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    OBSTRUCTING MEMBER FOR A FLUIDIZED BED REACTOR
    11.
    发明申请
    OBSTRUCTING MEMBER FOR A FLUIDIZED BED REACTOR 有权
    流化床反应器阻塞构件

    公开(公告)号：US20160047043A1

    公开(公告)日：2016-02-18

    申请号：US14462048

    申请日：2014-08-18

    Applicant: REC Silicon Inc.

    Inventor： Michael V. Spangler ,  Matthew J. Miller

    IPC: C23C16/455 ,  C23C16/24 ,  C23C16/44 ,  C23C16/442

    CPC classification number: C23C16/24 ,  C01B33/027 ,  C23C16/4417 ,  C23C16/442

    Abstract: Embodiments of an obstructing member and methods for its use in a fluidized bed reactor are disclosed. The obstructing member comprises a plurality of receiving members, each receiving member comprising a tubular wall defining a passageway dimensioned to receive an internal reactor component, and a plurality of connecting elements connecting the receiving members, wherein the obstructing member occupies from 15-60% of a horizontal cross-section of a reaction chamber of the fluidized bed reactor.

    Abstract translation: 公开了阻塞构件的实施例及其在流化床反应器中的用途。 阻挡构件包括多个接收构件，每个接收构件包括限定用于容纳内部反应器部件的尺寸的通道的管状壁和连接接收构件的多个连接元件，其中阻挡构件占据了接收构件的15-60％ 流化床反应器的反应室的水平横截面。

    High Vessel Outlet
    12.
    发明申请
    High Vessel Outlet 审中-公开
    高容器出口

    公开(公告)号：US20140252024A1

    公开(公告)日：2014-09-11

    申请号：US13786261

    申请日：2013-03-05

    Applicant: REC SILICON INC

    Inventor： E. Wayne Osborne ,  Matthew J. Miller ,  Michael V. Spangler

    IPC: B67D7/06 ,  B65D88/26

    CPC classification number: B65D88/28 ,  B65D90/10 ,  B65D2590/023

    Abstract: Embodiments of an outlet tube assembly for use with a dispensing vessel are disclosed. The dispensing vessel has a side wall defining a chamber; the side wall has an upper portion and has a lower portion that tapers downwardly to an outlet. The outlet tube assembly facilitates accurate measurement of a particulate material level within the dispensing vessel and/or reduces contamination of the particulate material.

    Abstract translation: 公开了一种用于分配容器的出口管组件的实施例。 分配容器具有限定腔室的侧壁; 侧壁具有上部并且具有向下朝向出口逐渐变细的下部。 出口管组件有助于准确测量分配容器内的颗粒物质水平和/或减少颗粒物质的污染。

    METHOD FOR ANNEALING GRANULAR SILICON WITH AGGLOMERATION CONTROL
    14.
    发明申请
    METHOD FOR ANNEALING GRANULAR SILICON WITH AGGLOMERATION CONTROL 审中-公开

    公开(公告)号：US20180208470A1

    公开(公告)日：2018-07-26

    申请号：US15416274

    申请日：2017-01-26

    Applicant: REC Silicon Inc

    Inventor： Matthew J. Miller ,  Robert J. Geertsen ,  Justin Johnston ,  Stein Julsrud ,  Sefa Yilmaz

    IPC: C01B33/037

    CPC classification number: C01B33/037 ,  C01P2006/80

    Abstract: This disclosure concerns embodiments of an annealing device and a method for annealing flowable, finely divided solids, such as annealing granular silicon to reduce a hydrogen content of the granular silicon. The annealing device comprises at least one tube through which flowable, finely divided solids are flowed downwardly. The tube includes a heating zone and (i) a residence zone below the heating zone, (ii) a cooling zone below the heating zone, or (iii) a residence zone below the heating zone and a cooling zone below the residence zone. An inert gas is flowed upwardly through the tube. The tube may be constructed from two or more tube segments. The annealing device may include a plurality of tubes arranged and housed within a shell. The annealing device and method are suitable for a continuous process.

    Method and apparatus for consolidation of granular silicon and measuring non-metals content
    15.
    发明授权
    Method and apparatus for consolidation of granular silicon and measuring non-metals content 有权
    用于固结颗粒状硅并测量非金属含量的方法和装置

    公开(公告)号：US09580327B2

    公开(公告)日：2017-02-28

    申请号：US14178103

    申请日：2014-02-11

    Applicant: REC Silicon Inc

    Inventor： Sefa Yilmaz ,  Theodore F. Ciszek ,  Matthew J. Miller ,  Stein Julsrud

    IPC: C01B33/021 ,  G01N21/3563 ,  C01B33/037 ,  C01B33/02 ,  C01B33/035 ,  C01B31/14 ,  G01N21/35

    CPC classification number: C01B33/021 ,  C01B32/384 ,  C01B33/02 ,  C01B33/035 ,  C01B33/037 ,  G01N21/3563 ,  G01N2021/3595

    Abstract: Apparatus and methods for consolidating granular silicon and determining trace elements content of the consolidated silicon are disclosed. Silicon granules are placed in a vessel, and a silicon slug of known purity is embedded at least partially in the granules. The slug is preheated to a temperature sufficient to couple with an induction heater. As the silicon slug melts, silicon granules adjacent the molten silicon also melt. The vessel passes through an induction coil to successively inductively heat and melt regions of the silicon granules from the leading end to the trailing end with each region solidifying as the molten silicon exits the induction coil to provide a multicrystalline silicon ingot. The multicrystalline silicon ingot is sliced into wafers, which are analyzed by low-temperature Fourier transform infrared spectroscopy to determine levels of trace elements in the ingot.

