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公开(公告)号：US08981138B2
公开(公告)日：2015-03-17
申请号：US13375081
申请日：2010-06-01
Applicant: Michael Stepp
Inventor： Michael Stepp
CPC classification number: C07F7/1892 , Y02P20/582
Abstract: The invention relates to a method (a) for producing aminoorganyltriorganylsilanes of the general formula (1) R′3-nR1nSi—R2—NR3R4 (1), a method (b) for producing cyclic aminosilanes of the general formula (4), and a method (III) for producing silylorganoamines of the general formula (7) R013-tR11tSi—R12—NR13—R14—SiR023-sR15s (7), wherein amines are reacted with halogen organylsilanes, wherein R′, R1, R2, R3, R4, R, R5, R6, R01, R02, R11, R12, R13, R14, R15, n, and s have the meanings specified in claims 1 to 3, wherein after the reaction, the ammonium halides of the amines produced as by-products are released by adding a base (B) to the reaction mixture, the amines are removed from the reaction mixture by distillation, two liquid phases are formed by further adding base (B) to the reaction mixture, wherein the one phase contains at least 90 wt % of the hydrohalide of the base (B) and said phase is separated.
Abstract translation: 本发明涉及制备通式（1）R'3-nR1nSi-R2-NR3R4（1）的氨基有机三硼烷硅烷的方法（a），通式（4）的环状氨基硅烷的制备方法（b） 用于制备通式（7）R 10-13-t R 11 t Si-R 12 -NR 13 -R 14 -SiRO 23 -SR 15 S（7）的甲硅烷基有机胺的方法（III），其中胺与卤素有机硅烷反应，其中R'，R 1，R 2，R 3， R4，R，R5，R6，R01，R02，R11，R12，R13，R14，R15，n和s具有权利要求1至3中所定义的含义，其中反应后，胺的卤化铵按 - 通过向反应混合物中加入碱（B）来释放产物，通过蒸馏从反应混合物中除去胺，通过进一步向反应混合物中加入碱（B）形成两个液相，其中一相含有 将碱（B）的氢卤酸盐和所述相的至少90重量％分离。
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公开(公告)号：US20140228589A1
公开(公告)日：2014-08-14
申请号：US14345779
申请日：2012-09-07
Applicant: Michael Stepp , Michael Mueller , Birgit Peschanel
Inventor： Michael Stepp , Michael Mueller , Birgit Peschanel
IPC: C07F7/08
CPC classification number: C07F7/0836 , C07F7/0838
Abstract: Alkali metal silanolates are prepared by a process in which alcohol and water are removed from an alkali metal silanolate hydrolysis mixture in two steps, the second removal step occurring at a pressure lower than the first removal step.
Abstract translation: 碱金属硅烷醇盐通过两步法从碱金属硅烷醇盐水解混合物中除去醇和水的方法制备，第二除去步骤在低于第一除去步骤的压力下进行。
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公开(公告)号：US08748645B2
公开(公告)日：2014-06-10
申请号：US13810676
申请日：2011-07-11
Applicant: Daniel Schildbach , Dominik Auer , Karl-Heinz Felix , Michael Stepp
Inventor： Daniel Schildbach , Dominik Auer , Karl-Heinz Felix , Michael Stepp
IPC: C07F7/02
CPC classification number: C07F7/0836 , C04B24/42 , C04B2111/00672 , C04B2111/27 , C04B2111/60 , C04B2111/62 , C04B2111/70 , C04B2111/72 , C07F7/1804 , Y10T428/2982
Abstract: Organosilanolate powders having a low cation to silicon ratio provide superior hydrophobing ability. The powders may be prepared on an industrial scale by hydrolysis of a silane with a basic salt solution, adding an inert organic solvent, and removing gaseous or alcoholic hydrolysis products by evaporation or distillation, precipitating the organosilanolate as a fine powder.
