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    Method for revamping an HF or sulphuric acid alkylation unit
    2.
    发明授权
    Method for revamping an HF or sulphuric acid alkylation unit 有权
    改造HF或硫酸烷基化单元的方法

    公开(公告)号：US08692048B2

    公开(公告)日：2014-04-08

    申请号：US13388507

    申请日：2010-08-05

    Applicant: Zhichang Liu ,  Chunming Xu ,  Rui Zhang ,  Xianghai Meng ,  Ana Cecilia Patroni ,  Peter Anton August Klusener ,  Albertus Vincentius Petrus Van Den Bosch

    Inventor： Zhichang Liu ,  Chunming Xu ,  Rui Zhang ,  Xianghai Meng ,  Ana Cecilia Patroni ,  Peter Anton August Klusener ,  Albertus Vincentius Petrus Van Den Bosch

    IPC: C07C7/144

    CPC classification number: C07C2/58 ,  C07C2531/14 ,  C07C9/16

    Abstract: The present invention provides a method for revamping an HF or sulphuric acid alkylation unit to an ionic liquid alkylation unit, wherein the HF or sulphuric acid alkylation unit comprise at least: —a reactor unit for contacting catalyst and hydrocarbon reactants; —a separator unit for separating a reactor effluent into a catalyst phase and an alkylate-comprising hydrocarbon phase; —a fractionator unit for fractionating the alkylate-comprising hydrocarbon phase into at least one stream comprising alkylate; and which method includes: —providing a second separator unit suitable for the separation of solids from liquids downstream of the reactor unit suitable to reduce the solids content in at least part of the reactor effluent.

    Abstract translation: 本发明提供了将HF或硫酸烷基化单元改性为离子液体烷基化单元的方法，其中HF或硫酸烷基化单元至少包括： - 用于使催化剂和烃反应物接触的反应器单元; - 用于将反应器流出物分离成催化剂相和含烷基化物烃相的分离器单元; - 用于将含烷基化物烃相分级成至少一种包含烷基化物的流的分馏器单元; 并且哪种方法包括： - 提供适合于从反应器单元下游的液体中分离固体的第二分离器单元，其适于减少至少部分反应器流出物中的固体含量。

    METHODS FOR REGENERATING AND MAINTAINING ACTIVITY OF IONIC LIQUID CATALYST AND PRODUCING ALKYLATE
    3.
    发明申请
    METHODS FOR REGENERATING AND MAINTAINING ACTIVITY OF IONIC LIQUID CATALYST AND PRODUCING ALKYLATE 审中-公开
    再生和维持离子液体催化剂活性和生产烷基酸的方法

    公开(公告)号：US20120283500A1

    公开(公告)日：2012-11-08

    申请号：US13383946

    申请日：2010-07-15

    Applicant: Zhichang Liu ,  Chunming Xu ,  Rui Zhang ,  Xianghai Meng

    Inventor： Zhichang Liu ,  Chunming Xu ,  Rui Zhang ,  Xianghai Meng

    IPC: C07C2/62

    CPC classification number: B01J31/0278 ,  B01J31/0284 ,  B01J31/26 ,  B01J31/30 ,  B01J31/38 ,  B01J31/40 ,  B01J38/54 ,  B01J38/60 ,  C07C2/60 ,  C07C2527/055 ,  C07C2527/122 ,  C07C2527/125 ,  C07C2527/126 ,  C10G29/205 ,  C10G2300/1081 ,  C10G2300/1092 ,  C10G2300/70 ,  Y02P20/584

    Abstract: Disclosed is a method for regenerating and maintaining the activity of an ionic liquid catalyst, which comprises supplying hydrogen halide or halogenated hydrocarbon to the acidic ionic liquid catalyst or alkylation materials during alkylation reaction, wherein said ionic liquid catalyst is used to catalyze alkylation of C4 alkene and alkane. Disclosed is also a method for producing alkylate by alkylation reaction, which comprises supplying hydrogen halide or halogenated hydrocarbon to the acidic ionic liquid catalyst or reaction materials during said alkylation reaction. The method can prolong the service life of the acidic ionic liquid catalyst, does not influence the quality of the alkylate, and has simple operation. The processed amount of materials may be 1000 times more than the used amount of the ionic liquid.

