REACTOR AND MULTIFUNCTIONAL RISER AND DOWNER SIMULATOR INCORPORATING THE SAME

    公开(公告)号:US20170320036A1

    公开(公告)日:2017-11-09

    申请号:US15585780

    申请日:2017-05-03

    Inventor: Hugo de Lasa

    Abstract: A reactor comprises a reactor vessel defining a confined reactor volume, a support assembly extending about a periphery of the confined reactor volume, a basket positioned within the reactor vessel and supported by the support assembly, the basket having an interior surface and an exterior surface, a downflow zone being defined between the exterior surface of the basket and an interior surface of the confined reactor volume, an inlet screen positioned adjacent to one end of the interior surface and an outlet screen positioned adjacent to an opposite end of the interior surface, an upflow zone defined between the inlet screen and outlet screen, the inlet screen and the outlet screen containing a quantity of particulate catalyst, and a circulating device positioned above said upflow zone and configured to continuously circulate fluid upwardly though said upflow zone and downwardly through said downflow zone, the support assembly and the basket configured to promote the formation of a fluid vortex within a portion of the downflow zone.

    INTEGRATED CYCLONE ASSEMBLY
    75.
    发明申请
    INTEGRATED CYCLONE ASSEMBLY 有权
    集成圆环组件

    公开(公告)号:US20150158002A1

    公开(公告)日:2015-06-11

    申请号:US14097522

    申请日:2013-12-05

    Abstract: Integrated primary and secondary cyclone assembly includes a secondary cyclone having an outlet tube extending therefrom and a primary cyclone operatively coupled with the secondary cyclone. The outlet tube has a cross dimension and length and is configured to be secured to a pressure vessel closure head to support the secondary cyclone therefrom. The primary cyclone has a tubular support member extending therefrom. The tubular support member is aligned substantially parallel with and has a length similar to the outlet tube of the secondary cyclone and is configured to be joined to the pressure vessel closure head to support the primary cyclone therefrom.

    Abstract translation: 集成的初级和次级旋风组件包括具有从其延伸的出口管的次级旋风器和与次级旋风器可操作地连接的主旋流器。 出口管具有十字尺寸和长度,并且构造成固定到压力容器封闭头以从其支撑第二旋风分离器。 主旋风器具有从其延伸的管状支撑构件。 管状支撑构件与第二旋风分离器的出口管基本上平行并具有长度,并且构造成连接到压力容器闭合头以支撑主旋流器。

    Acetic anhydride production by way of carbonylation with enhanced reaction and flashing
    76.
    发明授权
    Acetic anhydride production by way of carbonylation with enhanced reaction and flashing 有权
    通过羰基化反应生成乙酸酐,反应和闪烁

    公开(公告)号:US08455685B2

    公开(公告)日:2013-06-04

    申请号:US12924429

    申请日:2010-09-27

    Applicant: Mark O. Scates

    Inventor: Mark O. Scates

    Abstract: A method of making acetic anhydride or a mixture of acetic anhydride and acetic acid comprising: (a) catalytically reacting a feedstock containing methyl acetate and/or dimethyl ether with carbon monoxide in the presence of a homogeneous rhodium catalyst and methyl iodide in a reactor vessel which contains a substantially anhydrous liquid reaction mixture including acetic acid, acetic anhydride, methyl acetate and/or dimethyl ether, methyl iodide and the homogeneous catalyst, the reactor vessel being operated at a reactor pressure; (b) withdrawing reaction mixture from the reaction vessel and feeding the withdrawn reaction mixture along with additional carbon monoxide to a pre-flasher/post reactor vessel operated at a reduced pressure below the reactor vessel pressure; (c) venting light ends in the pre-flasher vessel and concurrently consuming methyl acetate and/or dimethyl ether in the pre-flasher/post reactor vessel to produce a pre-flash mixture which is enriched in acetic anhydride and diminished in methyl iodide and methyl acetate and/or dimethyl ether as compared with the reaction mixture; (d) withdrawing the pre-flash reaction mixture from the pre-flasher/post reactor vessel and feeding the pre-flash mixture to a flash vessel; and (e) flashing a crude product stream from the mixture in a flash vessel operated at a pressure substantially below the pressure of the pre-flasher/post reactor vessel.

    Abstract translation: 一种制备乙酸酐或乙酸酐和乙酸的混合物的方法,包括:(a)在均匀的铑催化剂和甲基碘存在下在反应器容器中催化反应含有乙酸甲酯和/或二甲醚的原料与一氧化碳 其包含基本上无水的液体反应混合物,包括乙酸,乙酸酐,乙酸甲酯和/或二甲醚,甲基碘和均相催化剂,反应器容器在反应器压力下操作; (b)从反应容器中取出反应混合物,并将排出的反应混合物与另外的一氧化碳一起送入反应器/反应器前的反应器容器中,该反应器容器在低于反应器容器压力的压力下操作; (c)在预闪蒸器容器内放出轻质的末端,同时在预闪蒸发器/反应器容器中消耗乙酸甲酯和/或二甲醚,以产生富含乙酸酐并在甲基碘中减少的预闪蒸混合物, 与反应混合物相比,乙酸甲酯和/或二甲醚; (d)将预闪蒸反应混合物从预闪蒸发器/反应堆容器中取出并将预闪蒸混合物送入闪蒸容器; 和(e)在以基本上低于预闪蒸发器/反应器反应器容器的压力的压力下操作的闪蒸容器中从混合物中闪蒸粗产物流。

    Apparatus for high temperature hydrolysis of water reactive halosilanes and halides and process for making same
    80.
    发明申请
    Apparatus for high temperature hydrolysis of water reactive halosilanes and halides and process for making same 审中-公开
    用于水反应性卤代硅烷和卤化物的高温水解的装置及其制备方法

    公开(公告)号:US20100061912A1

    公开(公告)日:2010-03-11

    申请号:US12283077

    申请日:2008-09-08

    Abstract: A process for high temperature hydrolysis of halosilanes and halides with the steps of: providing a bed of fluidized particulate material heated to at least 300° C., injecting steam and an excess of reactants into the reactor, removing solid waste from a bottom outlet, removing the effluent gases through a solids removal device such as a cyclone, condensing and separating some of the unreacted waste from the effluent gas in a distillation column and sending the effluent gases containing hydrogen and hydrogen chloride to a compressor. In a preferred embodiment the reactants contain at least one water reactive halide, selected from the group halosilane, organohalosilane, aluminum halide, titanium halide, boron halide, manganese halide, copper halide, iron halide, chromium halide, nickel halide, indium halide, gallium halide and phosphorus halide and where the halide content is selected from chlorine, bromine and iodine.

    Abstract translation: 一种用于卤代硅烷和卤化物的高温水解的方法,其步骤为:提供加热到至少300℃的流化颗粒材料床,将蒸汽和过量的反应物注入反应器中,从底部出口除去固体废物, 通过诸如旋风分离器的固体去除装置除去流出气体,在蒸馏塔中冷凝并分离出一些未反应的废物与废气,并将含有氢气和氯化氢的废气送到压缩机。 在优选的实施方案中,反应物含有至少一种选自卤代硅烷,有机卤​​代硅烷,卤化铝,卤化钛,卤化硼,卤化锰,卤化铜,卤化铁,卤化铬,卤化镍,卤化铟,镓 卤化物和卤化磷,卤化物含量选自氯,溴和碘。

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