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    Method and materials for purifying hydride gases, inert gases, and non-reactive gases
    2.
    发明授权
    Method and materials for purifying hydride gases, inert gases, and non-reactive gases 失效

    公开(公告)号：US07033418B2

    公开(公告)日：2006-04-25

    申请号：US10260060

    申请日：2002-09-27

    申请人： Tadaharu Watanabe ,  Dan Fraenkel

    发明人： Tadaharu Watanabe ,  Dan Fraenkel

    IPC分类号： B01D53/02 ,  C01F7/02

    CPC分类号： B01J20/30 ,  B01D53/46 ,  B01D2253/10 ,  B01D2257/00 ,  B01J20/08 ,  Y02C10/08 ,  Y10S95/90

    摘要： A process for removing trace amounts of moisture and/or one or more impurities from contaminated hydride, inert and non-reactive gases, thus decreasing the concentration of the impurities to parts-per-billion (ppb) or parts-per-trillion (ppt) levels. The gas purifier materials of this invention include thermally activated aluminas, said aluminas including organic alumina materials, modified organic alumina materials, and modified inorganic aluminas. The thermally activated alumina materials of this invention are activated by heating the alumina material at a temperature between about 50° C.–1000° C. in an inert or non-inert atmosphere or in a vacuum and maintaining the activated material in the inert or non-inert atmosphere or in a vacuum atmosphere subsequent to said activation but prior to use.

    Gas purifier system for removing trace impurities from a reactive fluid
    4.
    发明授权
    Gas purifier system for removing trace impurities from a reactive fluid 失效
    用于从反应流体中除去痕量杂质的气体净化系统

    公开(公告)号：US06783576B2

    公开(公告)日：2004-08-31

    申请号：US10263433

    申请日：2002-10-02

    申请人： Hans H. Funke ,  Dan Fraenkel ,  Virginia H. Houlding

    发明人： Hans H. Funke ,  Dan Fraenkel ,  Virginia H. Houlding

    IPC分类号： B01D5302

    CPC分类号： C01B7/0743 ,  B01D53/02 ,  B01D2253/102 ,  B01J20/20 ,  C01B7/0725 ,  C01B7/093 ,  C01C1/024 ,  Y02C10/08 ,  Y02P20/52 ,  Y10S95/901 ,  Y10S210/906 ,  Y10S210/909 ,  Y10S210/915 ,  Y10S502/519

    摘要： Gas purifier system containing a preconditioned ultra-low emission (P-ULE) carbon for reducing trace impurities such as organic compounds and carbon monoxide in reactive fluids such as ammonia, hydrogen chloride, hydrogen bromide, and chlorine to sub-ppb levels. P-ULE is capable of removing impurities from a reactive fluid down to parts-per-billion (ppb) and sub-ppb levels without concurrently emitting other impurities such as moisture or carbon dioxide into the purified reactive fluid. The P-ULE carbon is prepared by heating a carbon material to temperatures between about 300° C. to 800° C. in an ultra-dry, inert gas stream, to produce an ultra-low emission (ULE) carbon material, subjecting the ULE carbon to a second activation process under a reactive gas atmosphere to produce a P-ULE carbon and storing the P-ULE carbon in an environment that minimizes contamination of the P-ULE prior to its use in a gas purifier system.

    摘要翻译： 含有预处理超低排放（P-ULE）碳的气体净化器系统，用于将反应性流体（如氨，氯化氢，溴化氢和氯）中的微量杂质如有机化合物和一氧化碳降至亚ppb水平。 P-ULE能够将反应性流体中的杂质去除至十亿分之一（ppb）和亚ppb水平，而不会将其他杂质如水分或二氧化碳排放到纯化的反应流体中。 通过在超干惰性气流中将碳材料加热到约300℃至800℃的温度来制备P-ULE碳，以产生超低排放（ULE）碳材料， ULE碳在反应气体气氛下进行第二活化过程以产生P-ULE碳并将P-ULE碳储存在使P-ULE在气体净化器系统中使用之前的污染最小化的环境中。

    Method and apparatus for removing trace impurities from a gas using superactivated carbon material
    8.
    发明授权
    Method and apparatus for removing trace impurities from a gas using superactivated carbon material 有权
    使用超活化碳材料从气体中除去痕量杂质的方法和设备

    公开(公告)号：US06425946B1

    公开(公告)日：2002-07-30

    申请号：US09748734

    申请日：2000-12-26

    申请人： Hans H. Funke ,  Dan Fraenkel ,  Virginia H. Houlding

    发明人： Hans H. Funke ,  Dan Fraenkel ,  Virginia H. Houlding

    IPC分类号： B01D5302

    CPC分类号： C01C1/024 ,  B01D53/02 ,  B01D2253/102 ,  B01J20/20 ,  C01B7/0725 ,  C01B7/0743 ,  C01B7/093 ,  Y02C10/08 ,  Y10S502/519

    摘要： Trace impurities such as organic compounds and carbon monoxide are reduced to sub-ppb levels in gases such as nitrogen, helium and argon, by gas purifying systems that contain an ultra-low emission (ULE) carbon material. Ultra-low emission (ULE) carbon materials can be made from commercially available carbon materials in the form of pellets, extrudates and beads and is capable of removing impurities from a gas stream down to parts-per-billion (ppb) and sub-ppb levels without concurrently emitting other impurities such as moisture or carbon dioxide to the purified gas stream. The carbon material is superactivated by heating the carbon to temperatures from 300° to about 800° degrees C. in an ultra-dry, inert gas stream. The ultra-low emission (ULE) carbon material is handled and stored in an environment that minimizes contamination from moisture and other oxygenated species in order to maintain its ppb and sub-ppb impurity removal and low emission properties. The ultra-low emission (ULE) carbon material can be used as “stand-alone” purifier material or in combination with other scavenging materials that are capable of removing large quantities of impurities such as oxygen and moisture that are not removed or only marginally removed by the ultra-low emission (ULE) carbon material.

