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公开(公告)号：US07629413B2
公开(公告)日：2009-12-08
申请号：US11792034
申请日：2006-01-18
申请人： Allen David Godwin , Didier Naert
发明人： Allen David Godwin , Didier Naert
CPC分类号： C08K5/101 , C08K2201/014 , C08L27/06 , Y10T428/31504
摘要： C9 to C11 alkyl benzoates are used as plasticisers for polyvinyl chloride in particular in combination with plasticisers such as di-2-ethyl hexyl phthalate, diisononyl phthalate, di-2-propyl heptyl phthalate, diisodecyl phthalate or di-2-ethyl hexyl terephthalate. The use of the C9 to C11 alkyl benzoates provides low viscosity low volatility plasticisers, which are fast fusing with lower hot bench gelation temperature and which can be used to reduce the staining problems associated with use of di-2-ethyl hexyl phthalate and diisononyl phthalate. The low viscosity of the C9 to C11 alkyl benzoates allows the formulation of solvent free flexible PVC formulations meeting stringent VOC limitations.
摘要翻译： C9至C11烷基苯甲酸酯用作聚氯乙烯的增塑剂，特别是与增塑剂如邻苯二甲酸二-2-乙基己酯，邻苯二甲酸二异壬酯，邻苯二甲酸二-2-丙基庚酯，邻苯二甲酸二异癸酯或对苯二甲酸二-2-乙基己酯的增塑剂。 使用C9至C11烷基苯甲酸酯提供低粘度低挥发性增塑剂，其具有较低的热台凝胶化温度的快速熔融，并且可用于减少与邻苯二甲酸二-2-乙基己酯和邻苯二甲酸二异壬酯的使用相关的染色问题 。 C9至C11烷基苯甲酸酯的低粘度使配方的无溶剂柔性PVC配方满足严格的VOC限制。
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公开(公告)号：US20080275267A1
公开(公告)日：2008-11-06
申请号：US11911641
申请日：2006-05-24
申请人： Brady Compton , John Lyford , Nicolaas Anthony De Munck , Aad Gerrit Oskam , Allen David Godwin , Leendert Johannes Van Dop
发明人： Brady Compton , John Lyford , Nicolaas Anthony De Munck , Aad Gerrit Oskam , Allen David Godwin , Leendert Johannes Van Dop
IPC分类号： C07C67/58
CPC分类号： C07C67/56 , C07C2601/14 , C08K5/10 , Y02P20/582 , C07C69/44 , C07C69/80 , C07C69/78 , C07C69/76 , C07C69/60 , C07C69/75
摘要： Esters produced by the catalyzed reaction of alcohols and acids or anhydrides are neutralized by treatment with an aqueous alkaline alkali metal salt solution in an amount that provides less than a stoichiometric amount of alkali metal salt in relation to the acidity of the crude ester and the amount of water present during the treatment is from 0.8 to 1.4 wt % of water based on the weight of crude ester. When using titanium as the esterification catalyst, the ester resulting from this process contains less than 0.01 ppm by weight of titanium residue, so that it is storage stable when stored in the presence of an antioxidant.
摘要翻译： 通过醇和酸或酸酐的催化反应制备的酯通过用碱金属碱金属盐水溶液处理而中和，其量相对于粗酯的酸度提供小于化学计量量的碱金属盐， 在处理期间存在的水是基于粗酯重量的0.8至1.4重量％的水。 当使用钛作为酯化催化剂时，由该方法得到的酯含有小于0.01重量ppm的钛残基，因此在存在抗氧化剂时储存稳定。
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公开(公告)号：US06982295B2
公开(公告)日：2006-01-03
申请号：US10462354
申请日：2003-06-16
CPC分类号： H01B3/443 , C07C69/44 , C07C69/76 , C07C69/80 , C08K5/11 , C08K5/12 , Y10T428/294 , C08L27/06
摘要： Less branched C13 alcohols are used to provide plasticizer esters particularly suitable for high temperature applications such as wire and cable insulation.
摘要翻译： 较少支化的C 13醇用于提供特别适用于高温应用如电线和电缆绝缘的增塑剂酯。
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公开(公告)号：US5698747A
公开(公告)日：1997-12-16
申请号：US193202
申请日：1994-04-12
摘要： Ethers, for example those produced by acid-catalyzed dehydration of alcohols, are freed from esters by treatment with an alkoxide, and are especially suitable as drilling fluid components.
