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    Functionalized substrates with ion-exchange properties
    3.
    发明授权
    Functionalized substrates with ion-exchange properties 有权
    具有离子交换性能的功能化底物

    公开(公告)号：US09314712B2

    公开(公告)日：2016-04-19

    申请号：US12118447

    申请日：2008-05-09

    Applicant: Xiaodong Liu ,  Christopher A. Pohl ,  Jinhua Chen ,  L. Andy Woodruff

    Inventor： Xiaodong Liu ,  Christopher A. Pohl ,  Jinhua Chen ,  L. Andy Woodruff

    IPC: B01D15/36 ,  B01D15/32 ,  B01J20/28 ,  B01J20/32 ,  B01J39/26 ,  B01J43/00 ,  B01D15/38

    CPC classification number: B01D15/362 ,  B01D15/325 ,  B01D15/361 ,  B01D15/363 ,  B01D15/3847 ,  B01J20/28097 ,  B01J20/3221 ,  B01J20/3285 ,  B01J20/3295 ,  B01J39/26 ,  B01J43/00 ,  B01J41/20

    Abstract: The current invention provides compositions, which are useful as stationary phases for a variety of chromatographic applications, such as high performance liquid chromatography (HPLC) and solid-phase extraction (SPE). The compositions include a porous solid support (e.g., silica gels, silica monoliths or synthetic organic resins) having an exterior surface and pore openings defined by “interior walls”. To the solid support are covalently bound organic ion-exchange ligands (e.g., silyl ligands), which incorporate at least one ion-exchange group (e.g., ionic or ionizable group). The compositions further include micro-particles (e.g., latex particles) incorporating ion-exchange groups having a charge that is opposite to the charge found on the support. The micro-particles are bound to the exterior surface of the support (e.g., via electrostatic forces). The micro-particles have a size that is sufficient to minimize the number of particles that can enter the pores of the support thereby reducing or essentially preventing binding of the micro-particles to the interior walls of the pores. While the pores are essentially too small for the micro-particles, they can still be accessed by the analytes present in a chromatographic sample. The physical separation of ion-exchange groups located within the pores and the surface of the micro-particles, respectively, prevents reactions (e.g., formation of salt-bridges) between the oppositely charged groups and provides compositions with both anion-exchange and cation-exchange capabilities within the same stationary phase. The ligands bound to the solid support can optionally include additional (e.g., reverse-phase) functionalities creating multi-modal (e.g., trimodal) stationary phases.

    Abstract translation: 本发明提供了用于各种色谱应用的固定相的组合物，例如高效液相色谱（HPLC）和固相萃取（SPE）。 组合物包括具有由“内壁”限定的外表面和孔开口的多孔固体支持物（例如硅胶，二氧化硅整料或合成有机树脂）。 固体支持物是共价结合的有机离子交换配体（例如，甲硅烷基配体），其结合至少一个离子交换基团（例如离子或可离子化基团）。 组合物还包括结合离子交换基团的微粒（例如胶乳颗粒），其具有与载体上发现的电荷相反的电荷。 微粒子结合到支撑体的外表面（例如通过静电力）。 微粒具有足以使能够进入载体的孔的颗粒数量最小化的尺寸，从而减少或基本上防止微粒与孔内壁的结合。 虽然孔对于微粒基本上太小，但是它们仍然可以通过色谱样品中存在的分析物进行访问。 分别位于孔和微粒表面之间的离子交换基团的物理分离防止相反电荷基团之间的反应（例如，形成盐桥），并提供具有阴离子交换和阳离子交换的组合物， 交换能力在同一个固定阶段。 与固体支持物结合的配体可以任选地包括产生多模态（例如，三峰）固定相的另外的（例如反相）官能团。

