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    Method for Producing Aromatic Compound Polymer
    65.
    发明申请
    Method for Producing Aromatic Compound Polymer 有权
    生产芳香族化合物聚合物的方法

    公开(公告)号：US20090018309A1

    公开(公告)日：2009-01-15

    申请号：US11571280

    申请日：2005-06-24

    申请人： Hideyuki Higashimura ,  Daisuke Fukushima ,  Kazuei Ohuchi

    发明人： Hideyuki Higashimura ,  Daisuke Fukushima ,  Kazuei Ohuchi

    IPC分类号： C08G65/00 ,  C07F9/00

    CPC分类号： C08G61/12 ,  C07C49/92 ,  C07F9/005 ,  C08G61/02 ,  C08G61/10

    摘要： A method for producing an aromatic compound polymer comprising oxidatively polymerizing one or more of aromatic compound(s) having two or more hydrogen atoms directly connected to aromatic ring(s), in the presence of an oxidizing agent, wherein the method employs a catalyst composed of a transition metal complex or a catalyst prepared from a transition metal complex and an activating agent, and said catalyst has a parameter P defined by the following formula (A) of 0.50 or more, and a parameter Eo defined by the following formula (B) of 0.50 [V] or more: P=Af/Ai  (A) and Eo=(Epa+Epc)/2[V]  (B).

    摘要翻译： 一种芳族化合物聚合物的制造方法，其特征在于，在氧化剂的存在下，使直接与芳香环连接的2个以上的氢原子的一种以上的芳香族化合物氧化聚合， 的过渡金属络合物或由过渡金属络合物和活化剂制备的催化剂，所述催化剂具有下式（A）定义的参数P为0.50以上，以及由下式（B ）0.50 [V]以上：<？in-line-formula description =“In-line Formulas”end =“lead”？> P = Af / Ai（A）<？in-line-formula description =“In -line公式“end =”tail“？> <？in-line-formula description =”In-line Formulas“end =”lead“？>和<？in-line-formula description =”In-line Formulas“end =“tail”？> <？in-line-formula description =“In-line formula”end =“lead”？> Eo =（Epa + Epc）/ 2 [V]（B） 公式描述=“内联公式”end =“tail”？>

    Method for producing phenol condensate
    66.
    发明授权
    Method for producing phenol condensate 有权
    生产苯酚缩合物的方法

    公开(公告)号：US07161000B2

    公开(公告)日：2007-01-09

    申请号：US10854334

    申请日：2004-05-27

    申请人： Hideyuki Higashimura ,  Eiichi Kotake ,  Masaaki Kubota ,  Shiro Kobayashi

    发明人： Hideyuki Higashimura ,  Eiichi Kotake ,  Masaaki Kubota ,  Shiro Kobayashi

    IPC分类号： C07D225/00 ,  C07C39/12

    CPC分类号： C07C49/753 ,  C07C45/39

    摘要： Provided is a method for producing a phenol condensate by oxidative condensation of a phenol compound not having a substituted group on at least one ortho-position, in the presence of a specific complex (II) and oxygen, wherein a condensate coupled at para-position of the phenol can be produced in an excellent yield, L-M (X)n  (II) wherein L represents a ligand having 2 to 4 nitrogen atoms as donor atoms, M represents copper ion, nickel ion, cobalt ion, iron ion, manganese ion, chromium ion or vanadyl ion, X represents a counter ion, n is a number of Xs.

    摘要翻译： 本发明提供一种通过在特定络合物（II）和氧气存在下，在至少一个邻位的不具有取代基的酚化合物进行氧化缩合来制备苯酚缩合物的方法，其中在对位 可以以优异的产率制备苯酚，<？在线公式描述=“在线公式”end =“lead”？> LM（X）n（II） 其中L表示作为供体原子的具有2〜4个氮原子的配体，M表示铜离子，镍离子，钴离子，铁离子，锰 离子，铬离子或氧离子离子，X表示抗衡离子，n是X的数量。

    Crystallizable poly (2,5-di-substituted-1,4-phenylene oxide) and a method of preparing the same
    67.
    发明授权
    Crystallizable poly (2,5-di-substituted-1,4-phenylene oxide) and a method of preparing the same 失效
    可结晶的聚（2,5-二取代-1,4-亚苯基氧化物）及其制备方法

    公开(公告)号：US06541596B1

    公开(公告)日：2003-04-01

    申请号：US09496268

    申请日：2000-02-01

    申请人： Hideyuki Higashimura ,  Kiyoshi Fujisawa ,  Yoshihiko Moro-oka ,  Shiro Kobayashi

