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21.
公开(公告)号:US20090301387A1
公开(公告)日:2009-12-10
申请号:US12133364
申请日:2008-06-05
Applicant: MARK P. D'EVELYN
Inventor: MARK P. D'EVELYN
IPC: C30B19/08
CPC classification number: C30B29/406 , B01J3/008 , B01J3/042 , B01J3/065 , B01J2203/0665 , B01J2203/067 , B01J2203/068 , B30B11/005 , C30B7/10 , C30B29/403 , Y02P20/544 , Y10T117/10 , Y10T117/1024 , Y10T117/1096
Abstract: A high pressure apparatus and related methods for processing supercritical fluids. In a specific embodiment, the present apparatus includes a capsule, a heater, at least one ceramic ring but can be multiple rings, optionally, with one or more scribe marks and/or cracks present. In a specific embodiment, the apparatus optionally has a metal sleeve containing each ceramic ring. The apparatus also has a high-strength enclosure, end flanges with associated insulation, and a power control system. IN a specific embodiment, the apparatus is capable of accessing pressures and temperatures of 0.2-2 GPa and 400-1200° C., respectively.
Abstract translation: 一种用于加工超临界流体的高压装置及相关方法。 在具体实施例中,本装置包括胶囊,加热器,至少一个陶瓷环,但可以是多个环,任选地,存在一个或多个划痕和/或裂纹。 在具体实施例中,该装置可选地具有包含每个陶瓷环的金属套筒。 该设备还具有高强度外壳,具有相关绝缘的端部法兰和电源控制系统。 在具体实施例中,该装置能够分别访问0.2-2GPa和400-1200℃的压力和温度。
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公开(公告)号:US20030185740A1
公开(公告)日:2003-10-02
申请号:US10402434
申请日:2003-03-28
Applicant: National Cheng Kung University
Inventor: Shyan-Lung Chung , Chun-Nan Lin , Jen-Chang Chen , Zheng-Xiuo Lin , Jing-Yuan Liu
IPC: C01B021/072 , C23C016/00
CPC classification number: B01J3/04 , B01J19/006 , B01J19/02 , B01J2203/067 , B01J2219/0002 , B01J2219/00063 , B01J2219/00065 , B01J2219/00135 , B01J2219/00153 , B01J2219/00777 , B01J2219/0277 , C01B21/0722 , C01P2002/72 , C01P2006/10 , C01P2006/60 , C01P2006/80
Abstract: A method and an apparatus for preparing aluminum nitride are disclosed. The method includes the steps of (a) providing an aluminum container, (b) providing a reactant to be received in the aluminum container, and proceeding at least one step selected from a group consisting of step (b1), step (b2) and a combination thereof, (c) placing the aluminum container into a reactor with a specific pressure and introducing nitrogen gas into the reactor, and (d) heating the reactant at a specific temperature till igniting, thereby preparing the aluminum nitride. The step (b1) is placing a layer of an aluminum nitride powder between the reactant and the aluminum container, and the step (b2) is perpendicularly placing at least one aluminum pipe into the reactant.
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