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公开(公告)号：US09328036B2
公开(公告)日：2016-05-03
申请号：US14270057
申请日：2014-05-05
申请人： UOP LLC
发明人： Susie C. Martins , Erin M. Broderick , Douglas A. Nafis , Kaitlin M. DeSalvo , Stuart Smith , Alakananda Bhattacharyya
CPC分类号： C07C2/62 , B01J27/053 , B01J27/08 , B01J27/16 , B01J27/28 , B01J27/285 , B01J27/30 , B01J27/32 , B01J31/0284 , B01J31/0288 , B01J35/12 , B01J37/16 , B01J38/56 , B01J38/60 , C07C2/60 , C07C2527/125 , C07C2531/02 , C07C2531/22 , C10G50/00 , C10G2300/1092 , C10G2400/02 , Y02P20/584 , C07C9/21
摘要： A hydrocarbon conversion process is described. The process includes contacting a hydrocarbon feed with an acidic catalyst under hydrocarbon conversion conditions in a hydrocarbon conversion zone. The hydrocarbon feed reacts to form a mixture comprising reaction products, the acidic catalyst, and deactivated acidic catalyst containing conjunct polymer. The mixture is separated into at least two streams, a first stream comprising the reaction products and a second stream comprising the deactivated acidic catalyst. The reaction products are recovered. The deactivated acidic catalyst is contacted with at least one silane or borane compound in a regeneration zone under regeneration conditions, the conjunct polymer reacting with the at least one silane or borane compound resulting in a catalyst phase and an organic phase containing the conjunct polymer and at least one silyl or boryl compound.
摘要翻译： 描述烃转化方法。 该方法包括在烃转化区的烃转化条件下使烃进料与酸性催化剂接触。 烃进料反应形成包含反应产物，酸性催化剂和含有结合聚合物的失活酸性催化剂的混合物。 将混合物分离成至少两股物流，包含反应产物的第一物流和包含失活的酸性催化剂的第二料流。 回收反应产物。 失活的酸性催化剂在再生条件下在再生区中与至少一种硅烷或硼烷化合物接触，该结合聚合物与至少一种硅烷或甲硼烷化合物反应，产生催化剂相和含有结合聚合物的有机相， 至少一种甲硅烷基或硼基化合物。
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公开(公告)号：US20160075557A1
公开(公告)日：2016-03-17
申请号：US14419181
申请日：2014-06-06
发明人： Naoki Yahata , Tetsuo Nishida
IPC分类号： C01B25/455
CPC分类号： C01B25/455 , B01J31/0288 , C01P2006/80 , H01M10/0525 , H01M10/0567 , H01M2300/0025
摘要： Provided is a method for purifying a difluorophosphate, in which a difluorophosphate is purified to a high purity. The method includes a method for purifying a difluorophosphate, comprising bringing hydrogen fluoride into contact with a difluorophosphate containing an impurity and subsequently heating and drying the difluorophosphate, or bringing the hydrogen fluoride into contact with the difluorophosphate containing the impurity while heating and drying the difluorophosphate containing the impurity, thereby removing the impurity.
摘要翻译： 提供了一种纯化二氟磷酸盐以纯化至高纯度的二氟磷酸盐的方法。 该方法包括一种纯化二氟磷酸盐的方法，包括使氟化氢与含有杂质的二氟磷酸盐接触，随后加热和干燥二氟磷酸盐，或使氟化氢与含有杂质的二氟磷酸盐接触，同时加热和干燥含二氟磷酸盐 杂质，从而除去杂质。
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公开(公告)号：US09156747B2
公开(公告)日：2015-10-13
申请号：US13796776
申请日：2013-03-12
申请人： UOP LLC
CPC分类号： C07C2/56 , B01J31/0288 , B01J31/0298 , B01J2231/44 , C07C2/60 , C07C2527/125 , C07C2531/02 , C07C9/16
摘要： A process for making an alkylate is presented. The process includes mixing an isoparaffin stream with an olefin stream in an alkylation reactor. The alkylation reactor includes a catalyst for performing the reaction. The catalyst is an ionic liquid that is a quaternary phosphonium based ionic liquid, and the reaction is performed at or near ambient temperatures.
