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    Dumbbell-like nanoparticles and a process of forming the same
    21.
    发明授权
    Dumbbell-like nanoparticles and a process of forming the same 失效
    哑铃状纳米颗粒及其形成方法

    公开(公告)号：US07288134B2

    公开(公告)日：2007-10-30

    申请号：US10938897

    申请日：2004-09-10

    Applicant: Shouheng Sun ,  Heng Yu ,  Shan X. Wang

    Inventor： Shouheng Sun ,  Heng Yu ,  Shan X. Wang

    IPC: B22F1/02

    CPC classification number: C01G1/00 ,  B22F1/0022 ,  B22F1/0096 ,  B22F2999/00 ,  B82Y25/00 ,  B82Y30/00 ,  C01B17/20 ,  C01B19/007 ,  C01P2002/72 ,  C01P2002/84 ,  C01P2004/04 ,  C01P2004/30 ,  C01P2004/64 ,  C01P2004/80 ,  C01P2006/42 ,  C09C3/063 ,  H01F1/0054 ,  Y10S977/835 ,  B22F1/0018

    Abstract: Dumbbell-shaped or flower-shaped nanoparticles and a process of forming the same, wherein the process comprises forming a mixture of a nanoparticle with a precursor in a first solvent, wherein the nanoparticle comprises a hydrophobic outer coating; heating the mixture; cooling the mixture to room temperature; modifying the hydrophobic outer coating into a hydrophilic outer coating; precipitating a solid product from the mixture, and dispersing the product in a second solvent. The nanoparticles comprise any of a semiconducting, magnetic, and noble metallic material, wherein the nanoparticles comprise a first portion comprising any of PbSe, PbS, CdSe, CdS, ZnS, Au, Ag, Pd, and Pt, and wherein the precursor comprises any of a cationic, neutral or particulate Au, Ag, Pd, Pt, or transition metal (Fe, Co, Ni) precursors of Fe(CO)5, Co(CO)8, Ni(CO)4 or their analogues. The first and second solvents comprise any of alkanes, arenes, ethers, nitrites, ketones, and chlorinated hydrocarbons.

    Abstract translation: 哑铃形或花形纳米颗粒及其形成方法，其中所述方法包括在第一溶剂中形成纳米颗粒与前体的混合物，其中所述纳米颗粒包含疏水性外涂层; 加热混合物; 将混合物冷却至室温; 将疏水性外涂层改性为亲水性外涂层; 从混合物中沉淀出固体产物，并将产物分散在第二溶剂中。 纳米颗粒包括半导体，磁性和贵金属材料中的任何一种，其中纳米颗粒包括包含PbSe，PbS，CdSe，CdS，ZnS，Au，Ag，Pd和Pt中的任何一种的第一部分，并且其中前体包含任何 的阳离子，中性或微粒Au，Ag，Pd，Pt或过渡金属（Fe，Co，Ni）前体Fe（CO）5，Co（CO） （CO）4或它们的类似物。 第一和第二溶剂包括任何烷烃，芳烃，醚，亚硝酸盐，酮和氯代烃。

    Dumbbell-like nanoparticles and a process of forming the same
    23.
    发明申请
    Dumbbell-like nanoparticles and a process of forming the same 失效
    哑铃状纳米颗粒及其形成方法

    公开(公告)号：US20060053971A1

    公开(公告)日：2006-03-16

    申请号：US10938897

    申请日：2004-09-10

    Applicant: Shouheng Sun ,  Heng Yu ,  Shan Wang

    Inventor： Shouheng Sun ,  Heng Yu ,  Shan Wang

    IPC: B22F9/00

    CPC classification number: C01G1/00 ,  B22F1/0022 ,  B22F1/0096 ,  B22F2999/00 ,  B82Y25/00 ,  B82Y30/00 ,  C01B17/20 ,  C01B19/007 ,  C01P2002/72 ,  C01P2002/84 ,  C01P2004/04 ,  C01P2004/30 ,  C01P2004/64 ,  C01P2004/80 ,  C01P2006/42 ,  C09C3/063 ,  H01F1/0054 ,  Y10S977/835 ,  B22F1/0018

