公开(公告)号：US20170037688A1

公开(公告)日：2017-02-09

申请号：US15297882

申请日：2016-10-19

Applicant: Baker Hughes Incorporated

Inventor： Valery N. Khabashesku ,  Vladimir P. Filonenko

IPC: E21B10/567 ,  B24D3/06 ,  B24D18/00

CPC classification number: E21B10/567 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/0685 ,  B24D3/06 ,  B24D18/0009

Abstract: A polycrystalline compact includes diamond, cubic boron nitride, and at least one hard material, which may be aluminum nitride, gallium nitride, silicon nitride, titanium nitride, silicon carbide, titanium carbide, titanium boride, titanium diboride, and/or aluminum boride. The diamond, the cubic boron nitride, and the hard material are intermixed and interbonded to form a polycrystalline material. An earth-boring tool includes a bit body and a polycrystalline diamond compact secured to the bit body. Methods of fabricating polycrystalline compacts include forming a mixture comprising diamond, non-cubic boron nitride, and a metal or semimetal; encapsulating the mixture in a container; and subjecting the encapsulated mixture to high-pressure and high-temperature conditions to form a polycrystalline material.

Abstract translation: 多晶结构体包括金刚石，立方氮化硼和至少一种硬质材料，其可以是氮化铝，氮化镓，氮化硅，氮化钛，碳化硅，碳化钛，硼化钛，二硼化钛和/或硼化铝。 将金刚石，立方氮化硼和硬质材料混合并键合以形成多晶材料。 钻孔工具包括固定在钻头体上的钻头体和多晶金刚石块。 制造多晶压块的方法包括形成包含金刚石，非立方氮化硼和金属或半金属的混合物; 将混合物包封在容器中; 并将包封的混合物经受高压和高温条件以形成多晶材料。

公开(公告)号：US20020122757A1

公开(公告)日：2002-09-05

申请号：US09946118

申请日：2001-09-04

Applicant: National Cheng Kung University

Inventor： Shyan-Lung Chung ,  Chun-Nan Lin ,  Jen-Chang Chen ,  Zheng-Xiuo Lin ,  Jing-Yuan Liu

IPC: C01B021/072 ,  F28D021/00 ,  G05D023/19 ,  G05D016/00

CPC classification number: B01J3/04 ,  B01J19/006 ,  B01J19/02 ,  B01J2203/067 ,  B01J2219/0002 ,  B01J2219/00063 ,  B01J2219/00065 ,  B01J2219/00135 ,  B01J2219/00153 ,  B01J2219/00777 ,  B01J2219/0277 ,  C01B21/0722 ,  C01P2002/72 ,  C01P2006/10 ,  C01P2006/60 ,  C01P2006/80

Abstract: A method and an apparatus for preparing aluminum nitride are disclosed. The method includes the steps of (a) providing an aluminum container, (b) providing a reactant to be received in the aluminum container, and proceeding at least one step selected from a group consisting of step (b1), step (b2) and a combination thereof, (c) placing the aluminum container into a reactor with a specific pressure and introducing nitrogen gas into the reactor, and (d) heating the reactant at a specific temperature till igniting, thereby preparing the aluminum nitride. The step (b1) is placing a layer of an aluminum nitride powder between the reactant and the aluminum container, and the step (b2) is perpendicularly placing at least one aluminum pipe into the reactant.

Abstract translation: 公开了一种制备氮化铝的方法和装置。 该方法包括以下步骤：（a）提供铝容器，（b）提供待容纳在铝容器中的反应物，并且进行至少一个选自步骤（b1），步骤（b2）和 其组合，（c）将铝容器放入具有特定压力的反应器中并将氮气引入反应器中，和（d）在特定温度下加热反应物直到点燃，由此制备氮化铝。 步骤（b1）在反应物和铝容器之间放置一层氮化铝粉末，步骤（b2）将至少一个铝管垂直放置在反应物中。

公开(公告)号：US09498867B2

公开(公告)日：2016-11-22

申请号：US14090018

申请日：2013-11-26

Applicant: Baker Hughes Incorporated

Inventor： Valery N. Khabashesku ,  Vladimir P. Filonenko

IPC: E21B10/56 ,  B22F3/14 ,  B24D18/00 ,  B24D3/06 ,  E21B10/567

CPC classification number: E21B10/567 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/0685 ,  B24D3/06 ,  B24D18/0009