摘要翻译： 提出了制备烷基化物的方法。 该方法包括在烷基化反应器中将异链烷烃流与烯烃物流混合。 烷基化反应器包括用于进行反应的催化剂。 催化剂是基于季鏻的离子液体的离子液体，反应在环境温度或接近环境温度下进行。
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64.发明授权Regeneration of an acidic ionic liquid catalyst by addition of brønsted acids 有权通过添加布朗斯台德酸来再生酸性离子液体催化剂公开(公告)号：US09079176B1
公开(公告)日：2015-07-14
申请号：US14229329
申请日：2014-03-28
申请人： UOP LLC
CPC分类号： B01J31/4053 , B01J31/0277 , B01J31/0288 , B01J31/26 , B01J31/4092 , B01J2231/323 , C07C2/60 , C07C2527/125 , C07C2531/02 , Y02P20/584 , C07C9/16
摘要： A method for regenerating deactivated acidic ionic liquid catalyst containing conjunct polymer is described. The method includes contacting the deactivated acidic ionic liquid catalyst containing the conjunct polymer with at least one Brønsted acid in a regeneration zone under regeneration conditions, resulting in a mixture comprising regenerated acidic ionic liquid catalyst, the Brønsted acid, the released conjunct polymer. The Brønsted acid is derived from a mineral acid and contains at least one organic group. The released conjunct polymer can be separated from the regenerated acidic ionic liquid catalyst and the at least one Brønsted acid.
摘要翻译： 描述了一种用于再生含有结合聚合物的失活酸性离子液体催化剂的方法。 该方法包括在再生条件下将含有结合聚合物的失活的酸性离子液体催化剂与再生区中的至少一种布朗斯台德酸接触，得到包含再生酸性离子液体催化剂布朗斯台德酸，释放的结合聚合物的混合物。 布朗斯台德酸衍生自无机酸，并含有至少一个有机基团。 释放的结合聚合物可以与再生的酸性离子液体催化剂和至少一种布朗斯台德酸分离。
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公开(公告)号：US20150165430A1
公开(公告)日：2015-06-18
申请号：US14632366
申请日：2015-02-26
申请人： Chevron U.S.A. Inc.
IPC分类号： B01J31/40 , B01J35/12 , C07D213/20 , B01J38/54 , C01B17/90 , B01J27/30 , B01J31/02 , B01J38/50
CPC分类号： B01J31/4092 , B01J27/30 , B01J27/32 , B01J31/0284 , B01J31/0288 , B01J31/0298 , B01J35/12 , B01J38/50 , B01J38/54 , B01J2231/12 , B01J2231/20 , B01J2231/4205 , B01J2231/44 , B01J2531/31 , C01B17/905 , C07D213/20 , Y02P20/584
摘要： We provide a process for regenerating a used acidic ionic liquid catalyst which has been deactivated by conjunct polymers in a reactor, by removing at least 57 wt % of the conjunct polymers originally present in the used acidic ionic liquid catalyst in a separate regeneration reactor, so as to increase the activity of the catalyst. We also provide a regenerated used acidic ionic liquid catalyst having increased activity.
摘要翻译： 我们提供一种再生使用的酸性离子液体催化剂的方法，其通过在反应器中通过结合聚合物失活，通过除去至少57重量％的原始存在于使用的酸性离子液体催化剂中的结合聚合物在另外的再生反应器中，因此 以增加催化剂的活性。 我们还提供一种具有增加的活性的再生使用的酸性离子液体催化剂。
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66.发明申请PROCESS FOR REDUCING CHLORIDE IN HYDROCARBON PRODUCTS USING AN IONIC LIQUID CATALYST 有权使用离子液体催化剂在碳氢化合物产品中还原氯化物的方法公开(公告)号：US20140171720A1
公开(公告)日：2014-06-19
申请号：US13715873
申请日：2012-12-14
IPC分类号： C07C7/10
CPC分类号： C07C7/10 , B01D3/009 , B01J31/0284 , B01J31/0288 , B01J31/0289 , B01J31/26 , B01J2231/64 , C10G29/16
摘要： We provide a process comprising: a. feeding a chlorinated-hydrocarbon and an ionic liquid catalyst to a treatment unit; b. operating the treatment unit at an elevated temperature to produce dechlorinated-hydrocarbon and HCl; and c. collecting the dechlorinated-hydrocarbon, wherein at least 90 wt % of the chlorides are removed. A second process comprises: a. creating an ionic liquid catalyst-rich zone in a distillation unit; b. passing chlorinated-hydrocarbon to the distillation unit; c. operating the unit under conditions causing removal of alkyl chloride to produce dechlorinated-hydrocarbon having a final boiling point close to a first final boiling point. A third process comprises: a. feeding alkylate gasoline blending component and ionic liquid catalyst to a treatment unit; b. operating the treatment unit; and c. collecting a dechlorinated-hydrocarbon, wherein at least 90 wt % of the chlorides have been removed and the dechlorinated-hydrocarbon has a second RON that is close to a first RON.