Abstract translation: 具有低阳离子与硅比的有机硅烷醇钠粉末提供了优异的疏水性能。 粉末可以通过用碱性盐溶液水解硅烷，加入惰性有机溶剂和通过蒸发或蒸馏除去气态或醇水解产物而以工业规模制备，将有机硅烷醇化物作为细粉末沉淀。
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公开(公告)号：US20120296106A1
公开(公告)日：2012-11-22
申请号：US13497673
申请日：2010-10-19
Applicant: Michael Stepp , Tobias Weiss
Inventor： Michael Stepp , Tobias Weiss
IPC: C07F7/16
Abstract: The invention relates to a process for preparing diorganyldihalosilanes of the general formula (1) R2SiX2 (1), in which dihalodihydrosilanes of the general formula (2) X2SiH2 (2), in a mixture with silanes of the general formula (3) R′3SiH (3), are reacted with halogenated hydrocarbons of the general formula (4) R-X (4), in the presence of a free-radical initiator, which is selected from alkanes, diazenes and organodisilanes, where R is a monovalent C1-C18 hydrocarbon radical, R′ is a monovalent C1-C18 hydrocarbon radical, hydrogen or halogen, and X is halogen.
Abstract translation: 本发明涉及通式（1）R2SiX2（1）的二有机基二卤代硅烷的制备方法，其中通式（2）X2SiH 2（2）的二卤代二氢化硅烷与通式（3）的硅烷的混合物R' 3SiH（3）与通式（4）RX（4）的卤代烃在选自烷烃，二氮烯和有机二硅烷的自由基引发剂存在下反应，其中R是一价C1-C18 烃基，R'是一价C1-C18烃基，氢或卤素，X是卤素。
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公开(公告)号：US20120100057A1
公开(公告)日：2012-04-26
申请号：US13379458
申请日：2010-06-16
Applicant: Michael Stepp
Inventor： Michael Stepp
IPC: C01B33/107
CPC classification number: C01B33/107
Abstract: The invention relates to a method for producing neopentasilanes of the general formula (1) Si(SiR3)4 (1), wherein silicon compounds of the general formula (2) R3Si— (SiR2—)xSiR3 (2), where R is selected from Cl, Br, and I, and x is a non-negative whole number up to 5, are converted in the presence of catalytically active compounds (K), wherein the separating of the tetrahalogen silane formed thereby takes place by distilling out in the presence of a compound (L) that is liquid at room temperature having a higher boiling point than the released tetrahalogen silane.
Abstract translation: 本发明涉及制备通式（1）Si（SiR 3）4（1）的新戊基硅烷的方法，其中通式（2）中的硅化合物R3Si-（SiR2-）xSiR3（2），其中选择R 来自Cl，Br和I，x是至多为5的非负整数，在催化活性化合物（K）的存在下转化，其中由此形成的四卤代硅烷的分离通过在 在室温下具有比释放的四卤代硅烷沸点高的化合物（L）的存在。
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Patent Agency Ranking
公开(公告)号：US20120071650A1
公开(公告)日：2012-03-22
申请号：US13375081
申请日：2010-06-01
Applicant: Michael STEPP
Inventor： Michael STEPP
CPC classification number: C07F7/1892 , Y02P20/582
Abstract: The invention relates to a method (a) for producing aminoorganyltriorganylsilanes of the general formula (1) R′3-nR1nSi—R2—NR3R4 (1), a method (b) for producing cyclic aminosilanes of the general formula (4), and a method (III) for producing silylorganoamines of the general formula (7) R013-tR11tSi—R12—NR13—R14—SiR023-sR15s (7), wherein amines are reacted with halogen organylsilanes, wherein R′, R1, R2, R3, R4, R, R5, R6, R01, R02, R11, R12, R13, R14, R15, n, and s have the meanings specified in claims 1 to 3, wherein after the reaction, the ammonium halides of the amines produced as by-products are released by adding a base (B) to the reaction mixture, the amines are removed from the reaction mixture by distillation, two liquid phases are formed by further adding base (B) to the reaction mixture, wherein the one phase contains at least 90 wt % of the hydrohalide of the base (B) and said phase is separated.
Abstract translation: 本发明涉及制备通式（1）R'3-nR1nSi-R2-NR3R4（1）的氨基有机三硼烷硅烷的方法（a），通式（4）的环状氨基硅烷的制备方法（b） 用于制备通式（7）R 10-13-t R 11 t Si-R 12 -NR 13 -R 14 -SiRO 23 -SR 15 S（7）的甲硅烷基有机胺的方法（III），其中胺与卤素有机硅烷反应，其中R'，R 1，R 2，R 3， R4，R，R5，R6，R01，R02，R11，R12，R13，R14，R15，n和s具有权利要求1至3中所定义的含义，其中反应后，胺的卤化铵按 - 通过向反应混合物中加入碱（B）来释放产物，通过蒸馏从反应混合物中除去胺，通过进一步向反应混合物中加入碱（B）形成两个液相，其中一相含有 将碱（B）的氢卤酸盐和所述相的至少90重量％分离。
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公开(公告)号：US08039426B2
公开(公告)日：2011-10-18
申请号：US12990257
申请日：2009-04-29
Applicant: Michael Stepp , Uwe Paetzold , Christian Schierlinger
Inventor： Michael Stepp , Uwe Paetzold , Christian Schierlinger
IPC: C23G5/06
CPC classification number: C01B33/107
Abstract: The invention relates to a method for hydrolyzing hydrolyzable metallic salts, the metallic salts being reacted with emulsions of a) water and b) an inert liquid.
