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公开(公告)号：US5260470A
公开(公告)日：1993-11-09
申请号：US939470
申请日：1992-09-02
申请人： Thomas Goebel , Peter Panster , Werner Will , Peter Kleinschmit
发明人： Thomas Goebel , Peter Panster , Werner Will , Peter Kleinschmit
CPC分类号： C07F7/20
摘要： A method of purifying alkoxysilanes contaminated by organosilicon compounds with hydrolyzable chlorine atoms is disclosed wherein the alkoxysilanes are reacted in a pressure reactor with an alcohol, preferably in the presence of an HCl acceptor, at a temperature of 5.degree. C. to 160.degree. C. above the boiling point of the alcohol used and at the pressure which develops in the reactor.
摘要翻译： 公开了一种纯化有机硅化合物被可水解氯原子污染的烷氧基硅烷的方法，其中烷氧基硅烷在压力反应器中与醇反应，优选在HCl受体存在下，在5℃至160℃的温度下反应。 高于所用醇的沸点和反应器中产生的压力。
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82.发明授权Inclusion pigments of zirconium silicate formed with spinel inclusions, a process for the preparation and use thereof 失效由尖晶石夹杂物形成的硅酸锆的包含颜料，其制备方法和用途
公开(公告)号：US5252125A
公开(公告)日：1993-10-12
申请号：US847493
申请日：1992-03-12
申请人： Dietrich Speer , Akos Kiss , Peter Kleinschmit , Christel Zell
发明人： Dietrich Speer , Akos Kiss , Peter Kleinschmit , Christel Zell
CPC分类号： C09C1/0081 , C01P2002/08 , C01P2002/32
摘要： Inclusion pigments are disclosed based on zirconium silicate as a casing component and cobalt-free spinels as discrete, included colored compounds. The inclusion pigments are prepared by fusing a mixture of a zirconium dioxide source, a silicon dioxide source, one or more mineralizer and cobalt-free oxides in a ratio suitable for spinel-formation. The inclusion pigments have high enamel-fastness and high color-fastness. Further, the pigments are drain-resistant under usual decoration firing conditions.
摘要翻译： 公开了基于硅酸锆作为套管组分和不含钴的尖晶石作为离散的，包括着色的化合物的包合颜料。 通过将二氧化锆源，二氧化硅源，一种或多种矿化剂和不含钴的氧化物的混合物以适于尖晶石形成的比例熔融来制备包合物颜料。 夹杂颜料具有高搪瓷坚牢度和高色牢度。 此外，颜料在通常的装饰烧制条件下是防漏的。
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公开(公告)号：US5205866A
公开(公告)日：1993-04-27
申请号：US857074
申请日：1992-03-12
申请人： Akos Kiss , Dietrich Speer , Peter Kleinschmit , Jenny Horst
发明人： Akos Kiss , Dietrich Speer , Peter Kleinschmit , Jenny Horst
IPC分类号： C09C1/00
CPC分类号： C09C1/0012 , C01P2004/51 , C01P2004/61 , C01P2006/60
摘要： Gray-black inclusion pigments are made using zirconium silicate as the encasing substance and carbon black particles as the inclusion phase by annealing a mixture of zirconium dioxide, a source for silicon dioxide, carbon black and mineralizers under reducing conditions at 900.degree.-1400.degree. C. The process uses zeolites with an SiO.sub.2 /Al.sub.2 O.sub.3 molar ratio of more than 4, preferably more than 10, as the SiO.sub.2 source. The depth of the color can be increased by also using an adhesion agent, especially silicon oil. The use of the zeolites facilities the employment of different zirconium dioxide qualities and permits the production of pigments with higher carbon black inclusion rates.
摘要翻译： 灰黑色夹杂物颜料是通过在900-114℃的还原条件下退火二氧化锆，二氧化硅源，炭黑和矿化剂的混合物，使用硅酸锆作为包裹物质和炭黑颗粒作为夹杂相来制备的。 该方法使用SiO 2 / Al 2 O 3摩尔比大于4，优选大于10的SiO 2源的沸石。 也可以通过使用粘合剂，特别是硅油来增加颜色的深度。 使用沸石设备使用不同的二氧化锆质量，并允许生产具有较高碳黑夹杂率的颜料。
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84.发明授权Method for the reduction of nitrogen oxides from waste gases using a zeolite 失效使用ZEOLITE从废气中还原氮氧化物的方法
公开(公告)号：US5116586A
公开(公告)日：1992-05-26
申请号：US448198
申请日：1989-12-14
申请人： Michael Baacke , Reinhold Beand , Bernd Engler , Akos Kiss , Peter Kleine-Mollhoff , Peter Kleinschmit , Edgar Koberstein , Mustafa Siray
发明人： Michael Baacke , Reinhold Beand , Bernd Engler , Akos Kiss , Peter Kleine-Mollhoff , Peter Kleinschmit , Edgar Koberstein , Mustafa Siray
CPC分类号： B01J29/26 , B01D53/9418 , B01J29/24 , B01D2251/2062 , B01D2255/2065 , B01D2255/20738 , B01D2255/20761 , B01D2255/20769 , B01D2255/50
摘要： A zeolite catalyst and a method for reduction of nitrogen oxides present in waste gas streams is described. The method includes mixing the waste gas containing nitrogen oxides with ammonia. At an elevated temperature, this mixture is passed over a zeolite catalyst. Preferably, the zeolite catalyst is in a monolithic or honeycomb form. The zeolite catalyst includes one or more of the following subgroup metals: copper, iron, molybdeum and cerium. The zeolite catalysts made in accordance with this invention show better conversion of nitrogen oxides and longer life than known catalysts.
