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    Heat-stable anion exchangers
    21.
    发明申请
    Heat-stable anion exchangers 有权
    热稳定阴离子交换剂

    公开(公告)号：US20080087604A1

    公开(公告)日：2008-04-17

    申请号：US11899125

    申请日：2007-09-04

    申请人： Pierre Vanhoorne ,  Wolfgang Podszun ,  Reinhold Klipper ,  Michael Schelhaas

    发明人： Pierre Vanhoorne ,  Wolfgang Podszun ,  Reinhold Klipper ,  Michael Schelhaas

    IPC分类号： C08J9/00 ,  B01D15/04

    CPC分类号： B01J41/14 ,  B01J31/08 ,  C02F1/42 ,  C02F2001/422 ,  C02F2103/023

    摘要： The present invention relates to heat-stable anion exchangers based on at least one aromatic monomer and at least one crosslinker having structural elements of the general formula (I) where Ak, Ak′, Ak″ are in each case independently of one another identically or differently a C1-C18-alkyl radical, n is an even number between 5 and 18, x+y=2 and X is Cl, Br, OH, HCO3, HSO4, ½ (SO4), ½ CO3, NO3, F, H2PO4, ½ HPO4, ⅓ PO4 with the result that these anion exchangers, preferably in the OH form, withstand a working temperature of at least 60° C., preferably of at least 80° C., over a relatively long time, a process for production thereof and also use thereof.

    摘要翻译： 本发明涉及基于至少一种芳族单体和至少一种具有通式（I）的结构元件的交联剂的热稳定阴离子交换剂，其中Ak，Ak'，Ak“在每种情况下彼此独立地彼此独立地 或者不同的是C 1 -C 18 - 烷基，n是5至18之间的偶数，x + y = 2，X是Cl，Br，OH， HCO 3，HSO 4，½（SO 4 S），1/3 CO 3，NO 3， / SUB，F，H 2 PO 4，1/2 HPO 4，1/3 PO 4，和 结果是这些阴离子交换剂优选为OH形式，在相当长的时间内经受至少60℃，优选至少80℃的工作温度，其制备方法及其用途。

    Picolylamine resins
    22.
    发明授权
    Picolylamine resins 有权
    吡啶基胺树脂

    公开(公告)号：US08563622B2

    公开(公告)日：2013-10-22

    申请号：US12919851

    申请日：2009-02-27

    申请人： Michael Schelhaas ,  Reinhold Klipper ,  Duilio Rossoni

    发明人： Michael Schelhaas ,  Reinhold Klipper ,  Duilio Rossoni

    IPC分类号： C08F8/32 ,  C08F212/08 ,  C01G13/00 ,  C01G49/00 ,  C01G3/00 ,  C01G9/00

    CPC分类号： C08F8/30 ,  B01J45/00 ,  C01G3/003 ,  C02F1/285 ,  C02F2101/20 ,  C02F2101/203 ,  C08F8/02 ,  C08F8/44 ,  C22B3/42 ,  C22B15/0089 ,  Y02P10/234 ,  Y02P10/236 ,  C08F212/08

    摘要： The present application relates to novel monodisperse, gel-type or macroporous picolylamine resins which are based on at least one monovinylaromatic compound and at least one polyvinylaromatic compound and/or a (meth)acrylic compound and contain tertiary nitrogen atoms in structures of the general formula (I) as functional group, where R1 is an optionally substituted radical from the group consisting of picolyl, methylquinoline and methylpiperidine, R2 is a radical —(CH2)q—COOR3, R3 is a radical from the group consisting of H, Na and K, m is an integer from 1 to 4, n and p are each, independently of one another, a number in the range from 0.1 to 1.9 and the sum of n and p is 2, q is an integer from 1 to 5 and M is the polymer matrix, a process for preparing them and their uses, in particular the use in hydrometallurgy and electroplating.

    摘要翻译： 本申请涉及基于至少一种单乙烯基芳族化合物和至少一种聚乙烯基芳族化合物和/或（甲基）丙烯酸化合物并且在通式结构中含有叔氮原子的新型单分散，凝胶型或大孔吡甲基胺树脂 （I）作为官能团，其中R 1是由吡啶甲基，甲基喹啉和甲基哌啶组成的组中的任选取代的基团，R 2是 - （CH 2）q -COOR 3基团，R 3是由H，Na和 K，m为1〜4的整数，n和p各自独立地为0.1〜1.9的数，n与p的和为2，q为1〜5的整数， M是聚合物基质，其制备方法及其用途，特别是在湿法冶金和电镀中的应用。

    AMPHOTERIC ION EXCHANGERS
    27.
    发明申请
    AMPHOTERIC ION EXCHANGERS 有权
    AMPHOTERIC离子交换剂

    公开(公告)号：US20090107918A1

    公开(公告)日：2009-04-30

    申请号：US12249148

    申请日：2008-10-10

    申请人： Reinhold Klipper ,  Hans Karl Soest ,  Ulrich Litzinger ,  Michael Schelhaas ,  Georg Martin

