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    Synthetic polymer particles for use as standards and calibrators in flow cytometry
    41.
    发明授权
    Synthetic polymer particles for use as standards and calibrators in flow cytometry 失效
    合成聚合物颗粒，用作流式细胞仪中的标准品和校准品

    公开(公告)号：US6074879A

    公开(公告)日：2000-06-13

    申请号：US099233

    申请日：1998-06-17

    Applicant: David Zelmanovic ,  William Moskalski ,  Ronny DeClercq ,  Frank Louwet ,  Eberhard Kuckert ,  Wolfgang Podszun

    Inventor： David Zelmanovic ,  William Moskalski ,  Ronny DeClercq ,  Frank Louwet ,  Eberhard Kuckert ,  Wolfgang Podszun

    IPC: G01N33/49 ,  G01N15/00 ,  G01N15/10 ,  G01N15/14 ,  G01N31/00

    CPC classification number: G01N15/1012 ,  G01N2015/1062 ,  G01N2015/1486 ,  G01N2015/149 ,  Y10T436/10 ,  Y10T436/101666

    Abstract: The invention describes novel methods for calibrating or standardizing flow cytometry instruments using synthetic polymer particles or beads having physical properties which provide advantages for their use in such instruments. The polymer particles or beads employed in the calibration methods are spherical, have an average particle diameter of from about 1 to about 8 microns, a relatively narrow particle distribution, and a low refractive index, i.e., from about 1.35 to about 1.45. The particles are safe, stable for long time periods and are particularly suitable for employment as hematology analyzer calibration substances. The invention provides an advantageous improvement over the types of standards currently used to calibrate a variety of instruments that rely on light scatter combined with other parameters to identify and measure biological particles or cells, as well as nonbiological particles. In particular, using the calibration/standardization method and polymer particles according to the present invention allows hematology instruments to be calibrated and standardized for subsequent accurate and reliable determinations of red blood cells, reticulocytes, white blood cells and platelets in whole blood samples.

    Abstract translation: 本发明描述了使用具有物理性质的合成聚合物颗粒或珠粒来校准或标准化流式细胞仪器的新方法，其提供了在这些仪器中使用的优点。 在校准方法中使用的聚合物颗粒或珠粒是球形的，平均粒径为约1至约8微米，相对较窄的颗粒分布和低折射率，即约1.35至约1.45。 颗粒安全，长时间稳定，特别适合用作血液分析仪校准物质。 本发明提供了相对于目前用于校准依赖于光散射的各种仪器与其他参数相结合以识别和测量生物颗粒或细胞以及非生物颗粒的标准类型的有利改进。 特别地，使用根据本发明的校准/标准化方法和聚合物颗粒允许血液仪器被校准和标准化，用于随后准确可靠地测定全血样品中的红细胞，网织红细胞，白细胞和血小板。

    Process for producing polymers of .alpha.,.omega.-unsaturated conjugated compounds
    43.
    发明授权
    Process for producing polymers of .alpha.,.omega.-unsaturated conjugated compounds 失效
    制备α，ω-不饱和共轭化合物的聚合物的方法

    公开(公告)号：US5763539A

    公开(公告)日：1998-06-09

    申请号：US538409

    申请日：1995-10-02

    Applicant: Roland Stern ,  Dirk Vanderzande ,  Frank Louwet ,  Joanes Gelan ,  Anna Issaris ,  Michael van der Broght

    Inventor： Roland Stern ,  Dirk Vanderzande ,  Frank Louwet ,  Joanes Gelan ,  Anna Issaris ,  Michael van der Broght

    IPC: C08G61/02 ,  C08G61/00 ,  C09K11/06 ,  H05B33/14 ,  C08F283/00

    CPC classification number: H05B33/14 ,  C08G61/00 ,  C09K11/06

    Abstract: A process for producing polymers of .alpha.,.omega.-unsaturated conjugated compounds, comprising reacting a precursor monomer of the formula I, ##STR1## wherein P denotes --SR.sup.3, --SO--R.sup.3, --SO.sub.2 --R.sup.3, --COOR.sup.3, --NO.sub.2, --CN, --CF.sub.3 or R.sup.3 ; L denotes --Cl, --Br, --I, --O-tosylate, --O-mesylate, --O-triflate, --(NR.sup.3.sub.3).sym. or --(SR.sup.3 R.sup.4).sym.; R.sup.1,R.sup.2 are the same or different and denote H, R.sup.3 or P; R.sup.3, R.sup.4 and A are as defined in the application. This reaction is characterized in that, on reaction of the base with the compound of the formula (I), a polymer is formed which is essentially soluble in said solvent, and a salt is formed as a by-product, which is essentially soluble in the solvent. That solvent comprises a compound selected from the group consisting of a) amides of the general formula (II) R.sup.5 --CO--NR.sup.6 H; b) amines of the general formula (III) R.sup.7.sub.2 --N--R.sup.8 ; c) sulfones of the general formula (IV) R.sup.8 --SO.sub.2 --R.sup.9 ; d) sulfoxides of the general formula (V) R.sup.8 --SO--R.sup.9 ; and e) a solvent from the group consisting of alcohols, polyalcohols, glycols and polyethers, where R.sup.5, R.sup.6, R.sup.7, R.sup.8, and R.sup.9 are as defined in the application. The process provides chemically and thermally stable, high molecular weight polymers of high purity and high regularity, in good yield. When the products of the novel process carry groups that undergo elimination to form double bonds, high quality electroluminescent materials can be prepared.