摘要翻译： 我们提供一个过程，包括：a。 将氯代烃和离子液体催化剂供给到处理单元; b。 在升高的温度下操作处理单元以产生脱氯烃和HCl; 和c。 收集脱氯烃，其中除去至少90重量％的氯化物。 第二个过程包括：a。 在蒸馏单元中产生离子液体催化剂富集区; b。 将氯化烃通入蒸馏单元; C。 在引起去除烷基氯的条件下操作该单元以产生具有接近第一最终沸点的最终沸点的脱氯烃。 第三个过程包括：a。 将烷基化汽油调和组分和离子液体催化剂加入到处理单元中; b。 操作治疗单元; 和c。 收集脱氯烃，其中已除去至少90重量％的氯化物，脱氯烃具有接近第一RON的第二RON。
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公开(公告)号：US20130345483A1
公开(公告)日：2013-12-26
申请号：US13796776
申请日：2013-03-12
申请人： UOP LLC
IPC分类号： C07C2/56
CPC分类号： C07C2/56 , B01J31/0288 , B01J31/0298 , B01J2231/44 , C07C2/60 , C07C2527/125 , C07C2531/02 , C07C9/16
摘要： A process for making an alkylate is presented. The process includes mixing an isoparaffin stream with an olefin stream in an alkylation reactor. The alkylation reactor includes a catalyst for performing the reaction. The catalyst is an ionic liquid that is a quaternary phosphonium based ionic liquid, and the reaction is performed at or near ambient temperatures.
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公开(公告)号：US20130303358A1
公开(公告)日：2013-11-14
申请号：US13938026
申请日：2013-07-09
IPC分类号： B01J27/32
CPC分类号： B01J31/4092 , B01J27/30 , B01J27/32 , B01J31/0284 , B01J31/0288 , B01J31/0298 , B01J35/12 , B01J38/50 , B01J38/54 , B01J2231/12 , B01J2231/20 , B01J2231/4205 , B01J2231/44 , B01J2531/31 , C01B17/905 , C07D213/20 , Y02P20/584
摘要： We provide a process for regenerating a used acidic ionic liquid catalyst which has been deactivated by conjunct polymers in a reactor, by removing at least 57 wt % of the conjunct polymers originally present in the used acidic ionic liquid catalyst in a separate regeneration reactor, so as to increase the activity of the catalyst. We also provide a regenerated used acidic ionic liquid catalyst having increased activity.
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69.发明申请CATALYTIC COMPOSITION CONTAINING AN ACID FUNCTION AND A PROCESS FOR THE SELECTIVE DIMERIZATION OF ISOBUTENE 审中-公开含有酸性功能的催化组合物及其选择性分级方法公开(公告)号：US20130137912A1
公开(公告)日：2013-05-30
申请号：US13688308
申请日：2012-11-29
CPC分类号： B01J31/0298 , B01J31/0279 , B01J31/0284 , B01J31/0285 , B01J31/0288 , B01J31/0289 , B01J31/0291 , B01J2231/20 , C07C2/08
摘要： Catalytic composition comprising at least one non-aqueous ionic liquid medium of general formula Q1+A1−, in which Q1+ represents an organic cation and A1− represents an anion, and at least one ionic component of general formula Q2+A2−, in which Q2+ represents an organic cation comprising at least one sulphonic acid or carboxylic acid function, and A2− represents an anion. The invention also relates to an isobutene dimerization process using the catalytic composition.
摘要翻译： 包含至少一种通式Q1 + A1-的非水离子液体介质的催化组合物，其中Q1 +表示有机阳离子，A1-表示阴离子，以及至少一种通式为Q2 + A2-的离子组分，其中 Q2 +表示包含至少一种磺酸或羧酸官能团的有机阳离子，而A2-表示阴离子。 本发明还涉及使用催化组合物的异丁烯二聚方法。
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70.发明申请公开(公告)号：US20130137911A1
公开(公告)日：2013-05-30
申请号：US13688591
申请日：2012-11-29
CPC分类号： B01J31/0291 , B01J31/0235 , B01J31/0279 , B01J31/0284 , B01J31/0285 , B01J31/0288 , B01J31/0289 , B01J2231/20 , C07C2/14
摘要： Catalytic composition comprising at least one Brønsted acid, designated HB, dissolved in a non-aqueous liquid medium of general formula Q1+A1−, in which Q1+ represents an organic cation and A1− represents an anion, said composition also comprising an additive Q2+A2− in which Q2+ represents an organic cation containing at least one alcohol function and A2− represents an anion. The invention also relates to an isobutene dimerization process using the catalytic composition.
摘要翻译： 催化组合物，其包含溶解在通式Q1 + A1-的非水性液体介质中的至少一种布朗斯台德酸，其中Q1 +表示有机阳离子，A1-表示阴离子，所述组合物还包含添加剂Q2 + A2-其中Q2 +表示含有至少一个醇官能团的有机阳离子，而A2-表示阴离子。 本发明还涉及使用催化组合物的异丁烯二聚方法。
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