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1.发明授权公开(公告)号：US06733715B2
公开(公告)日：2004-05-11
申请号：US09955074
申请日：2001-09-19
IPC分类号： B29C3338
CPC分类号： C04B35/62227
摘要： A method of manufacturing hollow ceramics fibers with the pores of the micron-scale hollow structure unidirectionally oriented, the method of manufacturing is characterized in the steps of dispersing organic fibers in a dielectric liquid and applying high voltage to the dielectric liquid containing the dispersed organic fibers to electrostatically align them to produce a fiber accumulation in which the organic fibers are unidirectionally oriented, using the fiber accumulation as a mold and dipping the fiber accumulation in a ceramics base solution, and then removing the mold by treatment with heat or organic solvents.
摘要翻译： 制造具有微米级中空结构的孔的中空陶瓷纤维单向取向的方法，其制造方法的特征在于将有机纤维分散在电介质液体中并向含有分散的有机纤维的介电液体施加高电压 使纤维聚集成为模具并将纤维堆积物浸渍在陶瓷基底溶液中，然后通过用热或有机溶剂处理除去模具，使它们静电排列以产生纤维堆积物，其中有机纤维是单向取向的。
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公开(公告)号：US5783260A
公开(公告)日：1998-07-21
申请号：US686366
申请日：1996-07-25
CPC分类号： C08J7/04 , C08J3/243 , C08J7/047 , C08J2333/12 , C08J2369/00
摘要： A thin-film forming method comprising an uncured-layer forming step in which a mixed composition containing an organic polymerizing agent curable composition and a silicone polymerizing curable composition is prepared to form an uncured layer consisting of this mixed composition on a resin substrate; a solvent removing step in which the solvent in the uncured layer is removed; a first polymerization curing step in which the organic polymerizing curable composition in the uncured layer is polymerized; and a second polymerization curing step in which the silicone polymerizing curable composition in the uncured layer is polymerized. The thin-film forming method can comprise formation of the uncured layer on a resin substrate through the intermediation of a primer layer or formation of an uncured underlayer and uncured top layer followed by separate underlayer polymerization and top layer polymerization curing steps. The methods are applicable to the production of abrasion-resistant and water-repellant resin glass for automobiles.
摘要翻译： 一种包含未固化层形成步骤的薄膜形成方法，其中制备含有有机聚合剂固化性组合物和硅氧烷聚合性固化性组合物的混合组合物，以在树脂基材上形成由该混合组合物构成的未固化层; 除去未固化层中的溶剂的溶剂除去步骤; 将未固化层中的有机聚合性固化性组合物聚合的第一聚合固化步骤; 和第二聚合固化步骤，其中未固化层中的硅氧烷聚合可固化组合物聚合。 薄膜形成方法可以包括通过底漆层或未固化的底层和未固化的顶层的形成，然后分开的下层聚合和顶层聚合固化步骤在树脂基材上形成未固化的层。 该方法适用于生产用于汽车的耐磨和防水树脂玻璃。
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公开(公告)号：US5571569A
公开(公告)日：1996-11-05
申请号：US420209
申请日：1995-04-11
CPC分类号： C08J7/04 , C08J3/243 , C08J7/047 , C08J2333/12 , C08J2369/00
摘要： A thin-film forming method comprising an uncured-layer forming step in which a mixed composition containing an organic polymerizing agent curable composition and a silicone polymerizing curable composition is prepared to form an uncured layer consisting of this mixed composition on a resin substrate; a solvent removing step in which the solvent in the uncured layer is removed; a first polymerization curing step in which the organic polymerizing curable composition in the uncured layer is polymerized; and a second polymerization curing step in which the silicone polymerizing curable composition in the uncured layer is polymerized. The thin-film forming method can comprise formation of the uncured layer on a resin substrate through the intermediation of a primer layer or formation of an uncured underlayer and uncured top layer followed by separate underlayer polymerization and top layer polymerization curing steps. The methods are applicable to the production of abrasion-resistant and water-repellent resin glass for automobiles.
