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    Polyisocyanate-modified polycarboxylic acids
    23.
    发明授权
    Polyisocyanate-modified polycarboxylic acids 有权
    多异氰酸酯改性多元羧酸

    公开(公告)号：US07329717B2

    公开(公告)日：2008-02-12

    申请号：US10873081

    申请日：2004-06-21

    Applicant: Hans-Josef Laas ,  Christoph Gürtler ,  Reinhard Halpaap ,  Michael Grahl ,  Peter Thometzek ,  James Rawlins

    Inventor： Hans-Josef Laas ,  Christoph Gürtler ,  Reinhard Halpaap ,  Michael Grahl ,  Peter Thometzek ,  James Rawlins

    IPC: C08G18/70

    CPC classification number: C08G18/792 ,  C08G18/341 ,  C08G18/4277 ,  C08G18/725 ,  C08G18/758 ,  C08G18/798 ,  C08G18/8064

    Abstract: A process for preparing polyisocyanate-modified polycarboxylic acids by conversion of anhydride-group-free polycarboxylic acids with isocyanate-functional compounds. The process includes reacting A) an anhydride-group-free polycarboxylic-acid component with B) an isocyanate-functional component having an (average) isocyanate functionality of at least 1.8, at an equivalent ratio of carboxylic acid groups to isocyanate groups of from 1.2:1 to 120:1. The polyisocyanate-modified polycarboxylic acids are solid below 40° C. and liquid above 130° C., and have an average carboxylic acid functionality of at least 1.8, a content of free carboxylic acid groups of from 4.0 wt. % to 80.0 wt. % and a content of amide groups of from 0.4 wt. % to 32.5 wt. %.

    Abstract translation: 一种通过使用无酸酐基的多元羧酸与异氰酸酯官能化合物的转化制备多异氰酸酯改性的多元羧酸的方法。 该方法包括使A）无酸酐基的多元羧酸组分与B）具有至少1.8的（平均）异氰酸酯官能度的异氰酸酯官能组分以羧酸基团与异氰酸酯基团的当量比为1.2 ：1〜120：1。 多异氰酸酯改性的多元羧酸是固体低于40℃，液体高于130℃，平均羧酸官能度至少为1.8，游离羧酸基团的含量为4.0重量％。 ％至80.0wt。 ％和酰胺基团的含量为0.4重量％ ％至32.5重量％ ％。

    Polyadducts containing uretidone groups
    24.
    发明授权
    Polyadducts containing uretidone groups 有权
    含有uretidone基团的多元体系

    公开(公告)号：US06987158B2

    公开(公告)日：2006-01-17

    申请号：US10613725

    申请日：2003-07-03

    Applicant: Hans-Josef Laas ,  Reinhard Halpaap ,  Peter Thometzek ,  Michael Grahl ,  Hans-Ulrich Meier-Westhues

    Inventor： Hans-Josef Laas ,  Reinhard Halpaap ,  Peter Thometzek ,  Michael Grahl ,  Hans-Ulrich Meier-Westhues

    IPC: C08G18/79 ,  C08G18/80 ,  C08G18/73 ,  C08G18/75 ,  C07D229/00

    CPC classification number: C08G18/2036 ,  C07D229/00 ,  C08G18/027 ,  C08G2150/00 ,  C08G2150/20

    Abstract: Polyaddition compounds containing uretdione groups prepared by reacting uretdione polyisocyanates formed from diisocyanates having exclusively secondary- and/or tertiary-attached isocyanate groups with a molar fraction of isocyanurate structures, based on the sum of uretdione groups and isocyanurate groups, of not more than 10%, with compounds reactive towards isocyanates. The polyaddition compounds can be use as a starting component in the preparation of polyurethane plastics, in particular as crosslinkers for heat-crosslinkable powder coating materials. The compounds may be used as starting components in the preparation of moldings and shaped parts, and as starting components in the preparation of coating materials and coatings.

