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公开(公告)号：US20170080408A1
公开(公告)日：2017-03-23
申请号：US15125370
申请日：2015-02-26
Applicant: Dow Global Technologies LLC
Inventor： David C. Molzahn , Michael L. Tulchinsky
CPC classification number: B01J23/96 , B01J21/18 , B01J23/46 , B01J23/464 , B01J35/006 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1028 , B01J35/1061 , B01J38/54 , B01J38/70 , C07D301/00 , C07D303/22 , Y02P20/584
Abstract: A process for at least partially reactivating the catalytic activity of at least a partially deactivated catalyst following a reaction cycle, the catalyst having been used in a catalytic reaction process for hydrogenating an aromatic epoxide to produce a hydrogenated aliphatic epoxide; said process including contacting the at least partially deactivated catalyst with an oxygen-containing source at a temperature of less than about 100° C. and in the presence of a reactivation solvent for a pre-determined period of time sufficient to at least partially re-oxidize and reactivate the catalyst for further use; and a catalytic reaction process for hydrogenating an aromatic epoxide to produce a hydrogenated aliphatic epoxide including the above reactivating process step; and optionally including a step for washing the deactivated catalyst with a solvent prior to re-oxidizing the deactivated catalyst.
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公开(公告)号：US09421529B2
公开(公告)日：2016-08-23
申请号：US14159187
申请日：2014-01-20
Applicant: Chevron Phillips Chemical Company LP
Inventor： An-Hsiang Wu
IPC: B01J29/90 , B01J23/96 , B01J37/24 , B01J37/26 , B01J38/12 , B01J38/44 , B01J38/46 , B01J38/54 , C10G45/68 , B01J29/62
CPC classification number: B01J29/90 , B01J23/96 , B01J29/62 , B01J37/24 , B01J37/26 , B01J38/12 , B01J38/44 , B01J38/46 , B01J38/54 , B01J2229/42 , C10G45/68
Abstract: A method of reactivating a spent catalyst comprising a metal and a catalyst support, the method comprising redispersing the metal in the spent catalyst to produce a redispersed spent catalyst, contacting the redispersed spent catalyst with a reactivating composition to produce a redispersed, reactivated spent catalyst, and thermally treating the redispersed, reactivated spent catalyst to produce a reactivated catalyst. A method comprising employing a fresh aromatization catalyst in one or more reaction zones for a time period sufficient to produce a spent catalyst, reducing the amount of carbonaceous material associated with the spent catalyst to produce a decoked spent catalyst, contacting the decoked spent catalyst with a redispersing composition to produce a decoked redispersed spent, contacting the decoked redispersed spent catalyst with a reactivating composition to produce a decoked redispersed reactivated spent catalyst, and thermally treating the decoked, reactivated spent catalyst to produce a reactivated catalyst.
Abstract translation: 一种重新激活包含金属和催化剂载体的废催化剂的方法，所述方法包括将废金属重新分散在废催化剂中以产生再分散的废催化剂，使再分散的废催化剂与再活化组合物接触以产生再分散的再活化的废催化剂， 并对再分散的再活化的废催化剂进行热处理以产生再活化的催化剂。 一种方法，包括在一个或多个反应区中使用新鲜的芳构化催化剂足以产生废催化剂的时间段，减少与废催化剂相关的碳质材料的量以产生经过处理的废催化剂，将经过处理的废催化剂与 再分散组合物以产生经过重新分配的再分散的废料，使经过重新分离的废催化剂与再活化组合物接触，以产生经过重新分离的再分解的再生废催化剂，并热处理所述经切割的再活化的废催化剂以产生再活化的催化剂。
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公开(公告)号：US20150360219A1
公开(公告)日：2015-12-17
申请号：US14834677
申请日：2015-08-25
Applicant: ARCHER DANIELS MIDLAND COMPANY
Inventor： ChiCheng Ma
IPC: B01J38/48 , B01J23/46 , B01J23/755 , B01J38/64 , B01J25/04 , B01J23/94 , B01J23/96 , C07C29/141 , B01J25/02
CPC classification number: B01J38/48 , B01J21/18 , B01J23/462 , B01J23/755 , B01J23/94 , B01J23/96 , B01J25/02 , B01J25/04 , B01J38/06 , B01J38/54 , B01J38/60 , B01J38/64 , B01J38/70 , C07C29/132 , C07C29/141 , C10G3/50 , C10G3/62 , Y02P30/20
Abstract: A process for regenerating catalysts that have been deactivated or poisoned during hydrogenation of biomass, sugars and polysaccharides is described, in which polymerized species that have agglomerated to catalyst surfaces can be removed by means of washing the catalyst with hot water at subcritical temperatures. A feature of the process can regenerate the catalysts in situ, which allows the process to be adapted for used in continuous throughput reactor systems. Also described is a continuous hydrogenation process that incorporated the present regeneration process.
