摘要:
A hydrogen-absorbing alloy electrode comprising a hydrogen-absorbing alloy represented by a formula ANi.sub.a Co.sub.b Mn.sub.c or ANi.sub.a Co.sub.b Mn.sub.c X.sub.d, A representing a mixture of rare earth elements including La and X representing at least one element selected from a group of Fe, Cu, Mo, W, B, Al, Si and Sn, wherein 2.5.ltoreq.a.ltoreq.3.5, 0.4.ltoreq.b.ltoreq.1.5, 0.2.ltoreq.c.ltoreq.1.0, and 3.85.ltoreq.a+b+c.ltoreq.4.78 in the case of ANi.sub.a Co.sub.b Mn.sub.c or 2.5.ltoreq.a.ltoreq.3.5, 0.4.ltoreq.b.ltoreq.1.5, 0.2.ltoreq.c.ltoreq.1.0, 0
摘要翻译:一种吸氢合金电极,其包含由式ANiaCobMnc或ANiaCobMncXd表示的吸氢合金,A表示包含La和X的稀土元素的混合物,所述稀土元素表示选自Fe,Cu,Mo,W, B,Al,Si和Sn,其中2.5≤a≤3.5,0.4≤b= 1.5,0.2,c = 1.0,和3.85 a + b + c < 在ANiaCobMnc或2.5 = a <3.5,0.4 = b = 1.5,0.2 = c <1.0,0
摘要:
An integration-proportional controller in a servo-control system comprises in one aspect, an integrator for integrating a deviation of an input speed reference signal from a feedback signal fed back from an object to be controlled, and a proportional amplifier connected with the integrator for amplifying the feedback signal, the integrator including a clamping function in which an output value therefrom and an initial value for the next successive integration are changed, when the output value as a result of integration of the deviation is out of a predetermined proper output region, to the nearest boundary of the predetermined region value. In another aspaect, a saturable integrator is provided for integrating a deviation of an input speed reference signal from a feedback signal fed back from an object to be controlled, a proportional amplifier is connected with the saturable integrator for amplifying the feedback signal, and a deviation clamping device is connected with the saturable integrator for limiting the upper and lower values of the deviation.