Polybasic acid amides and their use as digestively hydrolyzable oil
substitutes
    13.
    发明授权
    Polybasic acid amides and their use as digestively hydrolyzable oil substitutes 失效
    多元酸酰胺及其作为消化水解油替代品的用途

    公开(公告)号:US5194286A

    公开(公告)日:1993-03-16

    申请号:US879540

    申请日:1992-05-04

    IPC分类号: A23D9/007 A23L33/20

    CPC分类号: A23D9/007 A23L33/20

    摘要: This invention relates to digestively hydrolyzable low calorie edible oil substitutes. These compounds have the organoleptic properties of normal triglycerides fats, but are lower in available calories. Specifically, the invention is directed to a composition of matter. The compositions are in one embodiment amides of dimer acids or trimer acids made from glycinates. The compounds are in part directed to amides based on the amino acid esters of the amino acid glycine. The utility of these compounds is in a low caloric edible oil.

    摘要翻译: 本发明涉及可消化水解的低热量食用油替代品。 这些化合物具有正常甘油三酯脂肪的感官特性,但可用热量较低。 具体地,本发明涉及物质的组成。 组合物在一个实施方案中是由甘氨酸盐制备的二聚酸或三聚酸的酰胺。 所述化合物部分地基于氨基酸甘氨酸的氨基酸酯酰胺。 这些化合物的用途是在低热量食用油中。

    Preparation of 4,6-diaminoresorcinol through a bisazoarylresorcinol
intermediate
    16.
    发明授权
    Preparation of 4,6-diaminoresorcinol through a bisazoarylresorcinol intermediate 失效
    通过双偶氮芳基间苯二酚中间体制备4,6-二氨基间苯二酚

    公开(公告)号:US5453542A

    公开(公告)日:1995-09-26

    申请号:US201297

    申请日:1994-02-24

    CPC分类号: C09B41/001 C07C245/08

    摘要: The present invention is a method of preparing a 4,6-bisarylazoresorcinol comprising reacting an aryldiazonium salt and resorcinol in the presence of a base and a reaction medium containing water and a water-miscible solvent at a temperature in the range of about -5.degree. C to about -60.degree. C. The present invention is also a method of preparing a 2-substituted 4,6-bisarylazoresorcinol comprising reacting an aryldiazonium salt with a 2-substituted resorcinol. The 4,6-bisarylazoresorcinol or 2-substituted 4,6-bisarylazoresorcinol can then be hydrogenated to a 4,6-diaminoresorcinol, which is a precursor to polybisbenzoxazoles (PBOs), polymers which are useful as insulators, solar arrays, and tear-resistant gloves.

    摘要翻译: 本发明是一种制备4,6-二芳基氮杂环戊二烯的方法,包括在碱和含有水和水混溶性溶剂的反应介质存在下,在约-5℃的温度下使芳基重氮盐和间苯二酚反应 本发明也是制备2-取代的4,6-二芳基氮杂环戊醇的方法,包括使芳基重氮盐与2-取代的间苯二酚反应。 然后可以将4,6-二芳基氮杂环戊二烯或2-取代的4,6-二芳基氮杂环戊二烯氢化成4,6-二氨基间苯二酚,其是聚双苯并恶唑(PBO)的前体,可用作绝缘体,太阳能阵列和撕裂 - 防护手套

    Synthesis of diaminoresorcinal from resorcinol
    17.
    发明授权
    Synthesis of diaminoresorcinal from resorcinol 失效
    二氨基间苯二酚

    公开(公告)号:US5410083A

    公开(公告)日:1995-04-25

    申请号:US137654

    申请日:1993-10-15

    申请人: Bassam S. Nader

    发明人: Bassam S. Nader

    IPC分类号: C07C213/02 C07C209/36

    CPC分类号: C07C213/02

    摘要: The invention relates to a novel process for preparing 4,6-diaminoresorcinol, a precursor to polybenzoxazole, from resorcinol according to the following scheme. ##STR1## Resorcinol (I) is reacted with a di-tert-alkylating reagent to form a 4,6,-di-tert-alkylresorcinol (II), which is then halogenated to form a 2-halo-4,6-di-tert-alkylresorcinol (III). The 2-halo-4,6-di-tert-alkylresorcinol is nitrated in one of two ways to form a 2-halo-4,6-dinitroresorcinol (IV), which is then hydrogenated to from the 4,6-diaminoresorcinol.The invention also relates to a novel chemical composition-2-halo-4,6-di-tert-alkylresorcinol (III )--and a process for preparing same.

    摘要翻译: 本发明涉及根据以下方案从间苯二酚制备聚苯并恶唑的前体的4,6-二氨基间苯二酚的新方法。 间苯二酚(I)与二叔烷基化试剂反应形成4,6'-二叔烷基间苯二酚(II),然后将其卤化形成2-卤代 -4,6-二 - 叔 - 间 - 间苯二酚(III)。 2-卤代-4,6-二叔烷基间苯二酚以两种方式之一进行硝化以形成2-卤代-4,6-二硝基间苯二酚(IV),然后将其氢化成4,6-二氨基间苯二酚。 本发明还涉及一种新颖的化学组合物2-卤代-4,6-二 - 叔 - 间 - 间苯二酚(III)及其制备方法。

    Novel aryl ether sulfones
    19.
    发明授权
    Novel aryl ether sulfones 失效
    新型芳基醚砜

    公开(公告)号:US5066409A

    公开(公告)日:1991-11-19

    申请号:US581616

    申请日:1990-09-12

    申请人: Bassam S. Nader

    发明人: Bassam S. Nader

    IPC分类号: C07C317/22 C10M135/08

    摘要: Disclosed is an aryl ether sulfone of the following formula: ##STR1## wherein R.sup.1 is independently in each occurrence hydrogen, alkyl, alkoxy, aryl, aryloxy, polyhaloaryl, polyhaloaryloxy, polyhaloalkylaryl, or polyhaloalkylaryloxy, R.sup.2 is independently in each occurrence hydrogen, alkyl, alkoxy, aryl, aryloxy, polyhaloaryl, polyhaloaryloxy, polyhaloalkylaryl, or polyhaloalkylaryloxy, and n is a whole number from 1 to 5. Also disclosed is a lubricant composition which comprises a lubricating fluid and an aryl ether sulfone as shown above, wherein the aryl ether sulfone is present in an amount sufficient to increase the lubricity of the lubricating fluid component.

    摘要翻译: 公开了下式的芳基醚砜:其中R 1在每次出现中独立地为氢,烷基,烷氧基,芳基,芳氧基,多卤代芳基,多卤代芳氧基,多卤代烷基芳基或多卤代烷氧基,R2各自独立地为氢 ,烷基,烷氧基,芳基,芳氧基,多卤代芳基,多卤代芳基氧基,多卤代烷基芳基或多卤代烷氧基,n为1〜5的整数。还公开了一种润滑剂组合物,其包含如上所示的润滑流体和芳基醚砜,其中 芳基醚砜的存在量足以增加润滑液成分的润滑性。