    发明人： Hideyuki Higashimura ,  Kiyoshi Fujisawa ,  Yoshihiko Moro-oka ,  Shiro Kobayashi

    IPC分类号： C08G5950

    CPC分类号： C08G65/44

    摘要： There is disclosed a crystallizable poly(2,5-di-substituted-1,4-phenylene oxide), which exhibits an exothermic peak for crystallization of not less than 5 J/g at 150° C. or over when cooled after melting, and/or an endothermic peak, at the time of melting of crystals thereof, of not less than 5 J/g at 150° C. or over when re-heated after cooling of the melt, and which comprises a recurring unit of the following formula (I), and a method of preparing the same by polymerization of a 2,5-di-substituted-phenol of the following formula (II) by use of a copper complex catalyst made of a tridentate ligand of which nitrogen atoms coordinate to a copper atom in coexistence with oxygen: wherein R1's independently represent a hydrocarbon group or a substituted hydrocarbon group, and they may be the same or different. The crystallizable poly(2,5-di-substituted-1,4-phenylene oxide) is able to provide a melt molding which has a reduced degree of coloration and good heat resistance.

    摘要翻译： 公开了一种可结晶的聚（2,5-二取代-1,4-亚苯基氧化物），其在熔化后冷却时在150℃或更高温度下表现出不低于5J / g的结晶放热峰， 和/或其结晶时的吸热峰在熔融物冷却后再加热时在150℃以上不低于5J / g，并且其包含以下的重复单元 式（I）的方法和通过使用由氮原子配位的三齿配体构成的铜络合物催化剂聚合下述式（II）的2,5-二取代苯酚而制备的方法 与氧共存的铜原子：其中R1独立地表示烃基或取代的烃基，它们可以相同或不同。 可结晶的聚（2,5-二取代-1,4-亚苯基氧化物）能够提供具有降低的着色程度和良好的耐热性的熔融模塑。

    THIN FILM AND COMPOUND USED IN THE SAME
    68.
    发明申请
    THIN FILM AND COMPOUND USED IN THE SAME 审中-公开
    薄膜及其使用的化合物

    公开(公告)号：US20130001472A1

    公开(公告)日：2013-01-03

    申请号：US13583177

    申请日：2011-03-04

    申请人： Joji Ohshita ,  Toshihiro Murafuji ,  Yusuke Kuramochi ,  Takashi Kaikoh ,  Hideyuki Higashimura

    发明人： Joji Ohshita ,  Toshihiro Murafuji ,  Yusuke Kuramochi ,  Takashi Kaikoh ,  Hideyuki Higashimura

    IPC分类号： C07F9/94 ,  C09K11/06 ,  B82Y30/00

    CPC分类号： C07F9/94 ,  C09K2211/1029 ,  C09K2211/1044 ,  C09K2211/1088 ,  C09K2211/1092 ,  C09K2211/188 ,  H01L51/0077 ,  H01L51/5016 ,  H05B33/145

    摘要： To provide a novel material exhibiting excellent light-emitting characteristics using a heavy metal element having relatively abundant reserve.A thin film containing a compound of Formula (1): wherein Ar1 and Ar2 are each independently a C3-30 aromatic ring; R1 and R2 are a substituent; a and b are each independently an integer of 0 to 12, wherein when a is 2 or more, each R1 is optionally different from each other and two R1 are optionally bonded with each other to form a ring structure, and when b is 2 or more, each R2 is optionally different from each other and two R2 are optionally bonded with each other to form a ring structure; A1 is any of direct bond, —O—, —S—, —S(═O)—, —S(═O)2—, —PR3—, —NR4—, and —C(—R5)2—; R3 is a hydrogen atom or a substituent; R4 is a hydrogen atom or a substituent; R5 is a hydrogen atom or a substituent and two R5 are optionally different from each other; E1 is a monovalent group having 50 or less carbon atoms; L1 is a ligand having 50 or less carbon atoms; c is an integer of 0 to 3, wherein when c is 2 or more, each L1 is optionally different from each other; and each combination of a combination of E1 and Ar1 and a combination of E1 and Ar2 optionally forms a bond; and when c is 1 to 3, each combination of a combination of L1 and E1, a combination of L1 and Ar1, a combination of L1 and Ar2, and a combination of L1 and L1 optionally forms a bond.

