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    Amination of allylic alcohols
    61.
    发明授权
    Amination of allylic alcohols 失效
    烯丙醇的胺化

    公开(公告)号：US5639916A

    公开(公告)日：1997-06-17

    申请号：US564666

    申请日：1995-11-29

    申请人： John William Mitchell ,  Gamini Ananda Vedage

    发明人： John William Mitchell ,  Gamini Ananda Vedage

    IPC分类号： C07C209/16 ,  C07C211/21

    CPC分类号： C07C211/21 ,  C07C209/16

    摘要： This invention relates to an improvement in a process for the catalytic amination of an allylic alcohol of the formula:CH.sub.2 .dbd.CR--CH.sub.2 OHwhere R is hydrogen or methyl with ammonia or an amine of the formula R.sub.1 R.sub.2 NH where R.sub.1 and R.sub.2 represent hydrogen or a C.sub.1-5 hydrocarbyl group in the presence of an effective amount of a phosphorous containing catalyst to effect reaction between the allylic alcohol and the ammonia or amine to produce an allylic amine. The improvement in the process resides in utilizing a neutral group IIA metal phosphate as a catalyst component. Calcium phosphate is preferred and the catalyst.

    摘要翻译： 本发明涉及用于下式的烯丙醇催化胺化的方法：CH 2 = CR-CH 2 OH，其中R是氢或甲基与氨或式R 1 R 2 NH的胺，其中R 1和R 2表示氢或C1 -5烃基，在有效量的含磷催化剂存在下进行烯丙醇与氨或胺之间的反应以产生烯丙基胺。 该方法的改进在于利用中性IIA族金属磷酸盐作为催化剂组分。 优选的是磷酸钙和催化剂。

    Mixed Polycycloaliphatic Amines (MPCA) And MPCA Alkylates
    69.
    发明申请
    Mixed Polycycloaliphatic Amines (MPCA) And MPCA Alkylates 有权
    混合多环脂族胺（MPCA）和MPCA烷基化物

    公开(公告)号：US20110301318A1

    公开(公告)日：2011-12-08

    申请号：US13216687

    申请日：2011-08-24

    申请人： Mark David Conner ,  Gamini Ananda Vedage ,  Peter Andrew Lucas ,  Courtney Thompson Thurau ,  RIchard V.C. Carr

    发明人： Mark David Conner ,  Gamini Ananda Vedage ,  Peter Andrew Lucas ,  Courtney Thompson Thurau ,  RIchard V.C. Carr

    IPC分类号： C08G18/32

    CPC分类号： C08G18/5024 ,  C08G18/3234 ,  C08G2150/50 ,  C09D175/02

    摘要： Mixed polycycloaliphatic amines (MPCA) and alkylates thereof (MPCA alkylates), methods for making mixed polycycloaliphatic MPCA amines and MPCA alkylates thereof, as well as polymeric compositions, such as spray-applied polyurea coating compositions, comprising said mixed amines MPCA and MPCA alkylates thereof are described herein. In one embodiment, the polymeric composition comprises an isocyanate component, and a resin component comprising an organic compound having the following Formula I: where R1, R2 and R3 are each independently selected from a hydrogen atom, an alkyl group comprising from 1 to 20 carbon atoms, an aryl group comprising from 3 to 12 carbon atoms, an aralkyl group comprising from 3 to 12 carbon atoms and combinations thereof, provided that there is at least one alkyl group within Formula I, and X is a methylene bridged polycycloaliphatic amine (MPCA).

    摘要翻译： 混合多环脂族胺（MPCA）及其烷基化物（MPCA烷基化物），制备混合多环脂肪族MPCA胺及其MPCA烷基化物的方法，以及聚合物组合物，例如喷雾施加的聚脲涂料组合物，其包含所述混合胺MPCA及其MPCA烷基化物 在此描述。 在一个实施方案中，聚合物组合物包含异氰酸酯组分和包含具有下式I的有机化合物的树脂组分：其中R 1，R 2和R 3各自独立地选自氢原子，含有1至20个碳的烷基 原子，包含3至12个碳原子的芳基，含有3至12个碳原子的芳烷基及其组合，条件是式I中至少有一个烷基，X是亚甲基桥连的聚环脂族胺（MPCA ）。

    Mixed polycycloaliphatic amines (MPCA) and MPCA alkylates
    70.
    发明授权
    Mixed polycycloaliphatic amines (MPCA) and MPCA alkylates 有权
    混合多环脂族胺（MPCA）和MPCA烷基化物

    公开(公告)号：US08026318B2

    公开(公告)日：2011-09-27

    申请号：US12196606

    申请日：2008-08-22

    申请人： Mark David Conner ,  Gamini Ananda Vedage ,  Peter Andrew Lucas ,  Courtney Thompson Thurau ,  Richard V. C. Carr

    发明人： Mark David Conner ,  Gamini Ananda Vedage ,  Peter Andrew Lucas ,  Courtney Thompson Thurau ,  Richard V. C. Carr

    IPC分类号： C08G18/32 ,  C08L61/00

    CPC分类号： C08G18/5024 ,  C08G18/3234 ,  C08G2150/50 ,  C09D175/02

    摘要： Mixed polycycloaliphatic amines (MPCA) and alkylates thereof (MPCA alkylates), methods for making mixed polycycloaliphatic MPCA amines and MPCA alkylates thereof, as well as polymeric compositions, such as spray-applied polyurea coating compositions, comprising said mixed amines MPCA and MPCA alkylates thereof are described herein. In one embodiment, the polymeric composition comprises an isocyanate component, and a resin component comprising an organic compound having the following Formula I: where R1, R2 and R3 are each independently selected from a hydrogen atom, an alkyl group comprising from 1 to 20 carbon atoms, an aryl group comprising from 3 to 12 carbon atoms, an aralkyl group comprising from 3 to 12 carbon atoms and combinations thereof, provided that there is at least one alkyl group within Formula I, and X is a methylene bridged polycycloaliphatic amine (MPCA).

    摘要翻译： 混合多环脂族胺（MPCA）及其烷基化物（MPCA烷基化物），制备混合多环脂肪族MPCA胺及其MPCA烷基化物的方法，以及聚合物组合物，例如喷雾施加的聚脲涂料组合物，其包含所述混合胺MPCA及其MPCA烷基化物 在此描述。 在一个实施方案中，聚合物组合物包含异氰酸酯组分和包含具有下式I的有机化合物的树脂组分：其中R 1，R 2和R 3各自独立地选自氢原子，含有1至20个碳的烷基 原子，包含3至12个碳原子的芳基，含有3至12个碳原子的芳烷基及其组合，条件是式I中至少有一个烷基，X是亚甲基桥连的聚环脂族胺（MPCA ）。