Liquid-liquid extraction system and process for use thereof

    公开(公告)号:US09889390B2

    公开(公告)日:2018-02-13

    申请号:US14650926

    申请日:2013-11-27

    摘要: A liquid-liquid extraction system (1) adapted for the flow of two or more liquids therein is disclosed. The system comprises a mixer settler sub-system (100) and a counter-current liquid-liquid extraction column (200). The sub-system (100) comprises one or more mixer settlers (110) connected in series, and the column (200) comprises either a mixing section (260) comprising an agitation means (261) and/or a static section (280) comprising an internal (281). The first outlet (131) of the mixer settler sub-system (100) is in fluid communication with the first inlet (221) of the column (200) and the second inlet (112) of the mixer settler sub-system (100) is in fluid communication with the second inlet (222) of the counter-current liquid-liquid extraction column (200). The invention further relates to a counter-current liquid-liquid extraction process for using said system 1. The present invention further relates also to the use of the system (5) or process in removing aromatic compounds from organic streams, in treating an oil stream of a refinery, or in a liquid-liquid extraction process having at least two feed streams of different viscosity, similar density, or low interfacial tension.

    Composite material and method for making
    65.
    发明授权
    Composite material and method for making 有权
    复合材料及其制造方法

    公开(公告)号:US09120251B2

    公开(公告)日:2015-09-01

    申请号:US13709477

    申请日:2012-12-10

    IPC分类号: B29C47/00 B01D11/04

    摘要: This invention relates to an improved method for making composite structures by dispersing a high tenacity fiber such as aramid in a polymeric matrix to form a premix, combining the premix with a natural fiber such as wood flour and extruding the resulting mixture through a fiber alignment plate and die such that the fibers are substantially aligned in the flow direction of the extrudate.

    摘要翻译: 本发明涉及通过将高强度纤维如芳族聚酰胺分散在聚合物基质中以形成预混物来制备复合结构的改进方法,将预混物与天然纤维如木粉混合,并将所得混合物通过纤维对准板 并且使得纤维在挤出物的流动方向上基本上对齐。

    METHOD AND APPARATUS FOR SEPARATING ALKYL AROMATIC HYDROCARBON
    66.
    发明申请
    METHOD AND APPARATUS FOR SEPARATING ALKYL AROMATIC HYDROCARBON 有权
    用于分离烷基芳烃的方法和装置

    公开(公告)号:US20150141730A1

    公开(公告)日:2015-05-21

    申请号:US14411289

    申请日:2013-06-25

    IPC分类号: C07C7/10 C07C7/152

    摘要: A method for separating an alkyl aromatic hydrocarbon, the method having a step of adding a first diluent and an extractant having a superacid to a mixture comprising the alkyl aromatic hydrocarbon and one or more isomers thereof to carry out an acid-base extraction to thereby form a complex of the alkyl aromatic hydrocarbon with the superacid, and thereafter separating the complex from the mixture, and a step of adding an eliminating agent having a relative basicity in a range of 0.06 to 10 with respect to the alkyl aromatic hydrocarbon and a second diluent to the complex, and carrying out complex exchange of the alkyl aromatic hydrocarbon for the eliminating agent to thereby separate the alkyl aromatic hydrocarbon from the complex.

    摘要翻译: 一种分离烷基芳族烃的方法,该方法具有将第一稀释剂和具有超强酸的萃取剂加入到包含烷基芳族烃的一种或多种异构体的混合物中以进行酸碱萃取从而形成 烷基芳族烃与超强酸的配合物,然后从混合物中分离配合物,以及相对于烷基芳族烃和第二稀释剂添加相对碱度在0.06至10范围内的消除剂的步骤 并进行用于消除剂的烷基芳族烃的复杂交换,从而将烷基芳族烃与络合物分离。

    LIQUID-LIQUID EXTRACTION PROCESS FOR THE PRODUCTION OF ACRYLIC ESTERS
    67.
    发明申请
    LIQUID-LIQUID EXTRACTION PROCESS FOR THE PRODUCTION OF ACRYLIC ESTERS 有权
    用于生产丙烯酸酯的液体 - 液体萃取方法

    公开(公告)号:US20150087857A1

    公开(公告)日:2015-03-26

    申请号:US14493559

    申请日:2014-09-23

    申请人: Arkema France

    摘要: The invention relates to a liquid-liquid extraction process, comprising: the provision of a main input liquid stream, comprising at least one compound of interest and an excess compound; the provision of a liquid scrubbing stream; the extraction of the excess compound from the main input liquid stream by contact with the liquid scrubbing stream, making it possible to collect a main output liquid stream, depleted in excess compound with respect to the main input liquid stream; in which: the main input liquid stream and the liquid scrubbing stream exhibit a difference in density of less than or equal to 50 kg/m3 and also an interfacial tension of less than or equal to 3 dyn/cm; and the extraction stage is carried out in a packed contactor with a ratio by weight as input liquid scrubbing stream/main liquid stream ranging from 0.3 to 0.5. The invention also relates to a process for the production of acrylic ester in which the production stream is treated by means of the above liquid-liquid extraction process.

