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    Alpha-hydroxyisobutyric acid process
    52.
    发明授权
    Alpha-hydroxyisobutyric acid process 失效
    α-羟基异丁酸方法

    公开(公告)号：US4351955A

    公开(公告)日：1982-09-28

    申请号：US204676

    申请日：1980-11-05

    申请人： Carl L. Willis ,  Lynn H. Slaugh

    发明人： Carl L. Willis ,  Lynn H. Slaugh

    IPC分类号： C07C51/08 ,  C07C59/00

    CPC分类号： C07C51/08

    摘要： Acetone cyanohydrin is converted to alpha-hydroxyisobutyric acid by contacting the cyanohydrin with alpha-hydroxymethanesulfonic acid and water at a temperature of about 70.degree.-125.degree. C. The alpha-hydroxymethanesulfonic acid is an equilibrium product of the reaction of water, sulfur dioxide and formaldehyde.

    摘要翻译： 丙酮氰醇通过使氰醇与α-羟基甲磺酸和水在约70-125℃的温度下接触而转化为α-羟基异丁酸.α-羟基甲磺酸是水，二氧化硫和 甲醛。

    SULFONATED BLOCK COPOLYMER LAMINATES WITH POLAR OR ACTIVE METAL SUBSTRATES
    53.
    发明申请
    SULFONATED BLOCK COPOLYMER LAMINATES WITH POLAR OR ACTIVE METAL SUBSTRATES 审中-公开
    具有极性或活性金属基材的磺化嵌段共聚物层压板

    公开(公告)号：US20130108880A1

    公开(公告)日：2013-05-02

    申请号：US13285306

    申请日：2011-10-31

    申请人： Kuitian Tan ,  Carl L. Willis

    发明人： Kuitian Tan ,  Carl L. Willis

    IPC分类号： B32B15/08 ,  F28F7/00 ,  B32B37/26 ,  B01J39/20 ,  B32B37/02

    CPC分类号： B32B38/164 ,  B32B15/08 ,  B32B37/0038 ,  B32B2038/166 ,  B32B2311/00 ,  C08J5/122 ,  F24F2203/1032 ,  F28D19/042 ,  Y10T428/31692

    摘要： A process for laminating a polar substrate with a film cast from a sulfonated block copolymer having at least one end block A and at least one interior block B wherein each A block contains essentially no sulfonic acid or sulfonate ester functional groups and each B block is a polymer block containing from about 10 to about 100 mol percent sulfonic acid or sulfonate ester functional groups based on the number of monomer units. The film is exposed to water and dried onto a polar or active metal substrate. The laminates do not delaminate in the presence of water and may be used for a variety of applications including energy exchange applications.

    摘要翻译： 一种用具有至少一个端嵌段A和至少一个内嵌块B的磺化嵌段共聚物的薄膜浇铸的极性基材层压的方法，其中每个A嵌段基本上不含磺酸或磺酸酯官能团，并且每个B嵌段是 聚合物嵌段，其含有约10至约100摩尔％的基于单体数目的磺酸或磺酸酯官能团。 将该膜暴露于水中并干燥至极性或活性金属基底上。 层压板在水的存在下不会分层，并可用于各种应用，包括能量交换应用。

    Block copolymer
    54.
    发明授权
    Block copolymer 有权
    嵌段共聚物

    公开(公告)号：US06699941B1

    公开(公告)日：2004-03-02

    申请号：US10289833

    申请日：2002-11-07

    申请人： Dale L. Handlin ,  David T. Williamson ,  Carl L. Willis

    发明人： Dale L. Handlin ,  David T. Williamson ,  Carl L. Willis

    IPC分类号： C08F27900

    CPC分类号： C08F8/04 ,  C08F297/04

    摘要： The present invention relates to selectively hydrogenated block copolymers where one of the blocks is a random copolymer of a mono-alkenyl arene monomer, such as styrene, and a 1,3-cyclodiene monomer, such as 1,3-cyclohexadiene, and one of the other blocks is a hydrogenated polymer or copolymer of an acyclic conjugated diene, such as 1,3-butadiene or isoprene.

    摘要翻译： 本发明涉及选择性氢化嵌段共聚物，其中一个嵌段是单链烯基芳族单体如苯乙烯的无规共聚物和1,3-环二烯单体如1,3-环己二烯，和 其它嵌段是非环状共轭二烯如1,3-丁二烯或异戊二烯的氢化聚合物或共聚物。

    Blends of modified radial polymers and engineering thermoplastic polymers
    57.
    发明授权
    Blends of modified radial polymers and engineering thermoplastic polymers 失效
    改性径向聚合物和工程热塑性聚合物的共混物

    公开(公告)号：US5218044A

    公开(公告)日：1993-06-08

    申请号：US505373

    申请日：1990-04-06

    申请人： Richard Gelles ,  Carl L. Willis ,  John E. Gorman ,  Andres M. Arismendi, Jr.