    摘要翻译： 使用具有相对丰富的储备的重金属元素提供显示出优异的发光特性的新型材料。 含有式（1）化合物的薄膜：其中Ar1和Ar2各自独立地为C3-30芳环; R1和R2是取代基; a和b各自独立地为0〜12的整数，其中当a为2以上时，每个R 1可以彼此不同，并且两个R 1彼此任意地键合形成环结构，当b为2或 更优选地，每个R 2彼此可选地彼此不同，并且两个R 2彼此可选地键合以形成环结构; A1是直接键合，-O - ， - S - ， - S（= O） - ， - S（= O）2 - ， - PR 3 - ， - NR 4 - 和-C（ - R 5） R3是氢原子或取代基; R4是氢原子或取代基; R5是氢原子或取代基，两个R5任选地彼此不同; E1是具有50个或更少碳原子的一价基团; L1是具有50个或更少碳原子的配体; c为0〜3的整数，其中，当c为2以上时，各L1彼此不同; 并且E1和Ar1的组合以及E1和Ar2的组合的每个组合可以任选地形成键; 当c为1〜3时，L1和E1的组合，L1和Ar1的组合，L1和Ar2的组合以及L1和L1的组合的组合可以任意地形成键。

    CYCLIC COMPOUND, ITS METAL COMPLEX AND MODIFIED METAL COMPLEX
    70.
    发明申请
    CYCLIC COMPOUND, ITS METAL COMPLEX AND MODIFIED METAL COMPLEX 有权
    周期化合物，金属复合物和改性金属络合物

    公开(公告)号：US20110015059A1

    公开(公告)日：2011-01-20

    申请号：US12811025

    申请日：2008-09-05

    申请人： Tadafumi Matsunaga ,  Nobuyoshi Koshino ,  Hideyuki Higashimura ,  Yusuke Ishii

    发明人： Tadafumi Matsunaga ,  Nobuyoshi Koshino ,  Hideyuki Higashimura ,  Yusuke Ishii

    IPC分类号： B01J31/22 ,  C07D471/22 ,  C07D487/22 ,  C07F15/06 ,  C07F19/00 ,  C07F15/04 ,  C07F1/08 ,  C08F26/06

    CPC分类号： H01M4/8652 ,  C07D207/335 ,  C07D471/04 ,  C07D471/22 ,  C07D487/22 ,  H01G9/2018 ,  H01L51/0083 ,  H01L51/009 ,  H01M4/9008 ,  H01M4/9075 ,  H01M4/9091 ,  H01M4/923 ,  H01M4/925 ,  H01M4/928 ,  H01M8/0289 ,  H01M8/1016 ,  Y02E10/542 ,  Y02E60/521

    摘要： A compound represented by formula (1): wherein Y1 to Y4 each independently represent any one of the following groups: in which Rα represents a hydrogen atom or a monovalent hydrocarbon group; P1 to P4 each independently represent a group of atoms necessary for forming a heterocyclic ring together with each of Y1 to Y4 and the two carbon atoms adjacent to each of Y1 to Y4, respectively; P5 and P6 each independently represent a group of atoms necessary for forming a cyclic skeleton together with the carbon atom to which Z1 bonds or Z2 bonds and the two carbon atoms adjacent to the carbon atom to which Z1 bonds or Z2 bonds; P1 and P2, P2 and P6, P6 and P4, P4 and P3, P3 and P5, and P5 and P1 may further combine with each other to form a ring; Q1 and Q2 each independently represent a connecting group or a direct binding; and Z1 and Z2 each independently represent any one of the following groups; —NRβ2, —ORβ, —SRβ, —PRβ2 in which Rβ represents a hydrogen atom or a monovalent hydrocarbon group, and when plural Rβs are present, these plural Rβs may be the same or different from each other.

    摘要翻译： 由式（1）表示的化合物：其中Y 1至Y 4各自独立地表示以下基团中的任一个：其中Rα表示氢原子或一价烃基; P1〜P4各自独立地表示与Y 1〜Y 4中的每一个以及Y1〜Y4中的每个相邻的2个碳原子一起形成杂环所需的原子团。 P5和P6各自独立地表示与Z1键或Z2键以及与Z1键或Z2键相邻的碳原子相邻的两个碳原子一起形成环状骨架所必需的一组原子; P1和P2，P2和P6，P6和P4，P4和P3，P3和P5，P5和P1可以进一步组合形成环; Q1和Q2各自独立地表示连接基团或直接结合; Z1和Z2各自独立地表示以下基团中的任何一个; -NR＆bgr; 2，-OR＆bgr; -SR＆bgr; -PR＆bgr; 2其中R＆bgr; 表示氢原子或一价烃基，当存在多个R b时，这些多个R a可相同或不同。