    Abstract translation: 公开了一种用于再生和保持离子液体催化剂的活性的方法，其包括在烷基化反应期间向酸性离子液体催化剂或烷基化材料供应卤化氢或卤代烃，其中所述离子液体催化剂用于催化C4烯烃的烷基化 和烷烃。 还公开了通过烷基化反应制备烷基化物的方法，其包括在所述烷基化反应期间向酸性离子液体催化剂或反应物质供应卤化氢或卤代烃。 该方法可延长酸性离子液体催化剂的使用寿命，不影响烷基化物质，操作简单。 处理量的材料可以是使用量的离子液体的1000倍。

    METHOD FOR REVAMPING AN HF OR SULPHURIC ACID ALKYLATION UNIT
    5.
    发明申请
    METHOD FOR REVAMPING AN HF OR SULPHURIC ACID ALKYLATION UNIT 有权
    用于逆转HF或硫酸碱化单元的方法

    公开(公告)号：US20120165592A1

    公开(公告)日：2012-06-28

    申请号：US13388507

    申请日：2010-08-05

    Applicant: Zhichang Liu ,  Chunming Xu ,  Rui Zhang ,  Xianghai Meng ,  Ana Cecilia Patroni ,  Peter Anton August Klusener ,  Albertus Vincentius Petrus Van Den Bosch

    Inventor： Zhichang Liu ,  Chunming Xu ,  Rui Zhang ,  Xianghai Meng ,  Ana Cecilia Patroni ,  Peter Anton August Klusener ,  Albertus Vincentius Petrus Van Den Bosch

    IPC: C07C2/58

    CPC classification number: C07C2/58 ,  C07C2531/14 ,  C07C9/16

    Abstract: The present invention provides a method for revamping an HF or sulphuric acid alkylation unit to an ionic liquid alkylation unit, wherein the HF or sulphuric acid alkylation unit comprise at least: a reactor unit for contacting catalyst and hydrocarbon reactants; a separator unit for separating a reactor effluent into a catalyst phase and an alkylate-comprising hydrocarbon phase; a fractionator unit for fractionating the alkylate-comprising hydrocarbon phase into at least one stream comprising alkylate; and which method includes: providing a second separator unit suitable for the separation of solids from liquids downstream of the reactor unit suitable to reduce the solids content in at least part of the reactor effluent.

    Abstract translation: 本发明提供了将HF或硫酸烷基化单元改性为离子液体烷基化单元的方法，其中HF或硫酸烷基化单元至少包括：用于使催化剂和烃反应物接触的反应器单元; 用于将反应器流出物分离成催化剂相和含烷基化物烃相的分离器单元; 用于将包含烷基化物的烃相分级成至少一种包含烷基化物的流的分馏器单元; 并且该方法包括：提供适于将固体从反应器单元下游的液体分离出来的第二分离器单元，其适于减少至少部分反应器流出物中的固体含量。

    Deep separation method and processing system for the separation of heavy oil through granulation of coupled post-extraction asphalt residue
    6.
    发明授权
    Deep separation method and processing system for the separation of heavy oil through granulation of coupled post-extraction asphalt residue 有权
    通过联合萃取后沥青残渣的造粒分离重油的深度分离方法和加工系统

    公开(公告)号：US07597794B2

    公开(公告)日：2009-10-06

    申请号：US11265468

    申请日：2005-11-01

    Applicant: Suoqi Zhao ,  Chunming Xu ,  Ren′an Wang ,  Zhiming Xu ,  Xuewen Sun ,  Keng H. Chung

    Inventor： Suoqi Zhao ,  Chunming Xu ,  Ren′an Wang ,  Zhiming Xu ,  Xuewen Sun ,  Keng H. Chung

    IPC: C10C1/18 ,  C10C3/08 ,  B01J8/04 ,  B01J10/00

    CPC classification number: C10C3/16

    Abstract: The present invention is a separation method and system in which granulation of coupled post-extraction asphalt residue is used to achieve deep separation of heavy oil. A dispersion solvent is introduced into the asphalt phase after separation by solvent extraction and the asphalt phase undergoes rapid phase change in a gas-solid separator and is dispersed into solid particles while the solvent vaporizes, resulting in low temperature separation of asphalt and solvent with adjustable size of the asphalt particles. The separation method of this invention also includes a three-stage separation of heavy oil feedstock, in which the deasphalted oil phase separated from heavy oil is treated with supercritical solvent and results in the further separation of the resin portion of the deasphalted oil, maximizing the yield and quality of the deasphalted oil. The processes and systems in this invention use atmospheric pressure and a low temperature gas-solid separator instead of a high temperature and high pressure furnace and do not require the feed pre-heating or heat exchange equipment at the inlet of resin separator column, resulting in a simplified process flow and reduced investment.

    Abstract translation: 本发明是一种分离方法和系统，其中使用联合萃取后沥青残渣的造粒来实现重油的深度分离。 通过溶剂萃取分离后，将分散溶剂引入沥青相中，沥青相在气固分离器中发生快速相变，溶剂蒸发时分散成固体颗粒，导致沥青和溶剂的低温分离，可调节 沥青颗粒尺寸。 本发明的分离方法还包括重油原料的三段分离，其中用超临界溶剂处理与重油分离的脱沥青油相，并导致脱沥青油的树脂部分的进一步分离，使 脱沥青油的产量和质量。 本发明的方法和系统使用大气压和低温气固分离器代替高温高压炉，并且不需要在树脂分离塔入口处的进料预热或热交换设备，导致 简化流程，减少投资。

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