    Abstract translation: 一种制备α，ω-不饱和共轭化合物的聚合物的方法，包括使式I的前体单体，其中P表示-SR 3，-SO-R 3，-SO 2 -R 3，-COOR 3， - NO 2，-CN，-CF 3或R 3; L表示-Cl，-Br，-I，-O-甲苯磺酸酯，-O-甲磺酸酯，-O-三氟甲磺酸酯， - （NR33）（+）或 - （SR3R4）（+）; R1，R2相同或不同，表示H，R3或P; R3，R4和A如申请中所定义。 该反应的特征在于，在碱与式（I）化合物的反应中，形成基本上可溶于所述溶剂的聚合物，并且盐形成为副产物，其基本上可溶于 溶剂。 该溶剂包括选自以下的化合物：a）通式（II）的酰胺R5-CO-NR6H; b）通式（III）的胺R72-N-R8; c）通式（Ⅳ）的砜：R8-SO2-R9; d）通式（V）的基团：R8-SO-R9; 和e）来自醇，多元醇，二醇和聚醚的溶剂，其中R 5，R 6，R 7，R 8和R 9如本申请中所定义。 该方法以高纯度和高规则性提供化学和热稳定的高分子量聚合物，产率高。 当新工艺的产物携带经过消除形成双键的基团时，可以制备高品质的电致发光材料。

    Toning agents for use in thermographic recording materials
    46.
    发明授权
    Toning agents for use in thermographic recording materials 失效
    用于热敏记录材料的调色剂

    公开(公告)号：US07179768B2

    公开(公告)日：2007-02-20

    申请号：US11257480

    申请日：2005-10-24

    Applicant: Carlo Uyttendaele ,  Johan Loccufier ,  Frank Louwet

    Inventor： Carlo Uyttendaele ,  Johan Loccufier ,  Frank Louwet

    IPC: B41M5/30

    CPC classification number: G03C1/49845 ,  G03C1/4989

    Abstract: A thermographic recording material comprising a support and a thermosensitive element, the thermosensitive element comprising at least one substantially light-insensitive organic silver salt, at least one organic reducing agent therefor in thermal working relationship therewith, at least one binder and at least one toning agent represented by formula (I): wherein X represents the optionally substituted atoms necessary to form a 6-membered ring.

    Abstract translation: 一种包含支持体和热敏元件的热敏记录材料，所述热敏元件包含至少一种基本上不光敏的有机银盐，至少一种与其热处理关系的有机还原剂，至少一种粘合剂和至少一种调色剂 由式（I）表示：其中X表示形成6元环所需的任选取代的原子。

    Process for preparing a substantially transparent conductive layer configuration
    47.
    发明授权
    Process for preparing a substantially transparent conductive layer configuration 失效
    制备基本上透明的导电层构型的方法

    公开(公告)号：US07026079B2

    公开(公告)日：2006-04-11

    申请号：US10645160

    申请日：2003-08-21

    Applicant: Frank Louwet ,  Tom Cloots ,  Hieronymus Andriessen

    Inventor： Frank Louwet ,  Tom Cloots ,  Hieronymus Andriessen

    IPC: G03C1/89 ,  G03C5/29 ,  G03C8/28 ,  G03C8/52 ,  G03C8/32

    CPC classification number: H05K3/106 ,  H01B1/127 ,  H01B1/22 ,  H01L51/0021 ,  H01L51/0037 ,  H01L51/445 ,  H01L51/5203 ,  H05K2201/0329 ,  Y02E10/549

    Abstract: A process for preparing a substantially transparent conductive layer configuration on a support, the layer configuration comprising in any order at least a first layer containing an intrinsically conductive polymer optionally containing structural units represented by formula (I): wherein n is larger than 1 and each of R1 and R2 independently represents hydrogen or an optionally substituted C1-4 alkyl group or together represent an optionally substituted C1-4 alkylene group or an optionally substituted cycloalkylene group, preferably an ethylene group, an optionally alkyl-substituted methylene group, an optionally C1-12 alkyl- or phenyl-substituted ethylene group, a 1,3-propylene group or a 1,2-cyclohexylene group; and a second layer consisting of a non-continuous layer of conductive silver, the process comprising the step of: preparing the second layer by a photographic process; and light emitting diodes, photovoltaic devices, transistors and electroluminescent devices comprising a layer configuration prepared according to this process.