    Abstract: Dumbbell-shaped or flower-shaped nanoparticles and a process of forming the same, wherein the process comprises forming a mixture of a nanoparticle with a precursor in a first solvent, wherein the nanoparticle comprises a hydrophobic outer coating; heating the mixture; cooling the mixture to room temperature; modifying the hydrophobic outer coating into a hydrophilic outer coating; precipitating a solid product from the mixture, and dispersing the product in a second solvent. The nanoparticles comprise any of a semiconducting, magnetic, and noble metallic material, wherein the nanoparticles comprise a first portion comprising any of PbSe, PbS, CdSe, CdS, ZnS, Au, Ag, Pd, and Pt, and wherein the precursor comprises any of a cationic, neutral or particulate Au, Ag, Pd, Pt, or transition metal (Fe, Co, Ni) precursors of Fe(CO)5, Co(CO)8, Ni(CO)4 or their analogues. The first and second solvents comprise any of alkanes, arenes, ethers, nitrites, ketones, and chlorinated hydrocarbons.

    Abstract translation: 哑铃形或花形纳米颗粒及其形成方法，其中所述方法包括在第一溶剂中形成纳米颗粒与前体的混合物，其中所述纳米颗粒包含疏水外涂层; 加热混合物; 将混合物冷却至室温; 将疏水性外涂层改性为亲水性外涂层; 从混合物中沉淀出固体产物，并将产物分散在第二溶剂中。 纳米颗粒包括半导体，磁性和贵金属材料中的任何一种，其中纳米颗粒包括包含PbSe，PbS，CdSe，CdS，ZnS，Au，Ag，Pd和Pt中的任何一种的第一部分，并且其中前体包含任何 的阳离子，中性或微粒Au，Ag，Pd，Pt或过渡金属（Fe，Co，Ni）前体Fe（CO）5，Co（CO） （CO）4或它们的类似物。 第一和第二溶剂包括任何烷烃，芳烃，醚，亚硝酸盐，酮和氯代烃。

    Method and apparatus for linking and/or patterning self-assembled objects
    24.
    发明授权
    Method and apparatus for linking and/or patterning self-assembled objects 失效
    用于连接和/或构图自组装物体的方法和装置

    公开(公告)号：US06866898B2

    公开(公告)日：2005-03-15

    申请号：US10341805

    申请日：2003-01-14

    Applicant: John E. E. Baglin ,  Hendrik F. Hamann ,  Shouheng Sun

    Inventor： John E. E. Baglin ,  Hendrik F. Hamann ,  Shouheng Sun

    IPC: G03F7/038 ,  G03F7/16 ,  G11B5/855 ,  B05D3/06

    CPC classification number: B82Y30/00 ,  G03F7/038 ,  G03F7/165 ,  G11B5/855 ,  Y10S977/901

    Abstract: A method and related apparatus to link and/or pattern self-assembled first objects to a second object. Each of the first object (e.g., a nanoparticle) can be embedded in a mobile binder (i.e., a stabilizer). The invention applies energy to the first object and stabilizer, links this first object to the second object, and provides a controlled linkage of the first object with respect to the second object. Applying this procedure to many such objects results in a larger a real arrangement of these linked objects. An appropriate solvent may be used to remove non-linked objects, yielding a patterned array. Thermal annealing can be applied to control the physical and chemical properties of the array.

    Abstract translation: 将自组装的第一物体链接和/或图案化为第二物体的方法和相关装置。 第一物体（例如，纳米颗粒）中的每一个可以嵌入移动的粘合剂（即稳定剂）中。 本发明将能量应用于第一物体和稳定器，将该第一物体与第二物体相连，并且提供第一物体相对于第二物体的受控连杆。 将此过程应用于许多这样的对象导致这些链接的对象的更大的真实布置。 可以使用合适的溶剂来除去未连接的物体，产生图案化的阵列。 可以应用热退火来控制阵列的物理和化学性质。

    Process of making metal containing iron oxide and iron sulfide based nanoparticle materials
    28.
    发明申请
    Process of making metal containing iron oxide and iron sulfide based nanoparticle materials 有权
    制备含有氧化铁和硫化铁的纳米颗粒材料的方法

    公开(公告)号：US20070056401A1

    公开(公告)日：2007-03-15

    申请号：US11511715

    申请日：2006-08-29

    Applicant: Shouheng Sun

    Inventor： Shouheng Sun

    IPC: B22F9/18

    CPC classification number: C04B35/628 ,  B22F1/0018 ,  B22F1/02 ,  B22F9/24 ,  B22F2998/00 ,  B22F2999/00 ,  B82Y25/00 ,  B82Y30/00 ,  C01G49/08 ,  C01G49/12 ,  C01P2002/72 ,  C01P2004/04 ,  C01P2004/64 ,  C01P2006/42 ,  C04B35/62826 ,  C04B35/62828 ,  C04B2235/3272 ,  C04B2235/3274 ,  C04B2235/5454 ,  C09C1/24 ,  C09C1/3054 ,  C09C3/063 ,  H01F1/0054 ,  Y10S977/773 ,  Y10S977/811