摘要翻译： PCT No.PCT / EP92 / 01875 Sec。 371日期1994年04月12日 102（e）日期1994年4月12日PCT提交1992年8月14日PCT公布。 出版物WO93 / 04028 日期1993年3月4日其他例如通过酸催化脱醇制得的那些，通过用醇盐处理而脱离酯，特别适合作为钻井液成分。
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25.发明授权Triglyceride plasticizers having low average levels of branching and process of making the same 失效具有低平均支化水平的甘油三酯增塑剂及其制备方法公开(公告)号：US08163825B2
公开(公告)日：2012-04-24
申请号：US12542407
申请日：2009-08-17
CPC分类号： C11C3/02 , C07C45/505 , C07C51/235 , C07C67/08 , C08K5/0016 , C08K5/10 , C08K5/103 , C07C47/02 , C07C53/128 , C07C69/30 , C08L91/00
摘要： Triglyceride PVC plasticizers can be produced by recovery of C5 to C10 aldehydes having low average levels of branching from a hydroformylation product, oxidizing the aldehydes with oxygen and/or air to form an acid, recovery of the resulting acid, and esterification with glycerol. Plasticizer compositions including such products or linear triglycerides combined with a secondary plasticizer and articles made therefrom are disclosed.
摘要翻译： 甘油三酯PVC增塑剂可以通过从加氢甲酰化产物中回收具有低平均支化水平的C5至C10醛来生产，用氧和/或空气氧化醛以形成酸，回收所得酸，并用甘油进行酯化。 公开了包含这些产物或直链甘油三酯与二级增塑剂和由其制成的制品的增塑剂组合物。
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公开(公告)号：US20110281987A1
公开(公告)日：2011-11-17
申请号：US13133317
申请日：2009-11-03
申请人： Allen David Godwin , Claudius Gosse
发明人： Allen David Godwin , Claudius Gosse
IPC分类号： C08K5/12
CPC分类号： C08K5/0016 , C08K5/12 , C08K2201/014
摘要： The invention is directed to plasticized compositions comprising esters of terephthalic acid, particularly PVC compositions.
摘要翻译： 本发明涉及包含对苯二甲酸酯，特别是PVC组合物的增塑组合物。
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公开(公告)号：US07667080B2
公开(公告)日：2010-02-23
申请号：US11632446
申请日：2005-07-14
IPC分类号： C07C31/125
CPC分类号： C07C69/80 , C07C31/125 , C07C43/11 , C07C305/06 , C08K5/05 , C08K5/10 , C11D1/146 , C11D1/29 , C11D1/72 , C11D3/2013 , C11D3/2017 , C11D3/202
摘要： Mixtures of C8-10 primary alcohols, preferably C9 alcohol rich, comprise from 15 to 70 wt. % unbranched molecules, the balance being branched molecules having an average branchiness of at most 2.00 branches per molecule, at least 80% of the ranches being methyl branches and at least 50% of the branched molecules being mono-methyl branched. Plasticiser esters and surfactant derivatives derived from these alcohol mixtures are also provided. The alcohol mixtures are preferably produced by hydroformylation of octene rich streams formed by Fischer-Tropsch synthesis.
摘要翻译： C8-10伯醇的混合物，优选C 9醇富含物，包含15至70wt。 ％的未分支的分子，其余为支化分子，每分子具有至多2.00个支链的平均分枝，至少80％的分枝是甲基支链，并且至少50％的支化分子是单甲基支链的。 还提供了源自这些醇混合物的增塑剂酯和表面活性剂衍生物。 醇混合物优选通过费 - 托合成形成的富含辛烯的流的加氢甲酰化产生。
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公开(公告)号：US06969735B1
公开(公告)日：2005-11-29
申请号：US10855105
申请日：2004-05-23
申请人： Allen David Godwin
发明人： Allen David Godwin
CPC分类号： C08K5/12 , Y10T428/294
摘要： Less branched C10 alcohols are used to provide plasticizer esters particularly suitable for high temperature applications such as wire and cable insulation.
摘要翻译： 较少支化的C 10醇用于提供特别适用于高温应用如电线电缆绝缘的增塑剂酯。
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