Method and an apparatus for recovering chemicals from an alkaline lignin material

    公开(公告)号:US11407778B2

    公开(公告)日:2022-08-09

    申请号:US16461202

    申请日:2017-11-14

    Abstract: In a method and an apparatus for recovering chemicals from an alkaline lignin material, the alkaline lignin material (3) which comprises NaOH or KOH is precipitated in presence of an acid in a precipitation stage (6) for forming a precipitated lignin (7), the precipitated lignin (7) is supplied to a separation stage (8) in which a purified lignin (9) is recovered and from which at least one fraction (10) which comprises Na or K is supplied to a crystallization stage (11), and the fraction (10) which comprises Na or K is treated by crystallization in the crystallization stage (11) for forming a crystallized compound (12). Further, the invention relates to use of the purified lignin, and lignin and chemical products.

    Method for producing nanofibrillar cellulose and nanofibrillar cellulose product

    公开(公告)号:US11274396B2

    公开(公告)日:2022-03-15

    申请号:US15930962

    申请日:2020-05-13

    Abstract: In a method for producing nanofibrillar cellulose, cellulose based fibre material, in which internal bonds in cellulose fibres have been weakened by 5 preliminary modification of cellulose, is subjected to disintegration treatment in form of pulp comprising fibres and liquid. The fibre material is supplied at a consistency higher than 10 wt-%, preferably at least 15 wt-%, to a disintegration treatment where fibrils are detached from the fibre material by joint effect of repeated impacts to the fibre material by fast moving 10 successive elements and the weakened internal bonds of the cellulose fibres. The nanofibrillar cellulose is withdrawn from the disintegration treatment at dry matter which is equal or higher than the consistency of the fibre material.

    METHOD AND AN APPARATUS FOR AN ENZYMATIC HYDROLYSIS, A LIQUID FRACTION AND A SOLID FRACTION

    公开(公告)号:US20210371890A1

    公开(公告)日:2021-12-02

    申请号:US17326442

    申请日:2021-05-21

    Abstract: In a method and an apparatus for an enzymatic hydrolysis in which plant based raw material is hydrolysed by means of enzymes in at least one enzymatic hydrolysis stage. A plant based feed (1) is fed to the enzymatic hydrolysis stage (2) in which the plant based feed is hydrolysed. A liquid fraction (3) comprising carbohydrates is separated from a solid fraction (4) in a solid-liquid separation stage (11). At least a part (5) of the solid fraction (4) comprising enzymes is recirculated to the plant based feed (1) of the enzymatic hydrolysis stage (2) or to the enzymatic hydrolysis stage (2), and a rest part (6) of the solid fraction (4) is recovered. Further, the invention relates to the liquid fraction and the solid fraction and their use.

    A METHOD AND AN APPARATUS FOR AN ENZYMATIC HYDROLYSIS, A LIQUID FRACTION AND A SOLID FRACTION

    公开(公告)号:US20190127771A1

    公开(公告)日:2019-05-02

    申请号:US16305924

    申请日:2017-06-01

    Abstract: In a method and an apparatus for an enzymatic hydrolysis in which plant based raw material is hydrolysed by means of enzymes in at least one enzymatic hydrolysis stage. A plant based feed (1) is fed to the enzymatic hydrolysis stage (2) in which the plant based feed is hydrolysed. A liquid fraction (3) comprising carbohydrates is separated from a solid fraction (4) in a solid-liquid separation stage (11). At least a part (5) of the solid fraction (4) comprising enzymes is recirculated to the plant based feed (1) of the enzymatic hydrolysis stage (2) or to the enzymatic hydrolysis stage (2), and a rest part (6) of the solid fraction (4) is recovered. Further, the invention relates to the liquid fraction and the solid fraction and their use.

    Method for producing nanofibrillar cellulose

    公开(公告)号:US09739011B2

    公开(公告)日:2017-08-22

    申请号:US14357706

    申请日:2012-11-14

    CPC classification number: D21D1/20 B02C13/205 D21D1/36

    Abstract: In a method for producing nanofibril cellulose, cellulose based fiber material, in which internal bonds in the cellulose fiber have been weakened by chemical modification, are supplied, for separating fibrils, through several counter-rotating rotors outwards in the radial direction with respect to the rotation axis of the rotors in such a way that the material is repeatedly subjected to shearing and impacting forces by the effect of the blades of the different counter-rotating rotors, whereby it is simultaneously fibrillated.

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