Abstract translation: 描述了在生物质，糖和多糖的氢化期间已经失活或中毒的催化剂的再生方法，其中可以通过在亚临界温度下用热水洗涤催化剂来除去已经凝聚到催化剂表面的聚合物质。 该方法的特征可以原位再生催化剂，这允许该方法适用于连续生产反应器系统中。 还描述了结合本发明再生方法的连续氢化方法。
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公开(公告)号：US20150165430A1
公开(公告)日：2015-06-18
申请号：US14632366
申请日：2015-02-26
Applicant: Chevron U.S.A. Inc.
Inventor： Saleh Ali Elomari , Thomas Van Harris
CPC classification number: B01J31/4092 , B01J27/30 , B01J27/32 , B01J31/0284 , B01J31/0288 , B01J31/0298 , B01J35/12 , B01J38/50 , B01J38/54 , B01J2231/12 , B01J2231/20 , B01J2231/4205 , B01J2231/44 , B01J2531/31 , C01B17/905 , C07D213/20 , Y02P20/584
Abstract: We provide a process for regenerating a used acidic ionic liquid catalyst which has been deactivated by conjunct polymers in a reactor, by removing at least 57 wt % of the conjunct polymers originally present in the used acidic ionic liquid catalyst in a separate regeneration reactor, so as to increase the activity of the catalyst. We also provide a regenerated used acidic ionic liquid catalyst having increased activity.
Abstract translation: 我们提供一种再生使用的酸性离子液体催化剂的方法，其通过在反应器中通过结合聚合物失活，通过除去至少57重量％的原始存在于使用的酸性离子液体催化剂中的结合聚合物在另外的再生反应器中，因此 以增加催化剂的活性。 我们还提供一种具有增加的活性的再生使用的酸性离子液体催化剂。
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公开(公告)号：US08664144B2
公开(公告)日：2014-03-04
申请号：US12617440
申请日：2009-11-12
Applicant: An-Hsiang Wu
Inventor： An-Hsiang Wu
IPC: B01J29/04 , B01J29/87 , B01J21/00 , B01J23/00 , B01J25/00 , B01J29/00 , B01J27/06 , B01J27/128 , B01J27/13
CPC classification number: B01J29/90 , B01J23/96 , B01J29/62 , B01J37/24 , B01J37/26 , B01J38/12 , B01J38/44 , B01J38/46 , B01J38/54 , B01J2229/42 , C10G45/68
Abstract: A method of reactivating a spent catalyst comprising a metal and a catalyst support, the method comprising redispersing the metal in the spent catalyst to produce a redispersed spent catalyst, contacting the redispersed spent catalyst with a reactivating composition to produce a redispersed, reactivated spent catalyst, and thermally treating the redispersed, reactivated spent catalyst to produce a reactivated catalyst. A method comprising employing a fresh aromatization catalyst in one or more reaction zones for a time period sufficient to produce a spent catalyst, reducing the amount of carbonaceous material associated with the spent catalyst to produce a decoked spent catalyst, contacting the decoked spent catalyst with a redispersing composition to produce a decoked redispersed spent, contacting the decoked redispersed spent catalyst with a reactivating composition to produce a decoked redispersed reactivated spent catalyst, and thermally treating the decoked, reactivated spent catalyst to produce a reactivated catalyst.