    UZM-39 ALUMINOSILICATE ZEOLITE
    7.
    发明申请
    UZM-39 ALUMINOSILICATE ZEOLITE 有权
    UZM-39铝酸钠沸石

    公开(公告)号：US20150025287A1

    公开(公告)日：2015-01-22

    申请号：US14507941

    申请日：2014-10-07

    Applicant: UOP LLC

    Inventor： Christopher P. Nicholas ,  Mark A. Miller

    IPC: B01J20/18 ,  B01J29/80 ,  B01J29/87 ,  C07C2/66

    CPC classification number: B01J43/00 ,  B01D15/08 ,  B01J20/18 ,  B01J29/70 ,  B01J29/80 ,  B01J29/86 ,  B01J29/87 ,  B01J29/88 ,  B01J35/002 ,  C01B39/023 ,  C01B39/46 ,  C01B39/48 ,  C07C2/66 ,  C07C2/76 ,  C07C7/13 ,  C07C2529/70 ,  C10G47/20

    Abstract: A new family of coherently grown composites of TUN and IMF zeotypes have been synthesized. These zeolites are represented by the empirical formula. NanMmk+TtAl1-xExSiyOz where “n” is the mole ratio of Na to (Al+E), M represents a metal or metals from zinc, Group 1, Group 2, Group 3 and or the lanthanide series of the periodic table, “m” is the mole ratio of M to (Al+E), “k” is the average charge of the metal or metals M, T is the organic structure directing agent or agents, and E is a framework element such as gallium. These zeolites are similar to TNU-9 and IM-5 but are characterized by unique compositions and synthesis procedures and have catalytic properties for carrying out various hydrocarbon conversion processes and separation properties for carrying out various separations.

    Abstract translation: 已经合成了一系列连续生长的TUN和IMF染色体型复合物。 这些沸石由经验公式表示。 NanMmk + TtAl1-xExSiyOz其中“n”是Na与（Al + E）的摩尔比，M表示来自锌，第1族，第2族，第3族和/或周期表的镧系的金属或金属， m“是M与（Al + E）的摩尔比，”k“是金属或金属M的平均电荷，T是有机结构导向剂或试剂，E是骨架元素如镓。 这些沸石类似于TNU-9和IM-5，但是其特征在于独特的组成和合成方法，并且具有用于进行各种烃转化方法和用于进行各种分离的分离性能的催化性能。

    PROCESS AND PLANT FOR TREATING WATER
    8.
    发明申请
    PROCESS AND PLANT FOR TREATING WATER 有权
    处理水处理和设备

    公开(公告)号：US20140263072A1

    公开(公告)日：2014-09-18

    申请号：US14289909

    申请日：2014-05-29

    Applicant: Clean TeQ Holdings Ltd.

    Inventor： Peter Voigt ,  Nikolai Zontov ,  John Carr

    IPC: C02F9/00 ,  C02F1/52 ,  C02F1/00 ,  C02F1/28

    CPC classification number: C02F1/004 ,  B01J39/05 ,  B01J39/07 ,  B01J41/05 ,  B01J41/07 ,  B01J43/00 ,  B01J45/00 ,  B01J47/018 ,  B01J49/06 ,  B01J49/07 ,  B01J49/53 ,  B01J49/57 ,  B01J49/70 ,  C02F1/28 ,  C02F1/42 ,  C02F1/52 ,  C02F1/5245 ,  C02F1/56 ,  C02F9/00 ,  C02F2303/16

    Abstract: A process for removing suspended particles and at least one ionic species from a feed water stream to produce a product water stream, the process includes the steps of forming agglomerates of the suspended particles in the feed water stream; passing the feed water stream containing agglomerated particles through a bed of particulate sorbent material so as to sorb the ionic species from the feed water onto the sorbent to provide a loaded sorbent and filter the agglomerated particles from the feed water using the bed of particulate sorbent material as a filtration medium to load the bed with the agglomerated particles, and thereby produce the product water stream; removing the filtered particles and the ionic species from the filtration medium; and re-using the regenerated sorbent in step b).

    Abstract translation: 一种从进料水流中除去悬浮颗粒和至少一种离子物质以产生产物水流的方法，该方法包括在进料水流中形成悬浮颗粒的附聚物的步骤; 使含有附聚颗粒的进料水流通过颗粒状吸附剂材料床，从而将来自进料水的离子物质吸附到吸附剂上以提供负载的吸附剂，并使用颗粒状吸附剂材料床将来自进料水的附聚颗粒过滤 作为过滤介质以使附聚的颗粒加载床，从而产生产物水流; 从过滤介质中除去过滤的颗粒和离子物质; 并在步骤b）中重新使用再生吸附剂。

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