    Abstract translation: 公开了用于固结颗粒状硅并确定固结硅的微量元素含量的装置和方法。 将硅颗粒放置在容器中，并且将至少部分地嵌入颗粒中的已知纯度的硅团块。 将坯料预热到足以与感应加热器相连的温度。 当硅团熔化时，与熔融硅相邻的硅颗粒也会熔化。 容器通过感应线圈，以随着熔融硅离开感应线圈而使硅颗粒的前端到后端逐渐地感应加热和熔融，每个区域都固化，从而提供多晶硅锭。 将多晶硅锭切成晶片，通过低温傅里叶变换红外光谱法分析晶锭中微量元素的含量。

    SILICON CARBIDE STACK BOTTOM SEAL ARRANGEMENT
    16.
    发明申请
    SILICON CARBIDE STACK BOTTOM SEAL ARRANGEMENT 审中-公开
    硅碳砖底部密封安装

    公开(公告)号：US20160186319A1

    公开(公告)日：2016-06-30

    申请号：US14977287

    申请日：2015-12-21

    Applicant: REC Silicon Inc

    Inventor： Michael V. Spangler ,  Jeffrey A. Hansen ,  Matthew J. Miller

    IPC: C23C16/44 ,  C23C16/455 ,  C23C16/24

    CPC classification number: C23C16/4409 ,  C23C16/24 ,  C23C16/44 ,  C23C16/4401 ,  C23C16/4417 ,  C23C16/442 ,  C23C16/45563

    Abstract: Fluidized bed reactor systems for producing high purity silicon-coated particles are disclosed. A vessel has an outer shell, an insulation layer inwardly of the outer shell, a concentric inner shell inwardly of the outer shell, and a concentric liner that is positioned inwardly of the inner shell and that defines a reactor chamber. The inner shell and liner are sealed together at their bottoms by an O-ring seal arrangement to prevent gas in the reactor chamber from entering a space between the inner shell and the liner. A central inlet nozzle produces a vertical gas plume in the reactor chamber.

    Abstract translation: 公开了用于生产高纯度硅涂覆颗粒的流化床反应器系统。 容器具有外壳，外壳内部的绝缘层，外壳向内的同心内壳，以及位于内壳内部并且限定反应室的同心衬套。 内壳和内衬在其底部通过O形环密封装置密封在一起，以防止反应器室中的气体进入内壳和衬套之间的空间。 中心入口喷嘴在反应器室中产生垂直气体羽流。

    HIGH-TEMPERATURE GRADE STEEL FOR FLUIDIZED BED REACTOR EQUIPMENT
    19.
    发明申请
    HIGH-TEMPERATURE GRADE STEEL FOR FLUIDIZED BED REACTOR EQUIPMENT 审中-公开
    用于流化床反应器设备的高温分级钢

    公开(公告)号：US20140174353A1

    公开(公告)日：2014-06-26

    申请号：US14109762

    申请日：2013-12-17

    Applicant: REC Silicon Inc

    Inventor： Michael V. Spangler ,  Matthew J. Miller

    IPC: C23C16/442 ,  C23C16/44

    CPC classification number: C23C16/442 ,  C21D1/25 ,  C21D6/002 ,  C22C38/18 ,  C22C38/40

    Abstract: Embodiments of a reaction chamber liner for use in a heated silicon deposition reactor are disclosed. The liner has an upper portion, a mid portion comprising a material other than a stainless steel alloy, and a lower portion comprising a martensitic stainless steel alloy. The liner's upper portion may have a composition substantially similar to the lower portion.

    Abstract translation: 公开了用于加热的硅沉积反应器中的反应室衬套的实施例。 衬套具有上部，中间部分包括不锈钢合金以外的材料，以及包含马氏体不锈钢合金的下部。 衬垫的上部可以具有与下部基本相似的组成。

    PRESSURE-BASED CONTROL OF FLUIDIZED BED REACTOR
    20.
    发明申请
    PRESSURE-BASED CONTROL OF FLUIDIZED BED REACTOR 审中-公开

    公开(公告)号：US20200306712A1

    公开(公告)日：2020-10-01

    申请号：US16833446

    申请日：2020-03-27

    Applicant: REC Silicon Inc

    Inventor： Kahl Brown ,  Matthew J. Miller ,  Benjamin Center ,  Gerald A. Zeininger ,  Stein Julsrud

    IPC: B01J8/18

    Abstract: A method of controlling particle additions to a fluidized bed reactor includes measuring pressure fluctuations inside the fluidized bed reactor over a selected time period, determining a pressure parameter indicative of amplitudes of the pressure fluctuations, comparing the pressure parameter to a specified threshold, and controlling particle additions to the fluidized bed reactor when the pressure parameter deviates from the specified threshold.

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