摘要翻译： 描述了沸石催化剂和还原废气流中存在的氮氧化物的方法。 该方法包括将含有氮氧化物的废气与氨混合。 在升高的温度下，将该混合物通过沸石催化剂。 优选地，沸石催化剂为整体或蜂窝形式。 沸石催化剂包括一种或多种以下亚族金属：铜，铁，钼和铈。 根据本发明制备的沸石催化剂表现出比已知催化剂更好的氮氧化物转化和更长的寿命。
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公开(公告)号：US5043016A
公开(公告)日：1991-08-27
申请号：US634487
申请日：1990-12-27
申请人： Dietrich Speer , Akos Kiss , Peter Kleinschmit
发明人： Dietrich Speer , Akos Kiss , Peter Kleinschmit
CPC分类号： C09C1/0012 , C01P2002/08 , C01P2002/52
摘要： The invention relates to new brown to gray inclusion pigments, based on zirconium silicate as casing substance, which are characterized in that they contain mixed crystals of the type (Fe.sub.1-x Mn.sub.x).sub.2 O.sub.3, in which x stands for a number in the range from 0.05 to 0.60, as colored compounds. The production takes place by means of annealing a mixture of SiO.sub.2 and ZrO.sub.2, or of precursors, in the presence of iron compounds and manganese compounds, in an Fe/Mn atomic ratio of 90:10 to 20:80, and mineralizers at 750.degree. to 1200.degree. C. The brown pigments are formed especially at temperatures of 850.degree. to 1000.degree. C. and if x is between 0.05 and 0.20. The gray pigments are formed especially at 1050.degree. to 1200.degree. C. and if x is 0.30 to 0.60.
摘要翻译： 本发明涉及基于硅酸锆作为外壳物质的新型棕色至灰色夹杂物，其特征在于它们含有（Fe1-xMnx）2O3型混合晶体，其中x代表0.05 至0.60，作为有色化合物。 通过在铁化合物和锰化合物的存在下以30:10至20:80的Fe / Mn原子比和750℃的矿化剂退火SiO 2和ZrO 2或前体的混合物进行生产。 至1200℃。褐色颜料特别是在850℃至1000℃的温度下形成，如果x在0.05至0.20之间。 特别是在1050℃〜1200℃，如果x为0.30〜0.60，则形成灰色颜料。
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86.发明授权Method for the preparation of gray-green pigments based on zirconium silicate/vanadium compounds and sodium compound 失效基于硅酸锆/钒化合物和钠化合物的灰绿色颜料的制备方法
公开(公告)号：US5021092A
公开(公告)日：1991-06-04
申请号：US389761
申请日：1989-08-04
申请人： Dietrich Speer , Akos Kiss , Peter Kleinschmit
发明人： Dietrich Speer , Akos Kiss , Peter Kleinschmit
CPC分类号： C09C1/0012 , C01P2002/70
摘要： The preparation of gray-green unitary pigment bodies based on zirconium silicate-vanadium oxide wherein a mixture of zirconium oxide and silicon oxide in the presence of a vanadium and lithium compound is calcined above 600.degree. C. and wherein the amount of V.sub.2 O.sub.5 is more than 17 percent by weight and the amount of lithium compound added is such that the atom ratio Li/Li+V is from 0.1 to 0.5.
摘要翻译： 制备基于硅酸锆 - 氧化钒的灰绿色整体色素体，其中在钒和锂化合物的存在下，氧化锆和氧化硅的混合物在600℃以上煅烧，其中V 2 O 5的量大于 17重量％，添加的锂化合物的量使得Li / Li + V的原子比为0.1〜0.5。
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公开(公告)号：US5008223A
公开(公告)日：1991-04-16
申请号：US487295
申请日：1990-03-02
申请人： Dietrich Speer , Akos Kiss , Peter Kleinschmit , Juergen Hanich
发明人： Dietrich Speer , Akos Kiss , Peter Kleinschmit , Juergen Hanich
CPC分类号： C09C1/0012 , C01P2002/08 , C01P2004/84 , C01P2006/12
摘要： The grayish-black encapsulated pigments contain carbon black particles with specific surface areas of 10 to 1000 m.sup.2 /g (BET) encapsulated in colorless crystals of zirconium silicate. In order to produce the pigments, mixtures of zirconium oxide with a particle size distribution (D50 values) between 7 and 10 .mu.m and a spec. surface between 2 and 4 m.sup.2 /g, silicon oxide, carbon black and mineralizers are heated under reducing conditions to 900.degree. to 1400.degree. C. and calcined for 0.5 to 8 hours and recalcined under oxidizing conditions to remove the non-included carbon black. The encapsulated pigments of the invention are suitable for the pigmented coloration of glazes.
