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    Liquid crystalline diketopyrrolopyrroles
    72.
    发明授权
    Liquid crystalline diketopyrrolopyrroles 失效
    液晶二酮吡咯并吡咯

    公开(公告)号：US5969154A

    公开(公告)日：1999-10-19

    申请号：US988419

    申请日：1997-12-10

    申请人： Zhimin Hao ,  Abul Iqbal ,  Nancy Tebaldi ,  Klaus Praefcke

    发明人： Zhimin Hao ,  Abul Iqbal ,  Nancy Tebaldi ,  Klaus Praefcke

    IPC分类号： C07D487/04 ,  C09K19/34 ,  C07D317/12 ,  C07D319/06

    CPC分类号： C07D487/04 ,  C09K19/3483

    摘要： A liquid crystalline compound of formula ##STR1## wherein B and D are each independently of the other C.sub.6 -C.sub.24 alkyl, ##STR2## L is ##STR3## methyl or C.sub.10 -C.sub.18 alkyl, wherein R.sub.1 is C.sub.4 -C.sub.18 alkyl, with the proviso that when L is methyl, at least one of B and D is C.sub.6 -C.sub.24 alkyl;R2 is hydrogen, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, halogen, cyano or nitro,R3, R4 and R5 are each independently of one another hydrogen, OR6, SR6, SeR6, --NHR6, --NR6R7, ##STR4## with the proviso that at least one of R3, R4 and R5 is not hydrogen, R6 is C.sub.7 -C.sub.37 alkyl, C.sub.7 -C.sub.37 alkylene or C.sub.5 -C.sub.18 alkyl which is interrupted by 1 to 6 hetero atoms selected from the group consisting of O, S and N,R7 is hydrogen or R9,R8 is hydrogen or C.sub.1 -C.sub.4 alkyl, andR9 is C.sub.1 -C.sub.12 alkyl, C.sub.2 -C.sub.12 alkylene or C.sub.3 -C.sub.12 alkyl which is interrupted by 1 to 6 hetero atoms selected from the group consisting of O, S and N.

    摘要翻译： 一种下式的液晶化合物，其中B和D各自独立于C 6 -C 24烷基，L是甲基或C 10 -C 18烷基，其中R 1是C 4 -C 18烷基，条件是当L是甲基时，B和 D是C 6 -C 24烷基; R 2是氢，C 1 -C 4烷基，C 1 -C 4烷氧基，卤素，氰基或硝基，R 3，R 4和R 5各自彼此独立地是氢，OR 6，SR 6，SeR 6，-NHR 6，-NR 6 R 7，条件是至少一个 的R 3，R 4和R 5不是氢，R 6是被1至6个选自O，S和N的杂原子间隔的C 7 -C 37烷基，C 7 -C 37亚烷基或C 5 -C 18烷基，R 7是氢或R 9， R8为氢或C1-C4烷基，R9为C1-C12烷基，C2-C12亚烷基或C3-C12烷基，其被1至6个选自O，S和N的杂原子间隔。

    Monophase solid solutions containing asymmetric pyrrolo �4,3-c! pyrroles as hosts
    76.
    发明授权
    Monophase solid solutions containing asymmetric pyrrolo �4,3-c! pyrroles as hosts 失效
    含有不对称吡咯并[4,3-c]吡咯的单相固溶体作为宿主

    公开(公告)号：US5756746A

    公开(公告)日：1998-05-26

    申请号：US700349

    申请日：1996-09-23

    申请人： Zhimin Hao ,  Abul Iqbal

    发明人： Zhimin Hao ,  Abul Iqbal

    IPC分类号： C07D487/04 ,  C07D471/04 ,  C08K5/3412 ,  C08K5/3415 ,  C08K5/3417 ,  C08K5/3437 ,  C08L101/00 ,  C09B67/22 ,  C07D209/00 ,  C09B67/52