    发明人： Reinhold Klipper ,  Hans Karl Soest ,  Ulrich Litzinger ,  Michael Schelhaas ,  Georg Martin

    IPC分类号： C08J5/20 ,  B01D15/36

    CPC分类号： B01J43/00

    摘要： The present invention relates to novel amphoteric ion exchangers which possess not only phthalamide groups of the formula (I) but also —(CH2)mNR1R2 groups and/or if appropriate —(CH2)mNR1R2R3 groups, wherein m is an integer from 1 to 4 and R1, R2, R3 in each case independently of one another are hydrogen, —CH3, —CH2CH3, —CH2CH2CH3, benzyl, —OCH2CH3 or —CH2CH2OH and X is H or Na or K, to a process for production thereof and also use thereof.

    摘要翻译： 本发明涉及新型的两性离子交换剂，其不仅具有式（I）的邻苯二甲酰胺基团，而且还具有 - （CH 2）m N R 1 R 2基团和/或如果合适的 - （CH 2）m N R 21 R 3基团，其中m是1至4的整数 R 1，R 2，R 3各自独立地为氢，-CH 3，-CH 2 CH 3，-CH 2 CH 2 CH 3，苄基，-OCH 2 CH 3或-CH 2 CH 2 OH，X为H或Na或K，为其制备方法，并且还使用 其中。

    Preparation of aliphatic &agr;, &ohgr;-dicarboxylic acids
    29.
    发明授权
    Preparation of aliphatic &agr;, &ohgr;-dicarboxylic acids 失效
    脂肪族α，ω-二羧酸的制备

    公开(公告)号：US06437180B1

    公开(公告)日：2002-08-20

    申请号：US09568894

    申请日：2000-05-11

    申请人： Michael Schelhaas ,  Helmut Greiving ,  Manfred Jautelat

    发明人： Michael Schelhaas ,  Helmut Greiving ,  Manfred Jautelat

    IPC分类号： C07C5116

    CPC分类号： C07C51/285 ,  C07C55/02 ,  C07C55/14

    摘要： A process for preparing aliphatic C4-18 &agr;,&ohgr;-dicarboxylic acids by oxidation of C6-20 &agr;,&ohgr;-dienes with hydrogen peroxide or compounds which release hydrogen peroxide under the reaction conditions as is characterized in that the reaction is carried out in the presence of a transition metal catalyst of group VI and of a mixture containing at least one organic acid and one aprotic organic solvent. A specific temperature profile is maintained at different phases of the reaction, which increases yield and selectivity.

    摘要翻译： 通过在反应条件下通过氧化C6-20α，ω-二烯与过氧化氢或释放过氧化氢的化合物来制备脂族C4-18α，ω-二羧酸的方法，其特征在于反应在 存在第VI族的过渡金属催化剂和含有至少一种有机酸和一种非质子有机溶剂的混合物。 在反应的不同阶段保持特定的温度曲线，这提高了产率和选择性。

    Process for preparing 4-aminodiphenylamine
    30.
    发明授权
    Process for preparing 4-aminodiphenylamine 失效
    制备4-氨基二苯胺的方法

    公开(公告)号：US06414192B1

    公开(公告)日：2002-07-02

    申请号：US10007014

    申请日：2001-11-06

    申请人： Michael Schelhaas ,  Carl Casser ,  Dietmar Bielefeldt ,  Pieter Ooms ,  Joachim Haider ,  Manfred Jautelat ,  Christian Laue ,  Henry Giera

    发明人： Michael Schelhaas ,  Carl Casser ,  Dietmar Bielefeldt ,  Pieter Ooms ,  Joachim Haider ,  Manfred Jautelat ,  Christian Laue ,  Henry Giera

    IPC分类号： C07C20900

    CPC分类号： C07C209/38 ,  C07C211/55

    摘要： The invention provides a process for preparing 4-aminodiphenylamine, an important starting product for synthesizing antioxidants and stabilizers in the rubber and polymer industry, by hydrogenating nitrosobenzene with hydrogen in the presence of a proton acid as catalyst and in the presence of a hydrogenating catalyst, optionally in the presence of an inert organic solvent and thermally decomposing the 4-ADPA ammonium salt produced in this way, wherein 4-ADPA is obtained. 4-aminodiphenylamine is produced in good yields and high purity by the process according to the present invention. Furthermore, no effluent is produced, which makes the process particularly economic and ecological.

    摘要翻译： 本发明提供一种制备4-氨基二苯胺的方法，该方法是在质子酸作为催化剂存在下，在氢化催化剂存在下，通过在氢气存在下，用氢气将亚硝基苯氢化，在橡胶和聚合物工业中合成抗氧化剂和稳定剂的重要起始产物， 任选地在惰性有机溶剂的存在下，并以这种方式产生的4-ADPA铵盐热分解，得到4-ADPA。4-氨基二苯胺通过本发明的方法以良好的产率和高纯度生产。 此外，没有产生流出物，这使得该过程特别经济和生态。