Abstract translation: 本发明涉及水解可水解金属盐的方法，金属盐与a）水和b）惰性液体的乳液反应。
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28.发明申请公开(公告)号：US20090016947A1
公开(公告)日：2009-01-15
申请号：US12281550
申请日：2007-02-21
Applicant: Laszlo Fabry , Uwe Paetzold , Michael Stepp
Inventor： Laszlo Fabry , Uwe Paetzold , Michael Stepp
IPC: C01B33/107
CPC classification number: C01B33/10763
Abstract: Trichlorosilane production is increased while simultaneously lowering environmental burden due to destruction and disposition of high boilers by feeding high boilers from trichlorosilane production or from polycrystalline silicon production into a fluidized bed for production of trichlorosilane from metallic silicon and hydrogen chloride.
Abstract translation: 三氯硅烷生产增加，同时通过将来自三氯硅烷生产的高锅炉或从多晶硅生产送入用于从金属硅和氯化氢生产三氯硅烷的流化床，由于高锅炉的破坏和处置而降低环境负荷。
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29.发明授权Organosilicon compounds, processes for their preparation, and their use in crosslinkable organopolysiloxane compositions 失效有机硅化合物，其制备方法及其在可交联有机聚硅氧烷组合物中的用途公开(公告)号：US06313217B1
公开(公告)日：2001-11-06
申请号：US09366800
申请日：1999-08-04
Applicant: Herbert Barthel , Johann Schuster , Richard Weidner , Michael Stepp , Volker Frey
Inventor： Herbert Barthel , Johann Schuster , Richard Weidner , Michael Stepp , Volker Frey
IPC: C08G7708
CPC classification number: C08L83/04 , C07F7/0838 , C08G77/045 , C08G77/12 , C08G77/16 , C08G77/18 , C08G77/20 , C08G77/80 , C08K5/5419 , C08L83/00 , C08L2666/44 , C08L2666/54 , C08L2666/28
Abstract: The invention relates to aliphatically unsaturated organosilicon compounds having 2 to 17 silicon atoms, to processes for their preparation and to their use in crosslinkable organopolysiloxane compositions, especially in compositions which can be crosslinked peroxidically or by hydrosilylation.
Abstract translation: 本发明涉及具有2至17个硅原子的脂族不饱和有机硅化合物，其制备方法及其在可交联有机聚硅氧烷组合物中的用途，特别是在可以通过过氧化或通过氢化硅烷化反应的组合物中。
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30.发明授权Storage-stable polysiloxane composition which gives permanently water-wettable vulcanizates 失效储存稳定的聚硅氧烷组合物，其赋予永久性水润湿硫化橡胶
公开(公告)号：US5580921A
公开(公告)日：1996-12-03
申请号：US196106
申请日：1994-02-10
Applicant: Michael Stepp , Heinz Hefner, deceased , Peter Huber , Johann Mueller , Richard Schmidlkofer , Arnold Garhammer
Inventor： Michael Stepp , Heinz Hefner, deceased , Peter Huber , Johann Mueller , Richard Schmidlkofer , Arnold Garhammer
CPC classification number: A61K6/10 , C08G77/20 , C08L83/04 , C08G77/12 , C08G77/16 , C08G77/18 , C08G77/24
Abstract: The present invention relates to storage-stable polysiloxane compositions which give permanently water-wettable elastomers. The polysiloxane compositions of the present invention which vulcanize to yield elastomers are useful as dental impression compositions.
Abstract translation: PCT No.PCT / EP92 / 02036 Sec。 371日期：1994年2月10日 102（e）1994年2月10日PCT PCT 1992年9月3日PCT公布。 出版物WO93 / 04659 日本1993年3月18日本发明涉及赋予永久性水润湿弹性体的储存稳定的聚硅氧烷组合物。 硫化产生弹性体的本发明的聚硅氧烷组合物可用作牙印模组合物。
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