    摘要翻译: 本发明涉及一种液体 - 液体提取方法,包括:提供主要输入液体流,其包含至少一种目标化合物和过量化合物; 提供液体洗涤流; 通过与液体洗涤流接触从主输入液体流中提取过量化合物,使得可以收集相对于主要输入液体流消耗过量化合物的主要输出液体流; 其中:主输入液体流和液体洗涤流表现出小于或等于50kg / m 3的密度差,以及小于或等于3达因/厘米的界面张力; 并且萃取阶段在填充接触器中进行,重量比为输入液体洗涤流/主液流,范围为0.3至0.5。 本发明还涉及生产丙烯酸酯的方法,其中通过上述液 - 液萃取方法处理生产流。

    Ordered open-cellular materials for mass transfer and/or phase separation applications
    68.
    发明授权
    Ordered open-cellular materials for mass transfer and/or phase separation applications 有权
    用于传质和/或相分离应用的有序的开孔材料

    公开(公告)号:US08852523B1

    公开(公告)日:2014-10-07

    申请号:US12405996

    申请日:2009-03-17

    摘要: A mass transfer system including a housing and a three-dimensional ordered open-cellular micro-truss material within the housing for a mass transfer application. Here, the three-dimensional ordered open-cellular micro-truss material includes a plurality of first truss elements defined by a plurality of first self-propagating polymer waveguides and extending along a first direction, a plurality of second truss elements defined by a plurality of second self-propagating polymer waveguides and extending along a second direction, and a plurality of third truss elements defined by a plurality of third self-propagating polymer waveguides and extending along a third direction. The first, second, and third ordered truss elements interpenetrate each other at a plurality of nodes to form a continuous material. In one embodiment, the continuous material is a metal material.

    摘要翻译: 质量传递系统,包括壳体内的三维有序开孔微型桁架材料,用于传质应用。 这里,三维排序的开孔微型桁架材料包括由多个第一自传播聚合物波导限定并沿着第一方向延伸的多个第一桁架元件,多个第二桁架元件由多个 第二自传播聚合物波导并沿着第二方向延伸,以及由多个第三自传播聚合物波导限定并沿着第三方向延伸的多个第三桁架元件。 第一,第二和第三有序的桁架元件在多个节点处相互渗透以形成连续材料。 在一个实施例中,连续材料是金属材料。

    Process for preparing an aromatic amine and apparatus therefor
    69.
    发明授权
    Process for preparing an aromatic amine and apparatus therefor 有权
    芳香胺的制备方法及其设备

    公开(公告)号:US08748665B2

    公开(公告)日:2014-06-10

    申请号:US13318257

    申请日:2010-05-06

    IPC分类号: C07C209/00

    摘要: The invention relates to a process for obtaining at least one aromatic amine from a liquid mixture comprising water and the at least one aromatic amine by extracting with at least one nitroaromatic in an extraction column (1) to form an essentially water- comprising raffinate stream and an extract stream comprising the at least one nitroaromatic and the aromatic amine. The extraction column (1) is divided by a dividing wall (3) into two regions (5, 7), and, in the case of an amount of liquid for separation which is less than a minimum cross sectional loading of the entire extraction column (1), the liquid mixture to be separated is fed only to one of the regions (5, 7) of the extraction column (1) divided by the dividing wall (3). The invention further relates to a process for preparing an aromatic amine and to an apparatus for separating a liquid mixture comprising water and at least one aromatic amine by extracting with at least one nitroaromatic, comprising an extraction column (1).

    摘要翻译: 本发明涉及一种从包含水和至少一种芳族胺的液体混合物中获得至少一种芳族胺的方法,其通过在提取塔(1)中用至少一种硝基芳族化合物萃取以形成基本上含水的萃余液流和 包含至少一种硝基芳族和芳族胺的提取物流。 萃取塔(1)由分隔壁(3)分成两个区域(5,7),并且在分离液体的量小于整个萃取塔的最小横截面负荷的情况下 (1)中,待分离的液体混合物仅被供给到由分隔壁(3)分隔的萃取塔(1)的区域(5,7)中的一个。 本发明还涉及一种制备芳族胺的方法,以及用于通过用至少一种包含萃取塔(1)的硝基芳族化合物萃取来分离包含水和至少一种芳族胺的液体混合物的装置。