    CPC分类号： C08K5/3415 ,  C09B67/0033

    摘要： The present invention relates to a solid solution consisting of 60-90 mol-% of an asymmetric 2,5-dihydro-1,4-diketopyrrolo�3,4-c!pyrrole of the formula (I) ##STR1## in which G.sub.1 and G.sub.2 independently of one another are different substituted or unsubstituted aromatic radicals or pyridyl, but the volume of all substituents on G.sub.1 and G.sub.2 is greater than that of two methyl groups; and 40-10 mol-% of a 2,5-dihydro-1,4-diketopyrrolo�3,4-c!pyrrole of the formula (IIa) ##STR2## in which G.sub.3 and G.sub.4 independently of one another are different substituted or unsubstituted aromatic radicals or pyridyl, but the volume of all substituents on G.sub.3 and G.sub.4 is less than that of two butoxy groups; or 40-10 mol-% of a quinacridone of the formula (IIb) ##STR3## in which R.sub.9 is hydrogen, halogen, C.sub.1 -C.sub.4 alkyl or C.sub.1 -C.sub.4 alkoxy; which is a single-phase solid solution having the crystal structure of the asymmetric 2,5-dihydro-1,4-diketopyrrolo�3,4-c!pyrrole of the formula (I).

    摘要翻译： 本发明涉及由60-90mol％的式（I）的不对称2,5-二氢-1,4-二酮吡咯并[3,4-c]吡咯组成的固溶体。 其中G1和G2彼此独立地是不同的取代或未取代的芳族基团或吡啶基，但是G1和G2上所有取代基的体积大于两个甲基的取代基的体积; 和其中G3和G4彼此独立的式（IIa）（IIa）的2,5-二氢-1,4-二酮基吡咯并[3,4-c]吡咯和40-10摩尔％ 不同的取代或未取代的芳族基团或吡啶基，但是G3和G4上所有取代基的体积小于两个丁氧基的取代基的体积; 或者40-10摩尔％的式（IIb）的喹吖啶酮（IIb），其中R9是氢，卤素，C1-C4烷基或C1-C4烷氧基; 其是具有式（I）的不对称2,5-二氢-1,4-二酮基吡咯并[3,4-c]吡咯的晶体结构的单相固溶体。

    Isoindoline compounds and the manufacture and use thereof
    78.
    发明授权
    Isoindoline compounds and the manufacture and use thereof 失效
    异二氢吲哚化合物及其制备和应用

    公开(公告)号：US4385174A

    公开(公告)日：1983-05-24

    申请号：US242005

    申请日：1981-03-09

    申请人： Abul Iqbal ,  Paul Lienhard

    发明人： Abul Iqbal ,  Paul Lienhard

    IPC分类号： C07D209/44 ,  C07D403/06 ,  C07D413/06 ,  C07D417/06 ,  C09B26/02 ,  C09B57/04 ,  C07D403/12 ,  C07D413/12 ,  C07D417/12

    CPC分类号： C09B57/04 ,  C07D209/44 ,  C09B26/02

    摘要： The invention relates to a simplified process for the manufacture of 1:1 metal complexes of isoindoline azines of the formula ##STR1## wherein R is hydrogen, alkyl or aryl, Q contains an isocyclic or heterocyclic radical, acyl, carbamoyl or thiocarbamoyl, and Y is the radical of an active methylene group or aromatic amine, which comprises reacting a compound HQ or a hydrazone with an ortho ester or amidine in the presence of a metal donor at elevated temperature in a polar solvent. Pigments made by this process are lightfast and are useful in coloring plastics.

    摘要翻译： 本发明涉及用于制备式（1）的异吲哚啉吖嗪的1:1金属络合物的简化方法，其中R是氢，烷基或芳基，Q包含一个或多个杂环基，酰基，氨基甲酰基或硫代氨基甲酰基 并且Y是活性亚甲基或芳族胺的基团，其包括在金属供体存在下，在高温下在极性溶剂中使化合物HQ或腙与原酸酯或脒反应。 通过该方法制备的颜料是耐光的并且可用于着色塑料。