Abstract: A polycrystalline compact includes diamond grains, cubic boron nitride grains, and grains of an additional nitride, carbide, or boride. The additional nitride, carbide, or boride may be aluminum nitride, gallium nitride, silicon nitride, titanium nitride, silicon carbide, titanium carbide, titanium boride, titanium diboride, and/or aluminum boride. The diamond grains, the cubic boron nitride grains, and the grains of the additional nitride, carbide, or boride are intermixed and interbonded to form a polycrystalline material. An earth-boring tool includes a bit body and a polycrystalline diamond compact secured to the bit body. Methods of fabricating polycrystalline compacts include forming a mixture comprising diamond grains, non-cubic boron nitride grains, and a metal or semimetal; encapsulating the mixture in a container; and subjecting the encapsulated mixture to high-pressure and high-temperature conditions to form a polycrystalline material.

Abstract translation: 多晶压块包括金刚石晶粒，立方氮化硼晶粒和另外的氮化物，碳化物或硼化物的晶粒。 另外的氮化物，碳化物或硼化物可以是氮化铝，氮化镓，氮化硅，氮化钛，碳化硅，碳化钛，硼化钛，二硼化钛和/或硼化铝。 金刚石晶粒，立方氮化硼晶粒和附加氮化物，碳化物或硼化物的晶粒混合并键合以形成多晶材料。 钻孔工具包括固定在钻头体上的钻头体和多晶金刚石块。 制造多晶压块的方法包括形成包含金刚石晶粒，非立方氮化硼晶粒和金属或半金属的混合物; 将混合物包封在容器中; 并将包封的混合物经受高压和高温条件以形成多晶材料。

公开(公告)号：US20110183498A1

公开(公告)日：2011-07-28

申请号：US13013697

申请日：2011-01-25

Applicant: Mark P. D'Evelyn

Inventor： Mark P. D'Evelyn

IPC: H01L21/20 ,  C30B7/02 ,  C30B7/08

CPC classification number: B01J3/008 ,  B01J3/042 ,  B01J3/065 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/068 ,  C30B7/10 ,  C30B29/403 ,  C30B29/406 ,  Y02P20/544 ,  Y10T117/1004 ,  Y10T117/1024

Abstract: An improved high pressure apparatus and methods for processing supercritical fluids is described. The apparatus includes a capsule, a heater, and at least one ceramic ring contained by a metal sleeve. The apparatus is capable of accessing pressures and temperatures of 0.2-2 GPa and 400-1200° C.

Abstract translation: 描述了改进的高压装置和用于处理超临界流体的方法。 该装置包括胶囊，加热器和由金属套筒包含的至少一个陶瓷环。 该设备能够获得0.2-2GPa和400-1200℃的压力和温度。

公开(公告)号：US20030140845A1

公开(公告)日：2003-07-31

申请号：US09683658

申请日：2002-01-31

Applicant: General Electric Company

Inventor： Mark Philip D'Evelyn ,  Kristi Jean Narang ,  Robert Arthur Giddings ,  Robert Vincent Leonelli JR. ,  Stephen Lee Dole

IPC: C30B001/00 ,  C30B003/00 ,  C30B005/00 ,  C30B028/02 ,  C30B007/00 ,  C30B021/02 ,  C30B028/06

CPC classification number: B01J19/006 ,  B01J3/062 ,  B01J19/0013 ,  B01J19/0073 ,  B01J19/02 ,  B01J2203/067 ,  B01J2219/00063 ,  B01J2219/00094 ,  B01J2219/00135 ,  B01J2219/0236 ,  B01J2219/0277 ,  B01J2219/1943 ,  C30B7/00

Abstract: A pressure vessel for processing at least one material in a supercritical fluid. The pressure vessel includes a self-pressurizing capsule for containing at least one material and the supercritical fluid in a substantially air-free environment, a pressure transmission medium surrounding the capsule for maintaining an outer pressure on the capsule, at least one heating element insertable in the pressure transmission medium such that the heating element surrounds the capsule, a temperature measurement means for measuring a temperature of the capsule, a temperature controller for controlling the temperature and providing power to the heating element, a restraint to contain and hold in place the capsule, the pressure transmission medium, and the heating element, and at least one seal between the restraint and the pressure transmission medium for preventing escape of the pressure transmission medium. Methods of using the pressure vessel, processing a material at high temperature and high pressure in the presence of a supercritical fluid within the capsule are also described.