摘要翻译： 一种包含未固化层形成步骤的薄膜形成方法，其中制备含有有机聚合剂固化性组合物和硅氧烷聚合性固化性组合物的混合组合物，以在树脂基材上形成由该混合组合物构成的未固化层; 除去未固化层中的溶剂的溶剂除去步骤; 将未固化层中的有机聚合性固化性组合物聚合的第一聚合固化步骤; 和第二聚合固化步骤，其中未固化层中的硅氧烷聚合可固化组合物聚合。 薄膜形成方法可以包括通过底漆层或未固化的底层和未固化的顶层的形成，然后分开的下层聚合和顶层聚合固化步骤在树脂基材上形成未固化的层。 该方法适用于生产用于汽车的耐磨和防水树脂玻璃。
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公开(公告)号：US10138380B2
公开(公告)日：2018-11-27
申请号：US15119437
申请日：2015-02-19
申请人： NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY , Atsushi Hozumi , Chihiro Urata
发明人： Atsushi Hozumi , Chihiro Urata
IPC分类号： C09D5/16 , C09D183/04 , B32B27/28 , C08G77/00
摘要： In an aspect of the present invention, there is provided a water/oil repellent coating film, the water/oil repellent coating film being formed on a surface of a solid object, wherein the water/oil repellent coating film is terminated with a group expressed by chemical formula (A) and a three-dimensional crosslinking structure of siloxane bond is formed.
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公开(公告)号：US06841143B2
公开(公告)日：2005-01-11
申请号：US09946327
申请日：2001-09-06
申请人： Masahiko Inagaki , Atsushi Hozumi , Kei Teraoka , Kaori Nishizawa , Fukue Nagata , Yoshiyuki Yokogawa , Tetsuya Kameyama
发明人： Masahiko Inagaki , Atsushi Hozumi , Kei Teraoka , Kaori Nishizawa , Fukue Nagata , Yoshiyuki Yokogawa , Tetsuya Kameyama
CPC分类号： C04B38/009 , B01J23/10 , B01J35/1061 , C01B13/36 , C01B37/00 , C01P2006/16
摘要： This invention provides mesostructured oxide ceramics and a synthesizing method thereof, the synthesizing method employs a water-based solvent containing a metallic salt or metal complex as the ceramics precursor, template formed from an organic compound or the association thereof, and a precipitant, wherein mesostructured oxide ceramics are obtained from self-assembled oxide ceramics and organic substance by directly extracting oxide ceramics at a low temperature of 200° C. or less by utilizing a homogenous precipitation reaction from said ceramics precursor under the coexistence of a nanometer-sized template in the solvent, and separating and collecting the obtained precipitation, and mesostructured oxide ceramics is prepared by employing the synthesizing method described above.