Abstract translation: 一种重新激活包含金属和催化剂载体的废催化剂的方法，所述方法包括将废金属重新分散在废催化剂中以产生再分散的废催化剂，使再分散的废催化剂与再活化组合物接触以产生再分散的再活化的废催化剂， 并对再分散的再活化的废催化剂进行热处理以产生再活化的催化剂。 一种方法，包括在一个或多个反应区中使用新鲜的芳构化催化剂足以产生废催化剂的时间段，减少与废催化剂相关的碳质材料的量以产生经过处理的废催化剂，将经过处理的废催化剂与 再分散组合物以产生经过重新分配的再分散的废料，使经过重新分离的废催化剂与再活化组合物接触，以产生经过重新分离的再分解的再生废催化剂，并热处理所述经切割的再活化的废催化剂以产生再活化的催化剂。
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Patent Agency Ranking
公开(公告)号：US20130303358A1
公开(公告)日：2013-11-14
申请号：US13938026
申请日：2013-07-09
Applicant: Saleh Ali Elomari , Thomas Van Harris
Inventor： Saleh Ali Elomari , Thomas Van Harris
IPC: B01J27/32
CPC classification number: B01J31/4092 , B01J27/30 , B01J27/32 , B01J31/0284 , B01J31/0288 , B01J31/0298 , B01J35/12 , B01J38/50 , B01J38/54 , B01J2231/12 , B01J2231/20 , B01J2231/4205 , B01J2231/44 , B01J2531/31 , C01B17/905 , C07D213/20 , Y02P20/584
Abstract: We provide a process for regenerating a used acidic ionic liquid catalyst which has been deactivated by conjunct polymers in a reactor, by removing at least 57 wt % of the conjunct polymers originally present in the used acidic ionic liquid catalyst in a separate regeneration reactor, so as to increase the activity of the catalyst. We also provide a regenerated used acidic ionic liquid catalyst having increased activity.
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公开(公告)号：US12128393B2
公开(公告)日：2024-10-29
申请号：US17441358
申请日：2019-11-19
Applicant: Mitsubishi Power, Ltd.
Inventor： Kazuhiro Iwamoto , Masanao Yonemura , Katsumi Nochi , Yoshiharu Watanabe , Masanori Demoto
Abstract: Provided are a denitration catalyst regeneration method and a denitration catalyst regeneration system, which are capable of recovering denitration performance to a high level and reducing the SO2 oxidation rate of a catalyst. A denitration catalyst regeneration method according to the present invention includes: a chemical solution cleaning step for immersing a denitration catalyst in a chemical solution containing a fluorine compound and an inorganic acid; a step for extracting the denitration catalyst from the chemical solution; and a finish washing step for washing the denitration catalyst extracted from the chemical solution with a finish cleaning solution containing an organic acid.
