Processes for the preparation of 5-hydroxy-3-oxopentanoic acid derivatives
    121.
    发明授权
    Processes for the preparation of 5-hydroxy-3-oxopentanoic acid derivatives 有权
    5-羟基-3-氧代戊酸衍生物的制备方法

    公开(公告)号:US06340767B1

    公开(公告)日:2002-01-22

    申请号:US09762215

    申请日:2001-04-05

    IPC分类号: C07C5100

    摘要: This invention provides a process for producing a 5-hydroxy-3-oxopentanoic acid, a useful pharmaceutical intermediate, easily from a readily available, inexpensive starting material without using any extraordinary production equipment such as a very-low-temperature reactor. Thus, this invention provides a process for producing a 5-hydroxy-3-oxopentanoic acid which comprises permitting a lithium amide to act upon a mixture of an acetic acid ester and a 3-hydroxypropionic acid derivative at not below −20° C. Further, this invention also provides a process for producing a 5-hydroxy-3-oxopentanoic acid which comprises treating a mixture of an acetic acid ester and a 3-hydroxypropionic acid derivative with a Grignard reagent to prepare a mixture of a compound and an acetic acid ester of the above formula (I), and permitting a lithium amide to act upon the mixture at a temperature not below −20° C.

    摘要翻译: 本发明提供一种生产5-羟基-3-氧代戊酸的方法,该方法是一种有用的药物中间体,容易从现成的廉价起始原料中生产,而不使用任何非常低的生产设备如极低温反应器。因此, 本发明提供了一种生产5-羟基-3-氧代戊酸的方法,其包括允许氨化锂在不低于-20℃下作用于乙酸酯和3-羟基丙酸衍生物的混合物。此外,本发明还 提供了一种生产5-羟基-3-氧代戊酸的方法,其包括用格氏试剂处理乙酸酯和3-羟基丙酸衍生物的混合物,以制备上式的化合物和乙酸酯的混合物 (I)化合物,并允许在不低于-20℃的温度下使氨基化锂作用于混合物。

    Web transfer belt and production process for the same
    122.
    发明授权
    Web transfer belt and production process for the same 有权
    纸幅转印带和生产过程相同

    公开(公告)号:US06331231B1

    公开(公告)日:2001-12-18

    申请号:US09652092

    申请日:2000-08-31

    申请人: Kenji Inoue

    发明人: Kenji Inoue

    IPC分类号: D21F200

    摘要: The invention provides a web transfer belt, having good paper releasability, that can be produced with ease and at a low cost without increasing either its hardness or its weight, and a production process therefor. In one embodiment, the web transfer belt includes a high-molecular weight elastic member formed using a resin material mixed with microcapsules (alternatively, closed bubbles or closed bubbles created by a foaming agent), and having a web-receiving face for receiving a web P thereon to transfer, at whose web-receiving face there are provided a multitude of recesses having cut-openings of the microcapsules, such that a water film W easy to be formed between the web-receiving face and the web P can be broken by a large number of recesses.

    摘要翻译: 本发明提供一种纸张转印带,其具有良好的纸张脱模性,可以容易且低成本地生产,而不增加其硬度或重量,以及其生产工艺。 在一个实施方案中,幅材转印带包括使用与微胶囊混合的树脂材料形成的高分子量弹性构件(或者,由发泡剂产生的闭合气泡或闭合气泡),并且具有用于接收网的纸幅接收面 在其上的纸幅接收面上设置有多个具有微胶囊切口的凹部,使得易于在纸幅接收面和纸幅P之间形成的水膜W可以被打破, 大量的凹槽。

    Process for reducing &agr;-amino ketones
    123.
    发明授权
    Process for reducing &agr;-amino ketones 有权
    降低α-氨基酮的方法

    公开(公告)号:US06255522B1

    公开(公告)日:2001-07-03

    申请号:US09230887

    申请日:1999-09-29

    IPC分类号: C07C27114

    摘要: The present invention has its objects to provide a method for reducing &agr;-aminoketone derivatives under mild conditions with high stereoselectivity. This invention is a method for reducing &agr;-aminoketone which comprises reacting an a-aminoketone derivative of general formula (1) with a compound prepared from an organoaluminum compound of general formula (4), a sulfonic acid derivative of general formula (5), and an alcohol compound of general formula (6) to give an &agr;-aminoalcohol derivative of general formula (7)