摘要翻译： 本发明提供介观结构氧化物陶瓷及其合成方法，该合成方法采用含有金属盐或金属络合物作为陶瓷前体的水溶剂，由有机化合物形成的模板或其缔合物，以及沉淀剂，其中介孔结构 氧化物陶瓷由自组装的氧化物陶瓷和有机物质通过在200℃或更低的低温下直接提取氧化物陶瓷而获得，通过在纳米尺寸模板共存的情况下利用来自所述陶瓷前体的均匀沉淀反应 溶剂，并分离和收集所得沉淀，并通过使用上述合成方法制备介孔结构氧化物陶瓷。
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6.发明授权Process for producing ceramic porous bodies having hollow structures at low temperatures 失效在低温下制造具有中空结构的陶瓷多孔体的方法公开(公告)号：US06645571B1
公开(公告)日：2003-11-11
申请号：US09657398
申请日：2000-09-08
申请人： Osamu Takai , Hiroyuki Sugimura , Atsushi Hozumi
发明人： Osamu Takai , Hiroyuki Sugimura , Atsushi Hozumi
IPC分类号： B05D306
CPC分类号： C04B41/009 , C04B38/0022 , C04B38/062 , C04B41/4582 , C04B35/01 , C04B35/62218 , C04B38/0054 , C04B40/0017 , C04B40/0089 , C04B38/009 , C04B41/0045 , C04B41/4515 , C04B41/4554 , C04B41/5027
摘要： A process for producing the ceramic porous body comprising the steps of (1) forming micelles in liquid by mixing {circle around (1)} surfactant molecules, {circle around (2)} surfactant molecules and given organic molecules, or {circle around (3)} different kinds of surfactant molecules, (2) forming a precursor of a ceramic porous body having an organic-inorganic structure is formed through mixing a ceramic material or a precursor of the ceramic material into the liquid containing the micelles, the precursor of the ceramic porous body comprising a template having the micelles arranged in a hexagonal, cubic or lamella form and the ceramic material or the ceramic material precursor adsorbed around the micelles, (3) removing the surfactant molecules or the surfactant molecules and the given organic molecules in the precursor of the ceramic porous body by photo-oxidation through irradiating vacuum ultraviolet light upon the precursor to leave an inorganic skeleton alone, and (4) thereby forming the ceramic porous body having nanometer-scale pores at a low temperature.
摘要翻译： 一种制造陶瓷多孔体的方法，包括以下步骤：（1）通过混合（圆周（1个表面活性剂分子，2个表面活性剂分子和给定的有机分子，或3个不同的 表面活性剂分子，（2）通过将陶瓷材料或陶瓷材料的前体混合到含有胶束的液体中形成具有有机 - 无机结构的陶瓷多孔体的前体，陶瓷多孔体的前体包含 具有以六边形，立方体或薄片形式布置的胶束和陶瓷材料或陶瓷材料前体吸附在胶束周围的模板，（3）去除表面活性剂分子或表面活性剂分子和陶瓷多孔的前体中的给定有机分子 通过对前体照射真空紫外光进行光氧化，单独留下无机骨架，（4）由此形成 该陶瓷多孔体在低温下具有纳米尺度的孔。
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公开(公告)号：US06465388B1
公开(公告)日：2002-10-15
申请号：US09626658
申请日：2000-07-27
申请人： Atsushi Hozumi , Hitotoshi Murase
发明人： Atsushi Hozumi , Hitotoshi Murase
IPC分类号： B01J3100
摘要： A photocatalytic film is formed by: a step for forming an uncured underlayer from an organic composition on the surface of a resinous base and polymerizing the organic composition to convert the uncured underlayer into an underlayer having a hardness higher than that of the resinous base; a step for forming an uncured intermediate layer from a polymerizable and curable silicone composition on the uncured underlayer or on the underlayer to yield an uncured intermediate layer, and polymerizing the polymerizable and curable silicone composition to convert the uncured intermediate layer to an intermediate layer, the polymerizable and curable silicone composition being prepared mainly from a hydrolyzable tetrafunctional silane derivative; and a step for forming a photocatalytic layer on the intermediate layer. This process can form an intermediate layer having a very high hardness without cracking and can easily yield a photocatalytic film having a satisfactory abrasion resistance.
摘要翻译： 通过以下步骤形成光催化膜：通过在树脂基材的表面上形成有机组合物的未固化底层的步骤，并使有机组合物聚合，将未固化的底层转化为硬度高于树脂基材的硬度的底层; 从未固化的底层或底层上的可聚合和可固化的硅氧烷组合物形成未固化的中间层以产生未固化的中间层，并聚合可聚合和可固化的硅氧烷组合物以将未固化的中间层转化为中间层的步骤， 可聚合和可固化的有机硅组合物主要由可水解的四官能硅烷衍生物制备; 以及在中间层上形成光催化层的步骤。 该方法可以形成具有非常高的硬度而不破裂的中间层，并且可以容易地产生具有令人满意的耐磨性的光催化膜。
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公开(公告)号：US10023701B2
公开(公告)日：2018-07-17
申请号：US15319924
申请日：2015-06-19
申请人： Chihiro Urata , Atsushi Hozumi
发明人： Chihiro Urata , Atsushi Hozumi
摘要： In an embodiment of the present invention, a wet gel includes a crosslinked silicone resin in which a silicone resin composition is solidified; a first liquid capable of dissolving the silicone resin composition; and one of a solid capable of being dissolved in the first liquid, and a second liquid such that a degree of swelling, when the crosslinked silicone resin is immersed in the second liquid, is less than a degree of swelling when the crosslinked silicone resin is immersed in n-dodecane, wherein the second liquid is capable of being mixed with the first liquid.