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8.发明申请公开(公告)号：US20190247833A1
公开(公告)日：2019-08-15
申请号：US16391385
申请日：2019-04-23
Applicant: Chevron Phillips Chemical Company LP
Inventor： Ryan W. Snell , Gabriela D. Alvez-Manoli
IPC: B01J23/96 , C10G35/085 , B01J38/12 , C10G35/04 , B01J38/46 , C10G35/095 , B01J38/42 , B01J38/48 , B01J29/62 , B01J29/90 , C07C5/41 , B01J38/04 , B01J38/10 , B01J38/02 , B01J38/54 , B01J38/66 , B01J38/44 , B01J35/00 , B01J29/70 , B01J23/42 , C10G35/06
CPC classification number: B01J23/96 , B01J23/42 , B01J29/62 , B01J29/70 , B01J29/90 , B01J35/0006 , B01J38/02 , B01J38/04 , B01J38/10 , B01J38/12 , B01J38/42 , B01J38/44 , B01J38/46 , B01J38/48 , B01J38/54 , B01J38/66 , C07C5/412 , C07C5/415 , C07C5/417 , C07C2523/42 , C07C2529/068 , C07C2529/60 , C07C2529/62 , C10G35/04 , C10G35/06 , C10G35/085 , C10G35/095 , C10G2300/4037
Abstract: Methods for regenerating a spent catalyst are disclosed. Such methods may employ a step of chlorinating the spent catalyst in the gas phase, followed by decoking the chlorinated spent catalyst, and then fluorinating the de-coked catalyst in a fluorine-containing solution of a fluorine-containing compound.
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公开(公告)号：US09687839B2
公开(公告)日：2017-06-27
申请号：US15223401
申请日：2016-07-29
Applicant: Archer Daniels Midland Company
Inventor： ChiCheng Ma
IPC: C07C29/132 , B01J38/48 , B01J23/94 , C10G3/00 , B01J38/54 , B01J21/18 , B01J23/46 , B01J23/96 , B01J25/02 , B01J25/04 , B01J23/755 , B01J38/64 , C07C29/141 , B01J38/06 , B01J38/70 , B01J38/60
CPC classification number: B01J38/48 , B01J21/18 , B01J23/462 , B01J23/755 , B01J23/94 , B01J23/96 , B01J25/02 , B01J25/04 , B01J38/06 , B01J38/54 , B01J38/60 , B01J38/64 , B01J38/70 , C07C29/132 , C07C29/141 , C10G3/50 , C10G3/62 , Y02P30/20
Abstract: A process for regenerating catalysts that have been deactivated or poisoned during hydrogenation of biomass, sugars and polysaccharides is described, in which polymerized species that have agglomerated to catalyst surfaces can be removed by means of washing the catalyst with hot water at subcritical temperatures. A feature of the process can regenerate the catalysts in situ, which allows the process to be adapted for used in continuous throughput reactor systems. Also described is a continuous hydrogenation process that incorporated the present regeneration process.
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10.发明申请PROCESS FOR THE OXIDATION OF HYDROGEN CHLORIDE OVER A CATALYST HAVING A LOW SURFACE ROUGHNESS 审中-公开通过具有低表面粗糙度的催化剂氧化氢氯化物的方法公开(公告)号：US20150360210A1
公开(公告)日：2015-12-17
申请号：US14834947
申请日：2015-08-25
Applicant: BASF SE
Inventor： Guido Henze , Heiko Urtel , Martin Sesing , Martin Karches , Peter Van Den Abeel , Kai Thiele
CPC classification number: B01J23/96 , B01J21/04 , B01J21/20 , B01J23/462 , B01J23/892 , B01J23/8933 , B01J35/023 , B01J35/10 , B01J37/0201 , B01J38/42 , B01J38/54 , B01J38/68 , C01B7/04 , Y02P20/584
Abstract: The invention relates to a process for the catalytic oxidation of hydrogen chloride by means of oxygen to form chlorine in a fluidized-bed process in the presence of a catalyst comprising ruthenium on a particulate support composed of alpha-aluminum oxide having an average particle size of from 10 to 200 μm, wherein the catalyst support has a low surface roughness and can be obtained from a used catalyst which has been used in a fluidized-bed process for at least 500 hours of operation.
Abstract translation: 本发明涉及一种在流化床方法中，在包含钌的催化剂存在下，通过氧气催化氧化氯化氢以形成氯的方法，该催化剂由颗粒载体组成，所述颗粒载体由平均粒径为 10至200μm，其中催化剂载体具有低的表面粗糙度，并且可以从在流化床方法中使用的使用的催化剂获得至少500小时的操作。
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