    Abstract translation: 一种用于在载体上制备基本上透明的导电层构型的方法，所述层构型至少包含含有本发明的导电聚合物的第一层，所述第一层含有任选含有由式（I）表示的结构单元的固有导电聚合物：其中n大于1， R 1和R 2独立地表示氢或任选取代的C 1-4烷基，或者一起表示任选取代的C 1 -C 4烷基， 1-4个亚烷基或任选取代的亚环烷基，优选亚乙基，任选烷基取代的亚甲基，任选的C 1-12烷基或苯基取代的亚乙基 ，1,3-亚丙基或1,2-亚环己基; 以及由不连续的导电银层组成的第二层，该方法包括以下步骤：通过摄影法制备第二层; 以及发光二极管，光电器件，晶体管和电致发光器件，其包括根据该工艺制备的层构型。

    3,4-alkylenedioxy-thiophene copolymers
    48.
    发明授权
    3,4-alkylenedioxy-thiophene copolymers 有权

    公开(公告)号：US06995223B2

    公开(公告)日：2006-02-07

    申请号：US10321888

    申请日：2002-12-17

    Applicant: Bert Groenendaal ,  Frank Louwet

    Inventor： Bert Groenendaal ,  Frank Louwet

    IPC: C08F234/04 ,  C08F28/06 ,  C08L45/00 ,  C08G61/12

    CPC classification number: C08G61/126 ,  C09D165/00

    Abstract: An aqueous dispersion of a copolymer of at least one 3,4-alkylenedioxythiophene compound with a solubility in water at 25° C. of less than 2.2 g/L with at least one 3,4-alkylenedioxythiophene compound with a solubility in water at 25° C. of at least 2.2 g/L and a polyanion; a preparation process therefor; its use for coating; a printing ink containing the aqueous dispersion; an electro-conductive layer containing a copolymer of at least one 3,4-alkylenedioxythiophene compound with a solubility in water at 25° C. of less than 2.2 g/L with at least one 3,4-alkylenedioxythiophene compound with a solubility in water at 25° C. of at least 2.2 g/L and a polyanion derived from an aqueous dispersion thereof; and an antistatic layer containing a copolymer of at least one 3,4-alkylenedioxy-thiophene compound with a solubility in water at 25° C. of less than 2.2 g/L with at least one 3,4-alkylenedioxythiophene compound with a solubility in water at 25° C. of at least 2.2 g/L and a polyanion derived from an aqueous dispersion thereof.

    Stabilizers for use in substantially light-insensitive thermographic recording materials
    49.
    发明申请
    Stabilizers for use in substantially light-insensitive thermographic recording materials 有权

    公开(公告)号：US20050255415A1

    公开(公告)日：2005-11-17

    申请号：US11127645

    申请日：2005-05-12

    Applicant: Frank Louwet ,  Johan Loccufier

    Inventor： Frank Louwet ,  Johan Loccufier

    IPC: G03C1/00 ,  G03C1/498

    CPC classification number: G03C1/4989 ,  G03C1/49845 ,  Y10S430/165 ,  Y10S430/166

    Abstract: A substantially light-insensitive black and white monosheet thermographic recording material comprising a support and a thermosensitive element, said thermosensitive element containing a substantially light-insensitive organic silver salt, an organic reducing agent therefor in thermal working relationship therewith, at least one binder and at least one stabilizer represented by formula (I): wherein R1, R2, R3 and R4 are independently selected from the group consisting of a hydrogen atom, halogen atoms and aliphatic, alkoxy, nitro, acyl, sulfonyl, nitrile, alkaryl, aryl, amino, thioalkyl, aldehyde, urea, —O—(C═O)-alkyl, —O—(C═O)-aryl, —O—(C═O)—O-alkyl, —O—(C═O)—O-aryl, —NH—(C═O)-alkyl, —NH—(C═O)-aryl, —(C═O)—NH-alkyl, —(C═O)—NH-aryl, —NH—(SO2)-alkyl, —NH—(SO2)-aryl, —(SO2)—NH-alkyl, —(SO2)—NH-aryl groups; X is represented by -A(-M)n or is selected from the group consisting of substituted aliphatic groups, unsubstituted aliphatic groups, substituted cycloaliphatic groups, unsubstituted cycloaliphatic groups, substituted aromatic groups and unsubstituted aromatic groups where in each of said groups one or more of the chain or ring carbon atoms may be substituted by one of more atoms selected from the group consisting of S, O, Si, N and P atoms; n is 2, 3 or 4; A is selected from the group consisting of substituted aliphatic groups, unsubstituted aliphatic groups, substituted cycloaliphatic groups, unsubstituted cycloaliphatic groups, substituted aromatic groups and unsubstituted aromatic groups where in each of said groups one or more of the chain or ring carbon atoms may be substituted by one of more atoms selected from the group consisting of S, O, Si, N and P atoms; each (-M) is independently a substituted or unsubstituted group selected from the group consisting of -(2-S-imidazole) groups and -(2-S-imidazole) groups annelated with an aromatic ring system, the optional substituents for -M being selected from the group consisting of halogen atoms and aliphatic, alkoxy, nitro, acyl, sulfonyl, nitrile, alkaryl and aryl groups.