摘要翻译： 灰黑色胶囊状颜料含有炭黑颗粒，其表面积为10至1000m2 / g（BET），其包封在无色硅酸锆晶体中。 为了制备颜料，氧化锆的混合物的粒度分布（D50值）在7和10μm之间， 表面积为2〜4m2 / g，氧化硅，炭黑和矿化剂在还原条件下加热至900〜1400℃，煅烧0.5〜8小时，在氧化条件下重新煅烧，除去未包含的炭黑。 本发明的胶囊化颜料适用于釉料着色着色。
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公开(公告)号：US4976943A
公开(公告)日：1990-12-11
申请号：US351054
申请日：1989-05-12
申请人： Ingo Pauli , Peter Kleinschmit , Rudolf Schwarz
发明人： Ingo Pauli , Peter Kleinschmit , Rudolf Schwarz
CPC分类号： C01B33/183 , C01B33/12 , C01P2002/02 , C01P2004/32 , C01P2004/51 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/90
摘要： A spherical, hydrophilic silica consisting of compact, massive, non-crystalline particles without inner pores with a particle size of 0.5 to 10 .mu.m, preferably 0.5 to 4 .mu.m and especially 1 to 3 .mu.m with a BET surface of
摘要翻译： 一种球形的亲水性二氧化硅，其由紧凑的，块状的，非结晶的颗粒组成，没有内孔，粒径为0.5至10μm，优选0.5至4μm，特别是1至3μm，BET表面积<50m2 通过将水蒸气和气态四氯化硅分别加热至300-400℃的温度，以2:1至6.7:1的摩尔比彼此混合来制备/ g，优选1至10m 2 / g。 并在600-1200℃的温度下使混合物反应。
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89.发明授权Organopolysiloxanes containing acyl thiourea groups, methods of their preparation and use 失效含有酰基硫脲的有机聚硅氧烷，其制备方法和用途
公开(公告)号：US4851492A
公开(公告)日：1989-07-25
申请号：US160046
申请日：1988-02-24
IPC分类号： B01D15/00 , B01D15/08 , B01J20/22 , B01J20/26 , C02F1/28 , C02F1/62 , C08G77/02 , C08G77/26 , C08G77/28 , C08G77/38 , C08G77/392 , C08G77/54 , C08G77/58
CPC分类号： C08G77/392 , B01J20/22 , C02F1/285 , C22B3/24 , Y02P10/234
摘要： Organopolysiloxane products containing acyl thiourea groups and from the units: ##STR1## are disclosed. R.sup.1 stands for an optionally substituted phenyl group or an alky group and R.sup.2 and R.sup.3 forR.sup.4 --SiO.sub.3/2 (2)units. R.sup.4 is alkylene. The free valences of the oxygen atoms are saturated by Si atoms of further R.sup.4 --SiO.sub.3/2 groups and/or by Si atoms of: ##STR2## amine units, wherein R.sup.5 =H; R.sup.2 or R.sup.3 and/or by cross-linking compounds of Si, Ti or Al. The ratio between the Si atoms in (1) and (3) to the Si, Ti, Al cross-linking atoms is 1:0 to 1:10. Various methods of preparing the products are described. These polymers to separate metals from solutions.
摘要翻译： 公开了含有酰基硫脲基团和单元的有机聚硅氧烷产品：（IMAGE）（1）。 R1代表任选取代的苯基或烷基，R2和R3代表R4-SiO3 / 2（2）单元。 R4是亚烷基。 氧原子的自由价饱和由另外的R 4 -SiO 3/2基团的Si原子和/或由Si原子组成：其中R5 = H; R2或R3和/或交联Si，Ti或Al的化合物。 （1）和（3）中的Si原子与Si，Ti，Al交联原子之间的比例为1:0至1:10。 描述了制备产品的各种方法。 这些聚合物用于将金属与溶液分离开来。
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公开(公告)号：US4697009A
公开(公告)日：1987-09-29
申请号：US875867
申请日：1986-06-18
CPC分类号： C07F7/182
摘要： The invention is directed to N-silylpropyl-N'-acyl ureas and their production from an alkali cyanate, a 3-halopropylsilane and in a given case, a cyclic acidamide. By heating the compounds of the invention the blocked isocyanate function can be set free.
摘要翻译： 本发明涉及N-甲硅烷基丙基-N'-酰基脲，它们由碱式氰酸酯，3-卤代丙基硅烷的产生，在给定情况下是环状酰胺。 通过加热本发明的化合物，可以使封闭的异氰酸酯官能团自由。
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