    Abstract translation: 通过使仅由二级和/或三级连接的异氰酸酯基组成的二异氰酸酯形成的脲二酮多异氰酸酯与基于脲二酮基团和异氰脲酸酯基团的总量的异氰脲酸酯结构的摩尔分数反应制备的含有脲二酮基团的加聚化合物不超过10％ 具有对异氰酸酯反应的化合物。 加聚化合物可用作制备聚氨酯塑料的起始组分，特别是作为热交联粉末涂料的交联剂。 这些化合物可以用作制备模塑件和成型件的起始组分，并且可用作制备涂料和涂料的起始组分。

    Modified polyisocyanates
    26.
    发明授权
    Modified polyisocyanates 有权
    改性多异氰酸酯

    公开(公告)号：US06767958B2

    公开(公告)日：2004-07-27

    申请号：US10276344

    申请日：2002-11-14

    Applicant: Hans-Josef Laas ,  Reinhard Halpaap

    Inventor： Hans-Josef Laas ,  Reinhard Halpaap

    IPC: C08G1830

    CPC classification number: C08G18/283 ,  C08G18/0828 ,  C08G18/6254 ,  C08G18/706 ,  C08G18/807 ,  Y10T428/31551

    Abstract: The present invention relates to a modified polyisocyanate which is the reaction product of a polyisocyanate with 2-(cyclohexylamino)-ethanesulfonic acid and/or 3-(cyclohexylamino)-propanesulfonic acid, to a process for preparing these modified polyisocyanates, to coating compositions containing these modified polyisocyanates and to coated substrates prepared from these coating compositions.

    Abstract translation: 本发明涉及一种改性多异氰酸酯，其是多异氰酸酯与2-（环己基氨基） - 乙磺酸和/或3-（环己基氨基） - 丙磺酸的反应产物，涉及制备这些改性多异氰酸酯的方法， 这些改性的多异氰酸酯和由这些涂料组合物制备的涂布的基材。

    Process for the preparation of polyisocyanates with a biuret structure
    27.
    发明授权
    Process for the preparation of polyisocyanates with a biuret structure 有权
    制备具有缩二脲结构的多异氰酸酯的方法

    公开(公告)号：US06720400B2

    公开(公告)日：2004-04-13

    申请号：US09858057

    申请日：2001-05-15

    Applicant: Reinhard Halpaap ,  Dieter Mager ,  Siegfried Oeckl ,  Harald Mertes

    Inventor： Reinhard Halpaap ,  Dieter Mager ,  Siegfried Oeckl ,  Harald Mertes

    IPC: C08G1860

    CPC classification number: C08G18/7831 ,  C07C273/1818

    Abstract: The present invention relates to an improved process for the continuous preparation of polyisocyanates with a biuret structure comprising the steps of continuously reacting excess amounts of organic diisocyanates having exclusively aliphatically and/or cycloaliphatically bound isocyanate groups with organic diamines having exclusively aliphatically and/or cycloaliphatically bound primary amino groups at temperatures above 170° C. and adding acid before or during the reaction.

    Abstract translation: 本发明涉及连续制备具有缩二脲结构的多异氰酸酯的改进方法，其包括以下步骤：将仅含有脂族和/或环状结合的异氰酸酯基的过量的有机二异氰酸酯与仅具有脂族和/或环状结合的有机二胺连续反应 在高于170℃的温度下加入伯氨基并在反应之前或期间加入酸。

    Powder coating crosslinking agents containing uretdione groups and free isocyanate
    28.
    发明授权
    Powder coating crosslinking agents containing uretdione groups and free isocyanate 失效
    含有脲二酮基团和游离异氰酸酯的粉末涂料交联剂

    公开(公告)号：US06297343B1

    公开(公告)日：2001-10-02

    申请号：US09489984

    申请日：2000-01-21

    Applicant: Hans-Josef Laas ,  Ulrich Freudenberg ,  Reinhard Halpaap ,  Michael Grahl

    Inventor： Hans-Josef Laas ,  Ulrich Freudenberg ,  Reinhard Halpaap ,  Michael Grahl

    IPC: C08G1880

    CPC classification number: C08G18/44 ,  C08G18/4277 ,  C08G18/664 ,  C08G18/798 ,  C08G2150/20

    Abstract: The present invention relates to polyaddition compounds, which are solid below 40° C. and liquid above 125° C., are prepared by the reaction of an isocyanate component containing uretdione groups with a polyol containing ester and/or carbonate groups, other than hydroxypivalic acid neopentylglycol ester, and have a) an average isocyanate functionality of 2.0 to 8.0 and a content of free isocyanate groups (calculated as NCO; molecular weight=42) of 2.1 to 6.0 wt. %, b) a content of uretdione groups (calculated as C2N2O2; molecular weight=84) of 10 to 19 wt. %, c) a content of urethane groups (calculated as —NH—CO—O; molecular weight=59) of 10 to 17 wt. % and d) a content of ester groups —CO—O (calculated as —CO—O; molecular weight=44) and/or carbonate groups —O—CO—O (calculated as —CO—O; molecular weight=44) of 1 to 17 wt. %. The present invention also relates to a process for the preparation of these polyaddition compounds to two-component polyurethane powder coating compositions containing these polyaddition compounds as the crosslinking agent and isocyanate-reactive compounds as the binder.