    发明人： Richard Gelles ,  Carl L. Willis ,  John E. Gorman ,  Andres M. Arismendi, Jr.

    IPC分类号： C08L53/00 ,  C08L67/02 ,  C08L71/12 ,  C08L77/00

    CPC分类号： C08L53/005 ,  C08L67/02 ,  C08L71/123 ,  C08L77/00

    摘要： A super-tough polymeric composition comprising an engineering thermoplastic and a modified radial polymer. The engineering thermoplastic is selected from the group consisting of polyamides, thermoplastic polyesters, polyphenylene ether resins, polyarylene sulfide resins, polysulfone and the like. The modified radial polymer is modified by grafting a compound containing a carboxylic acid or carboxylic acid derivative group. The modified, radial polymer has from about 3 to about 50 arms, as determined using light scattering techniques and the arms will be olefin polymers. The polymer compositions will yield shaped articles which fail ductilely when tested using ASTM procedure D-256 at room temperature and some at -20.degree. F.

    摘要翻译： 包含工程热塑性塑料和改性径向聚合物的超韧性聚合物组合物。 工程热塑性塑料选自聚酰胺，热塑性聚酯，聚苯醚树脂，聚芳硫醚树脂，聚砜等。 通过接枝含有羧酸或羧酸衍生物基团的化合物改性改性的径向聚合物。 修饰的径向聚合物具有约3至约50个臂，如使用光散射技术测定的，臂将为烯烃聚合物。 聚合物组合物将产生成形制品，当在室温下使用ASTM程序D-256进行测试并且在-20°F下测试时，会使其延性失效。

    Functionalized polymers and process for modifying unsaturated polymers
    59.
    发明授权
    Functionalized polymers and process for modifying unsaturated polymers 失效
    官能化聚合物和改性不饱和聚合物的方法

    公开(公告)号：US4970265A

    公开(公告)日：1990-11-13

    申请号：US329059

    申请日：1989-03-27

    申请人： Carl L. Willis

    发明人： Carl L. Willis

    IPC分类号： C08F8/00 ,  C08F8/04

    CPC分类号： C08F8/00 ,  C08F8/04

    摘要： Unsaturated hydrocarbon polymers are hydrogenated in the presence of a catalyst obtained by combining a Group VIII-A metal alkoxide or carboxylate and an alkyl or hydride of a metal selected from Groups I-A, II-A and III-B and then functionalized by contacting the hydrogenated polymer with a functionalizing agent before the hydrogenation catalyst is quenched or otherwise deactivated. The hydrogenation is, generally, accomplished at relatively mild conditions to avoid degradation of the polymer and, in the case of unsaturated copolymers comprising aromatic unsaturation, to avoid any significant hydrogenation of the aromatic unsaturation. Generally, the hydrogen partial pressure employed will be below about 1000 psig and the hydrogenation temperature will be below about 125.degree. C. The hydrogenated polymer may be functionalized by reaction with functionalizing agent select from the group carbon dioxide, ethylene oxide, aldehydes, ketones, carboxylic acid salts and esters, halides, epoxides, sulfur, boron alkoxides, isocyanates, various silicon compounds and the like. Carbon dioxide is a particularly preferred functionalizing agent since the thus functionalized polymer is useful as a modifier in sheet and bulk molding compositions and readily responds to the presence of thickening agents.

    摘要翻译： 不饱和烃聚合物在通过将VIII-A族金属醇盐或羧酸盐与选自IA，II-A和III-B族的金属的烷基或氢化物组合而获得的催化剂存在下氢化，然后通过使氢化 在氢化催化剂淬灭或以其它方式失活之前，使用官能化剂的聚合物。 通常在相对温和的条件下进行氢化以避免聚合物的降解，并且在包含芳族不饱和键的不饱和共聚物的情况下，以避免芳族不饱和度的任何明显氢化。 一般来说，所用的氢气分压将低于约1000psig，氢化温度将低于约125℃。氢化聚合物可以通过与选自二氧化碳，环氧乙烷，醛，酮， 羧酸盐和酯，卤化物，环氧化物，硫，硼醇盐，异氰酸酯，各种硅化合物等。 二氧化碳是特别优选的官能化剂，因为如此官能化的聚合物可用作片材和本体模塑组合物中的改性剂，并且容易响应增稠剂的存在。