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    Method for producing carbonaceous film, and graphite film obtained by the same
    21.
    发明授权
    Method for producing carbonaceous film, and graphite film obtained by the same 有权
    制造碳质膜的方法和由其获得的石墨膜

    公开(公告)号：US08858847B2

    公开(公告)日：2014-10-14

    申请号：US13063419

    申请日：2009-09-11

    申请人： Takashi Inada ,  Yasushi Nishikawa ,  Makoto Mishiro

    发明人： Takashi Inada ,  Yasushi Nishikawa ,  Makoto Mishiro

    IPC分类号： C01B31/00 ,  C01B31/04

    CPC分类号： C01B31/02 ,  C01B32/05 ,  C01B32/20

    摘要： In a method for producing a carbonaceous film in which a polymer film is wrapped around a core and is subjected to a heat treatment, material film surfaces during the carbonization step are prevented from fusion, whereby a long carbonaceous having a large area film is obtained.Fusion can be prevented by subjecting a polymer film to a heat treatment under a reduced pressure, and under a reduced pressure while allowing an inert gas to flow. The range of the pressure reduction is preferably −0.08 MPa to −0.01 kPa. It is preferred to carry out carbonization with the pressure reduced in the range of from −0.08 MPa to −0.01 kPa while allowing an inert gas to flow. In addition, the polymer film wrapped around the core is placed in an outer casing, and provided that a value derived by dividing (internal diameter of the outer casing−diameter of the core) by 2 is designated as “a” (mm), and a thickness of wrapping of the polymer film is designated as “b” (mm), a value (b/a) derived by dividing the “b” by the “a” is set to fall within the range of from 0.2 to 0.9.

    摘要翻译： 在将聚合物膜缠绕在芯上并进行热处理的碳质膜的制造方法中，防止碳化工序中的材料膜表面熔融，得到面积大的膜的长碳素。 可以通过使聚合物膜在减压下进行热处理，并在减压下同时允许惰性气体流动来防止熔融。 减压的范围优选为-0.08MPa〜-0.01kPa。 优选在惰性气体流动的同时，将压力降低至-0.08MPa至-0.01kPa的压力进行碳化。 此外，包裹在芯体上的聚合物膜被放置在外壳中，并且将通过将芯部的外壳直径的内径除以2得到的值被指定为“a”（mm） 将聚合物膜的包裹厚度设为“b”（mm），将“b”除以“a”得到的值（b / a）设定为0.2〜0.9的范围 。

    METHOD FOR MANUFACTURING CARBONACEOUS FILM, AND GRAPHITE FILM OBTAINED THEREBY
    22.
    发明申请
    METHOD FOR MANUFACTURING CARBONACEOUS FILM, AND GRAPHITE FILM OBTAINED THEREBY 有权
    制造碳膜的方法和获得的石墨膜

    公开(公告)号：US20110169180A1

    公开(公告)日：2011-07-14

    申请号：US13063419

    申请日：2009-09-11

    申请人： Takashi Inada ,  Yasushi Nishikawa ,  Makoto Mishiro

    发明人： Takashi Inada ,  Yasushi Nishikawa ,  Makoto Mishiro

    IPC分类号： C01B31/00

    CPC分类号： C01B31/02 ,  C01B32/05 ,  C01B32/20

    摘要： In a method for producing a carbonaceous film in which a polymer film is wrapped around a core and is subjected to a heat treatment, material film surfaces during the carbonization step are prevented from fusion, whereby a long carbonaceous having a large area film is obtained.Fusion can be prevented by subjecting a polymer film to a heat treatment under a reduced pressure, and under a reduced pressure while allowing an inert gas to flow. The range of the pressure reduction is preferably −0.08 MPa to −0.01 kPa. It is preferred to carry out carbonization with the pressure reduced in the range of from −0.08 MPa to −0.01 kPa while allowing an inert gas to flow. In addition, the polymer film wrapped around the core is placed in an outer casing, and provided that a value derived by dividing (internal diameter of the outer casing−diameter of the core) by 2 is designated as “a” (mm), and a thickness of wrapping of the polymer film is designated as “b” (mm), a value (b/a) derived by dividing the “b” by the “a” is set to fall within the range of from 0.2 to 0.9.

    摘要翻译： 在将聚合物膜缠绕在芯上并进行热处理的碳质膜的制造方法中，防止碳化工序中的材料膜表面熔融，得到面积大的膜的长碳素。 可以通过使聚合物膜在减压下进行热处理，并在减压下同时允许惰性气体流动来防止熔融。 减压的范围优选为-0.08MPa〜-0.01kPa。 优选在惰性气体流动的同时，将压力降低至-0.08MPa至-0.01kPa的压力进行碳化。 此外，包裹在芯体上的聚合物膜被放置在外壳中，并且将通过将芯部的外壳直径的内径除以2得到的值被指定为“a”（mm） 将聚合物膜的包裹厚度设为“b”（mm），将“b”除以“a”得到的值（b / a）设定为0.2〜0.9的范围 。