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公开(公告)号：US20170130007A1
公开(公告)日：2017-05-11
申请号：US15319924
申请日：2015-06-19
申请人： Chihiro URATA , Atsushi HOZUMI
发明人： Chihiro URATA , Atsushi HOZUMI
CPC分类号： C08J3/092 , C08G77/12 , C08G77/20 , C08J3/098 , C08J2383/04 , C08K3/00 , C08K5/01 , C08K5/541 , C08L83/04 , C08K3/36 , C08K5/5415 , C08K5/56 , C08L83/00
摘要： In an embodiment of the present invention, a wet gel includes a crosslinked silicone resin in which a silicone resin composition is solidified; a first liquid capable of dissolving the silicone resin composition; and one of a solid capable of being dissolved in the first liquid, and a second liquid such that a degree of swelling, when the crosslinked silicone resin is immersed in the second liquid, is less than a degree of swelling when the crosslinked silicone resin is immersed in n-dodecane, wherein the second liquid is capable of being mixed with the first liquid.
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10.发明授权Artificial tooth root with anti-adherence of sordes and various germs, with acid resistance and its preparation method 失效人造牙根具有抗粘附性和各种细菌，具有耐酸性及其制备方法公开(公告)号：US06402517B1
公开(公告)日：2002-06-11
申请号：US09513200
申请日：2000-02-25
申请人： Atsushi Hozumi , Masahiko Inagaki , Kaori Nishizawa , Fukue Nagata , Yoshiyuki Yokogawa , Tetsuya Kameyama
发明人： Atsushi Hozumi , Masahiko Inagaki , Kaori Nishizawa , Fukue Nagata , Yoshiyuki Yokogawa , Tetsuya Kameyama
IPC分类号： A61C800
CPC分类号： A61C8/0012 , A61C8/0013 , A61K6/0008 , A61K6/0017 , A61K6/0044 , A61K6/0205 , A61K6/033 , A61K6/04 , A61K6/0643 , A61K6/08
摘要： The invention provides an artificial tooth root having acid resistance and anti-adherence of sordes and various germs, consisting of a substrate and a coating of calcium phosphate based ceramic having bioaffinity formed on the surface of this substrate, the substrate is composed of a polymer, ceramic, metal, or other material, the surface of the ceramic coating on the substrate surface is endowed with a protrusion-and-recession configuration, and is, chemically modified, and to a method for producing the artificial tooth root, by forming a coating of calcium phosphate based ceramic having bioaffinity over a substrate while imparting protrusions and recessions thereto, masking an area of the ceramic coating surface of which bioaffinity is required, and fixing a silane coupling agent exclusively over a predetermined area of the ceramic coating surface.
摘要翻译： 本发明提供了一种具有耐酸性和抗粘附性的人造牙根和各种细菌，由基材和在该基材的表面上形成的具有生物亲和性的磷酸钙基陶瓷涂层组成，基材由聚合物， 陶瓷，金属或其他材料，基板表面上的陶瓷涂层的表面具有突起 - 退回构型，并被化学改性，并且通过形成涂层来形成人造牙根的制造方法 的具有生物亲和力的磷酸钙基陶瓷，同时赋予其突起和凹陷，掩蔽需要生物亲和性的陶瓷涂层表面的区域，并将硅烷偶联剂固定在陶瓷涂层表面的预定区域上。
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