    Process for preparing an aqueous or non-aqueous solution or dispersion of a polythiophene or thiophene copolymer
    50.
    发明申请
    Process for preparing an aqueous or non-aqueous solution or dispersion of a polythiophene or thiophene copolymer 有权
    制备聚噻吩或噻吩共聚物的水溶液或非水溶液或分散体的方法

    公开(公告)号：US20050245723A1

    公开(公告)日：2005-11-03

    申请号：US11150774

    申请日：2005-06-10

    Applicant: Frank Louwet ,  Bert Groenendaal

    Inventor： Frank Louwet ,  Bert Groenendaal

    IPC: B41J2/01 ,  B05D5/00 ,  B41M5/00 ,  C08G61/12 ,  C08G75/00 ,  C08G75/06 ,  C08J3/09 ,  C08K5/00 ,  C08L1/00 ,  C08L25/18 ,  C08L65/00 ,  C09D5/24 ,  C09D11/00 ,  C09D11/10 ,  C09D125/18 ,  C09D165/00 ,  G03G7/00 ,  H01B1/00

    CPC classification number: C08G61/126 ,  C08G2261/122 ,  C08G2261/1424 ,  C08G2261/1426 ,  C08G2261/1452 ,  C08G2261/3223 ,  C08G2261/43 ,  C08G2261/51 ,  C08G2261/794 ,  C09D165/00 ,  H01G9/028 ,  H01G11/48 ,  Y02E60/13 ,  Y10T428/31533 ,  C08L25/18

    Abstract: A process for preparing an aqueous or non-aqueous solution or dispersion of a polythiophene or thiophene copolymer, containing structural units according to formula (I): in which R1 and R2 independently of one another represent hydrogen or a C1-5-alkyl group or together form an optionally substituted C1-5-alkylene residue, comprising the step of: preparing the polythiophene or thiophene copolymer with an initiator in a reaction is medium in the presence of polyanions under oxidizing or reducing conditions under an inert atmosphere such that when said initiator is added less than 3 mg of oxygen per litre of the reaction medium is present in the reaction medium; an aqueous or non-aqueous solution or dispersion prepared therewith; the use of an aqueous or non-aqueous dispersion or solution comprising the aqueous or non-aqueous solution or dispersion of a polythiophene or thiophene copolymer for coating an object; a printable paste containing the aqueous or non-aqueous solution or dispersion of a polythiophene or thiophene copolymer; and an electroconductive or an antistatic layer prepared using an aqueous or non-aqueous solution or dispersion comprising the aqueous or non-aqueous solution or dispersion of a polythiophene or thiophene copolymer.

    Abstract translation: 一种制备含有根据式（I）的结构单元的聚噻吩或噻吩共聚物的水溶液或非水溶液或分散体的方法：其中R 1和R 2 = >彼此独立地表示氢或C 1-5 - 烷基或一起形成任选取代的C 1-5 - 亚烷基残基，包括以下步骤：制备 在氧化或还原条件下，在惰性气氛下，在聚阴离子存在下，将聚噻吩或噻吩共聚物与反应中的引发剂进行介质反应，使得当每升反应介质中加入少于3mg氧气时， 反应介质; 用其制备的水性或非水溶液或分散体; 使用包含聚噻吩或噻吩共聚物的水溶液或非水溶液或分散体的水性或非水分散体或溶液来涂覆物体; 含有聚噻吩或噻吩共聚物的水溶液或非水溶液或分散体的可印刷浆料; 以及使用包含聚噻吩或噻吩共聚物的水溶液或非水溶液或分散体的水性或非水溶液或分散体制备的导电或抗静电层。

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