    Abstract translation: 本发明涉及通过含有脲二酮基团的异氰酸酯组分与含有多羟基酯和/或碳酸酯基团的异氰酸酯组分（羟基新戊酸新戊二醇）反应来制备固体低于40℃的加氢化合物和高于125℃的液体 酯和hasa）的平均异氰酸酯官能度为2.0至8.0，游离异氰酸酯基团的含量（以NCO计算;分子量= 42）为2.1至6.0重量％。 ％，b）脲二酮基团的含量（以C 2 N 2 O 2计算;分子量= 84）为10〜19重量％。 ％，c）氨基甲酸酯基团的含量（以-NH-CO-O计算;分子量= 59）为10〜17重量％。 ％和d）酯基-CO-O（以-CO-O计算;分子量= 44）和/或碳酸酯基团-O-CO-O（以-CO-O计算;分子量= 44）的含量为 1至17wt。 ％。 本发明还涉及将这些加聚化合物制备成双组分聚氨酯粉末涂料组合物的方法，该组合物含有这些加聚化合物作为交联剂和异氰酸酯反应性化合物作为粘合剂

    Coating compositions containing alkoxysilanes
    29.
    发明授权
    Coating compositions containing alkoxysilanes 失效
    含有烷氧基硅烷的涂料组合物

    公开(公告)号：US06281322B1

    公开(公告)日：2001-08-28

    申请号：US09451539

    申请日：1999-12-01

    Applicant: Stefan Groth ,  Reinhard Halpaap ,  Markus Mechtel ,  Lutz Schmalstieg ,  Philip E. Yeske

    Inventor： Stefan Groth ,  Reinhard Halpaap ,  Markus Mechtel ,  Lutz Schmalstieg ,  Philip E. Yeske

    IPC: C08G7726

    CPC classification number: C08G18/792 ,  C08G18/282 ,  C08G18/289 ,  C08G18/758 ,  C09D175/04 ,  Y10T428/31551 ,  Y10T428/31663

    Abstract: The present invention relates to coating compositions containing 40 to 100% by weight, based on resin solids, of an alkoxysilyl-functional polyisocyanate polyurea which is reaction product of A) a polyisocyanate component having an average functionality of 2.5 to 5.5, an NCO content of 11.0 to 20.0% by weight and a monomeric diisocyanate content of less than 10% by weight, and containing at least 50% by weight of a polyisocyanate prepared from 4,4′-diisocyanatodicyclohexyl-methane with B) at least 0.7 equivalents, based on the equivalents of isocyanate groups, of an aminosilane corresponding to formula (I) (RO)nY(3−n)Si—CH2CH2CH2—NHZ  (I),  wherein R represents methyl or ethyl, Y represents methyl, Z represents H, a C1-C12 alkyl or CH2CH2CH2—Si(OR)nY3−n, and n is 1, 2 or 3, and C) optionally other isocyanate-reactive compounds. The present invention also relates the hydrolyzates/condensates that are prepared by adding water or an aqueous solution of a catalyst to the coating compositions according to the invention.

    Abstract translation: 本发明涉及基于树脂固体含有40-100重量％的烷氧基甲硅烷基官能多异氰酸酯聚脲的涂料组合物，其是A）平均官能度为2.5至5.5的多异氰酸酯组分，NCO含量为11.0 至20.0重量％，并且单体二异氰酸酯含量小于10重量％，并且含有至少50重量％的由4,4'-二异氰酸根合二环己基甲烷制备的聚异氰酸酯与B）至少0.7当量，基于当量 的异氰酸酯基，对应于式（I）的氨基硅烷，其中R表示甲基或乙基，Y表示甲基，Z表示H，C1-C12烷基或CH2CH2CH2-Si（OR）nY3-n，n为1,2或3 ，和C）任选其它异氰酸酯反应性化合物。 本发明还涉及通过将水或催化剂的水溶液加入到根据本发明的涂料组合物中制备的水解产物/缩合物。

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