    摘要翻译: 本发明的目的是提供一种在高立体选择性的温和条件下还原α-氨基酮衍生物的方法。 本发明是一种还原α-氨基酮的方法,该方法包括使通式(1)的α-氨基酮衍生物与通式(4)的有机铝化合物,通式(5)的磺酸衍生物, 和通式(6)的醇化合物,得到通式(7)的α-氨基醇衍生物,

    Gas refining system
    127.
    发明授权
    Gas refining system 失效
    气体精炼系统

    公开(公告)号:US5980846A

    公开(公告)日:1999-11-09

    申请号:US74033

    申请日:1998-05-06

    CPC分类号: C10K1/26

    摘要: This invention relates to a gas refining system wherein a high-temperature and high-pressure reducing gas is introduced into a fixed-bed desulfurizer packed with an adsorbent by which sulfur compounds contained in the high-temperature and high-pressure reducing gas are adsorbed and removed in the form of a sulfide, and the adsorbent having the sulfide adsorbed thereon is regenerated by roasting it with a regenerating gas containing oxygen, characterized in that the gas refining system is equipped with oxygen concentration control means for controlling the oxygen concentration in the regenerating gas introduced into the desulfurizer so as to keep the internal temperature of the desulfurizer during the regeneration reaction within the allowable temperature range of the adsorbent. This invention includes an embodiment in which the exhaust gas obtained after the regeneration reaction gas is brought into contact with a calcium compound-containing slurry to recover gypsum is recycled to the desulfurizer for use as the regenerating gas for the adsorbent. Thus, the adverse effect of the heat of regeneration reaction on the adsorbent used in the fixed-bed desulfurizer can be avoided positively and easily.

    摘要翻译: 本发明涉及一种气体精炼系统,其中将高温高压还原气体引入填充有吸附剂的固定床脱硫器中,通过该吸附剂吸附高温高压还原气体中所含的硫化合物, 以硫化物的形式除去,吸附有硫化物的吸附剂通过用含氧的再生气体焙烧而再生,其特征在于,气体精炼系统配备有氧浓度控制装置,用于控制再生中的氧浓度 将气体引入脱硫器中,以便在再生反应期间将脱硫剂的内部温度保持在吸附剂的允许温度范围内。 本发明包括将再生反应气体与含钙化合物的浆料接触以回收石膏后获得的废气再循环至脱硫器,用作吸附剂的再生气体。 因此,可以积极且容易地避免再生反应的热量对固定床脱硫剂中使用的吸附剂的不良影响。

    Integration proportional controller in servo-control system
    130.
    发明授权
    Integration proportional controller in servo-control system 失效
    伺服控制系统中积分比例控制器

    公开(公告)号:US4999557A

    公开(公告)日:1991-03-12

    申请号:US345443

    申请日:1989-04-28

    申请人: Kenji Inoue

    发明人: Kenji Inoue

    IPC分类号: G05B11/42 H02P23/00

    CPC分类号: G05B11/42 H02P23/16

    摘要: An integration-proportional controller in a servo-control system comprises in one aspect, an integrator for integrating a deviation of an input speed reference signal from a feedback signal fed back from an object to be controlled, and a proportional amplifier connected with the integrator for amplifying the feedback signal, the integrator including a clamping function in which an output value therefrom and an initial value for the next successive integration are changed, when the output value as a result of integration of the deviation is out of a predetermined proper output region, to the nearest boundary of the predetermined region value. In another aspaect, a saturable integrator is provided for integrating a deviation of an input speed reference signal from a feedback signal fed back from an object to be controlled, a proportional amplifier is connected with the saturable integrator for amplifying the feedback signal, and a deviation clamping device is connected with the saturable integrator for limiting the upper and lower values of the deviation.

    摘要翻译: 伺服控制系统中的积分比例控制器在一个方面包括一个积分器,用于对来自被控制物体反馈的反馈信号的输入速度参考信号的偏差进行积分,以及与积分器连接的比例放大器, 放大反馈信号时,积分器包括一个钳位功能,当作为偏差积分的结果的输出值在预定的正确输出区域之外时,其中其输出值和下一个连续积分的初始值改变, 到预定区域值的最近边界。 在另一个aspaect中,提供了可饱和积分器,用于将输入速度参考信号与从被控制物体反馈的反馈信号的偏差积分,比例放​​大器与可饱和积分器连接,用于放大反馈信号,偏差 夹紧装置与可饱和积分器连接,用于限制偏差的上限和下限值。