Abstract translation: 用于处理超临界流体中的至少一种材料的压力容器。 压力容器包括用于在基本无空气环境中容纳至少一种材料和超临界流体的自加压胶囊，围绕胶囊的压力传递介质，用于保持胶囊上的外部压力，至少一个加热元件可插入 所述压力传递介质使得所述加热元件围绕所述胶囊，用于测量所述胶囊的温度的温度测量装置，用于控制所述温度并为所述加热元件提供电力的温度控制器，限制所述胶囊 压力传递介质和加热元件，以及限制器和压力传递介质之间的至少一个密封件，用于防止压力传递介质的逸出。 还描述了使用压力容器，在胶囊内的超临界流体存在下在高温高压下处理材料的方法。

公开(公告)号：US08986447B2

公开(公告)日：2015-03-24

申请号：US13343563

申请日：2012-01-04

Applicant: Mark P. D'Evelyn

Inventor： Mark P. D'Evelyn

IPC: C30B7/10 ,  C30B29/40 ,  B01J3/00 ,  B01J3/04 ,  B01J3/06 ,  B30B11/00

CPC classification number: C30B29/406 ,  B01J3/008 ,  B01J3/042 ,  B01J3/065 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/068 ,  B30B11/005 ,  C30B7/10 ,  C30B29/403 ,  Y02P20/544 ,  Y10T117/10 ,  Y10T117/1024 ,  Y10T117/1096

Abstract: A high pressure apparatus and related methods for processing supercritical fluids. In a specific embodiment, the present apparatus includes a capsule, a heater, at least one ceramic ring but can be multiple rings, optionally, with one or more scribe marks and/or cracks present. In a specific embodiment, the apparatus optionally has a metal sleeve containing each ceramic ring. The apparatus also has a high-strength enclosure, end flanges with associated insulation, and a power control system. In a specific embodiment, the apparatus is capable of accessing pressures and temperatures of 0.2-2 GPa and 400-1200° C., respectively.

Abstract translation: 一种用于加工超临界流体的高压装置及相关方法。 在具体实施例中，本装置包括胶囊，加热器，至少一个陶瓷环，但可以是多个环，任选地，存在一个或多个划痕和/或裂纹。 在具体实施例中，该装置可选地具有包含每个陶瓷环的金属套筒。 该设备还具有高强度外壳，具有相关绝缘的端部法兰和电源控制系统。 在具体实施例中，该装置能够分别访问0.2-2GPa和400-1200℃的压力和温度。

公开(公告)号：US08871024B2

公开(公告)日：2014-10-28

申请号：US13013697

申请日：2011-01-25

Applicant: Mark P. D'Evelyn

Inventor： Mark P. D'Evelyn

IPC: C30B7/08 ,  B01J3/06 ,  B01J3/04 ,  B01J3/00 ,  C30B29/40 ,  C30B7/10

CPC classification number: B01J3/008 ,  B01J3/042 ,  B01J3/065 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/068 ,  C30B7/10 ,  C30B29/403 ,  C30B29/406 ,  Y02P20/544 ,  Y10T117/1004 ,  Y10T117/1024

Abstract: An improved high pressure apparatus and methods for processing supercritical fluids is described. The apparatus includes a capsule, a heater, and at least one ceramic ring contained by a metal sleeve. The apparatus is capable of accessing pressures and temperatures of 0.2-2 GPa and 400-1200° C.

Abstract translation: 描述了改进的高压装置和用于处理超临界流体的方法。 该装置包括胶囊，加热器和由金属套筒包含的至少一个陶瓷环。 该设备能够获得0.2-2GPa和400-1200℃的压力和温度。

公开(公告)号：US20120118223A1

公开(公告)日：2012-05-17

申请号：US13343563

申请日：2012-01-04

Applicant: Mark P. D'Evelyn

Inventor： Mark P. D'Evelyn

IPC: C30B7/10

CPC classification number: C30B29/406 ,  B01J3/008 ,  B01J3/042 ,  B01J3/065 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/068 ,  B30B11/005 ,  C30B7/10 ,  C30B29/403 ,  Y02P20/544 ,  Y10T117/10 ,  Y10T117/1024 ,  Y10T117/1096

Abstract: A high pressure apparatus and related methods for processing supercritical fluids. In a specific embodiment, the present apparatus includes a capsule, a heater, at least one ceramic ring but can be multiple rings, optionally, with one or more scribe marks and/or cracks present. In a specific embodiment, the apparatus optionally has a metal sleeve containing each ceramic ring. The apparatus also has a high-strength enclosure, end flanges with associated insulation, and a power control system. In a specific embodiment, the apparatus is capable of accessing pressures and temperatures of 0.2-2 GPa and 400-1200° C., respectively.