    Abstract: A method and structure for making magnetite nanoparticle materials by mixing iron salt with alcohol, carboxylic acid and amine in an organic solvent and heating the mixture to 200-360° C. is described. The size of the particles can be controlled either by changing the iron salt to acid/amine ratio or by coating small nanoparticles with more iron oxide. Magnetite nanoparticles in the size ranging from 2 nm to 20 nm with a narrow size distribution are obtained with the invention. The invention can be readily extended to other iron oxide based nanoparticle materials, including M Fe2O4 (M=Co, Ni, Cu, Zn, Cr, Ti, Ba, Mg) nanomaterials, and iron oxide coated nanoparticle materials. The invention also leads to the synthesis of iron sulfide based nanoparticle materials by replacing alcohol with thiol in the reaction mixture. The magnetite nanoparticles can be oxidized to γ-Fe2O3, or α-Fe2O3, or can be reduced to bcc-Fe nanoparticles, while iron oxide based materials can be used to make binary iron based metallic nanoparticles, such as CoFe, NiFe, and FeCoSmx nanoparticles.

    Abstract translation: 描述了通过在有机溶剂中将铁盐与醇，羧酸和胺混合并将混合物加热至200-360℃来制备磁铁矿纳米颗粒材料的方法和结构。 颗粒的大小可以通过将铁盐改变成酸/胺的比例或通过用更多的氧化铁涂覆小的纳米颗粒来控制。 通过本发明获得尺寸范围为2nm至20nm且具有窄尺寸分布的磁铁矿纳米颗粒。 本发明可以容易地扩展到其它基于氧化铁的纳米颗粒材料，包括M Fe 2 O 4（M = Co，Ni，Cu，Zn，Cr，Ti，Ba ，Mg）纳米材料和氧化铁涂覆的纳米颗粒材料。 本发明还导致通过在反应混合物中用硫醇代替醇来合成基于硫化铁的纳米颗粒材料。 磁铁矿纳米粒子可被氧化成γ-Fe 2 O 3 3或α-Fe 2 O 3 3， 或者可以还原成bcc-Fe纳米颗粒，而基于氧化铁的材料可用于制备二元铁基金属纳米颗粒，例如CoFe，NiFe和FeCoSm纳米颗粒。

    Method and apparatus for linking and/or patterning self-assembled objects
    29.
    发明授权
    Method and apparatus for linking and/or patterning self-assembled objects 有权
    用于连接和/或构图自组装物体的方法和装置

    公开(公告)号：US06566665B2

    公开(公告)日：2003-05-20

    申请号：US09930979

    申请日：2001-08-17

    Applicant: John E. E. Baglin ,  Hendrik F. Hamann ,  Shouheng Sun

    Inventor： John E. E. Baglin ,  Hendrik F. Hamann ,  Shouheng Sun

    IPC: H01J3730

    CPC classification number: B82Y30/00 ,  G03F7/038 ,  G03F7/165 ,  G11B5/855 ,  Y10S977/901

    Abstract: The invention provides a method and related apparatus to link and/or pattern self-assembled first objects to a second object. Each of the first object (e.g., a nanoparticle) can be embedded in a mobile binder (i.e., a stabilizer). The invention applies energy to the first object and stabilizer, links this first object to the second object, and provides a controlled linkage of the first object with respect to the second object. Applying this procedure to many such objects results in a larger areal arrangement of these linked objects. An appropriate solvent may be used to remove non-linked objects, yielding a patterned array. Thermal annealing can be applied to control the physical and chemical properties of the array.

    Abstract translation: 本发明提供一种方法和相关装置，用于将自组装的第一物体链接和/或图案化为第二物体。 第一物体（例如，纳米颗粒）中的每一个可以嵌入移动的粘合剂（即稳定剂）中。 本发明将能量应用于第一物体和稳定器，将该第一物体与第二物体相连，并且提供第一物体相对于第二物体的受控连杆。 将此过程应用于许多这样的对象导致这些链接对象的更大的面积排列。 可以使用合适的溶剂来除去未连接的物体，产生图案化的阵列。 可以应用热退火来控制阵列的物理和化学性质。

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