Abstract translation: 一种用于加工超临界流体的高压装置及相关方法。 在具体实施例中，本装置包括胶囊，加热器，至少一个陶瓷环，但可以是多个环，任选地，存在一个或多个划痕和/或裂纹。 在具体实施例中，该装置可选地具有包含每个陶瓷环的金属套筒。 该设备还具有高强度外壳，具有相关绝缘的端部法兰和电源控制系统。 在具体实施例中，该装置能够分别访问0.2-2GPa和400-1200℃的压力和温度。

公开(公告)号：US20040000266A1

公开(公告)日：2004-01-01

申请号：US10455007

申请日：2003-06-05

Inventor： Mark Philip D'Evelyn ,  Thomas Richard Anthony ,  Stephen Daley Arthur ,  Lionel Monty Levinson ,  John William Lucek ,  Larry Burton Rowland ,  Suresh Shankarappa Vagarali

IPC: C30B001/00

CPC classification number: B01J3/065 ,  B01J3/062 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/066 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/0675 ,  B01J2203/069 ,  C30B33/00 ,  Y10T117/1004 ,  Y10T117/1008

Abstract: A method for removing defects at high pressure and high temperature (HP/HT) or for relieving strain in a non-diamond crystal commences by providing a crystal, which contains defects, and a pressure medium. The crystal and the pressure medium are disposed in a high pressure cell and placed in a high pressure apparatus, for processing under reaction conditions of sufficiently high pressure and high temperature for a time adequate for one or more of removing defects or relieving strain in the single crystal.

Abstract translation: 通过提供含有缺陷的晶体和压力介质，开始在高压高温（HP / HT）下除去非金刚石晶体中的缺陷或解除应变的方法。 将晶体和压力介质设置在高压电池中并放置在高压设备中，用于在足够高的压力和高温的反应条件下进行处理足够的时间以适应一个或多个去除缺陷或减轻单一应变的应变 水晶。

公开(公告)号：US6129900A

公开(公告)日：2000-10-10

申请号：US307493

申请日：1994-09-16

Applicant: Shuichi Satoh ,  Hitoshi Sumiya ,  Kazuwo Tsuji ,  Yasushi Gouda

Inventor： Shuichi Satoh ,  Hitoshi Sumiya ,  Kazuwo Tsuji ,  Yasushi Gouda

IPC: B01J3/06

CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/0655 ,  B01J2203/067 ,  B01J2203/068

Abstract: A colorless and transparent, substantially inclusion-free diamond crystal which can be applied to decorative uses and optical parts is synthesized by a process using a temperature gradient method in an ultra-high pressure apparatus. This process comprises using, as a solvent for the growth of the crystal, at least one metal selected from the group consisting of Fe, Co, Ni, Mn and Cr (at least two metals in the case of containing Fe) and as a nitrogen getter for the removal of nitrogen in the solvent, at least one metal selected from the group consisting of Al, Ti, Zr, Hf, V, Nb and Ta in a proportion of 0.5 to 7% by weight (at most 2% by weight when using only Al) to the solvent metal.

Abstract translation: PCT No.PCT / JP92 / 00149 Sec。 371日期：1992年10月14日 102（e）日期1992年10月14日PCT提交1992年2月14日PCT公布。 公开号WO92 / 14542 日期1992年9月3日可以应用于装饰用途和光学部件的无色透明的基本上不含夹杂的金刚石晶体通过在超高压装置中使用温度梯度法的方法合成。 该方法包括使用选自Fe，Co，Ni，Mn和Cr中的至少一种金属作为晶体生长的溶剂（在含有Fe的情况下至少有两种金属）和作为氮 吸附剂用于除去溶剂中的氮，至少一种选自Al，Ti，Zr，Hf，V，Nb和Ta的金属，其含量为0.5〜7重量％（最多2重量％ 当仅使用Al时）溶剂金属。