    摘要翻译： 通过含有超低排放（ULE）碳材料的气体净化系统，微量杂质如有机化合物和一氧化碳在气体如氮气，氦气和氩气中降低至亚ppb水平。 超低排放（ULE）碳材料可以由颗粒，挤出物和珠粒形式的市售碳材料制成，并且能够将气流中的杂质去除至十亿分之一（ppb）和亚ppb 而不同时向纯化的气流中发出诸如水分或二氧化碳的其它杂质。 碳材料通过在超干惰性气流中将碳加热至300℃至约800℃的温度来超活化。 超低排放（ULE）碳材料被处理和储存在最小化水分和其他氧化物质污染的环境中，以保持其ppb和亚ppb杂质去除和低排放性能。 超低排放（ULE）碳材料可以用作“独立”净化器材料或与其他能够去除大量杂质如氧气和水分的除去或仅略微去除的清除材料组合使用 通过超低排放（ULE）碳材料。

    Methods for removal of water from gases using superheated zeolites
    9.
    发明授权
    Methods for removal of water from gases using superheated zeolites 失效
    使用过热沸石从气体中除去水的方法

    公开(公告)号：US06110258A

    公开(公告)日：2000-08-29

    申请号：US166987

    申请日：1998-10-06

    申请人： Dan Fraenkel ,  Hans H. Funke ,  Gerald Cooper

    发明人： Dan Fraenkel ,  Hans H. Funke ,  Gerald Cooper

    IPC分类号： B01D53/28 ,  B01D53/04 ,  B01D53/26 ,  B01J20/18 ,  C01B39/02

    CPC分类号： B01D53/02 ,  B01D53/04 ,  B01D53/261 ,  B01J20/186 ,  B01D2253/108 ,  B01D2253/1085 ,  B01D2253/30 ,  B01D2253/304 ,  B01D2257/80 ,  B01D2259/40088 ,  Y10S95/902

    摘要： A method for removing trace moisture from a gas is disclosed. The method involves heating a zeolite having a high silica-to-alumina ratio to about 400.degree. C. to remove physically absorbed water from the zeolite, followed by heating the zeolite to a temperature in excess of 650.degree. C., to form a superheated zeolite. Heating to temperatures of 650.degree. C. or above is believed to cause dehydroxylation of the zeolite. A method for the preparation of a dehydroxylated zeolite is also disclosed. The superheated zeolite is contacted with the gas, thereby adsorbing water from the gas. A dehydroxylated zeolite for removing trace moisture from a gas wherein the zeolite has a high silica-to-alumina ratio and a low level of metallic impurities is also disclosed. The zeolite and methods of the invention are particularly useful for removing trace water from acid gases such as hydrogen chloride and hydrogen bromide.

    摘要翻译： 公开了从气体中除去痕量水分的方法。 该方法包括将具有高二氧化硅 - 氧化铝比的沸石加热至约400℃，以从沸石中除去物理吸收的水，然后将沸石加热至超过650℃的温度，形成过热 沸石。 认为加热到650℃以上的温度会引起沸石的脱羟基化。 还公开了一种制备脱羟基化沸石的方法。 过热沸石与气体接触，从气体中吸附水分。 还公开了用于从气体中除去痕量水分的脱羟基化沸石，其中沸石具有高二氧化硅与氧化铝的比例和低水平的金属杂质。 本发明的沸石和方法特别可用于从酸性气体如氯化氢和溴化氢中除去痕量水。

    Multi-staged wax displacement process for catalyst recovery from a slurry
    10.
    发明申请
    Multi-staged wax displacement process for catalyst recovery from a slurry 审中-公开
    用于从浆料中回收催化剂的多级蜡置换方法

    公开(公告)号：US20060111232A1

    公开(公告)日：2006-05-25

    申请号：US10994428

    申请日：2004-11-22

    申请人： Michael Spena ,  Doug Jack ,  Dan Fraenkel

    发明人： Michael Spena ,  Doug Jack ,  Dan Fraenkel

    IPC分类号： B01J20/34 ,  C07C1/04

    CPC分类号： B01J8/006 ,  B01J8/22 ,  B01J23/75 ,  B01J23/94 ,  B01J37/009 ,  B01J2208/0084 ,  B01J2219/00006 ,  B01J2219/0077 ,  C10G2/33 ,  Y02P20/582

    摘要： In a system and method for cleaning and recovering a solid catalyst, a solvent is added to a slurry comprising the catalyst and residual hydrocarbons. A portion of the residual hydrocarbons and the solvent are separated from the slurry, and the solvent addition and separating steps are repeated until a desired amount of the hydrocarbons have been removed. The solvent is finally removed from the catalyst using a stripping gas to recover a cleaned catalyst. In preferred embodiments, the slurry comprises a Fischer-Tropsch solid catalyst; the slurry exits a slurry bubble reactor, or both. In an embodiment, the solvent comprises naphtha; the residual hydrocarbons comprise waxy hydrocarbons; and one of the separation steps comprises filtration. In an embodiment, the repeating of the solvent addition and separating steps is carried out in a plurality of filters operated in series.

    摘要翻译： 在用于清洁和回收固体催化剂的系统和方法中，将溶剂加入到包含催化剂和残余烃的浆料中。 将一部分残余烃和溶剂与浆料分离，并重复溶剂添加和分离步骤，直到除去所需量的烃。 使用汽提气体最终从催化剂中除去溶剂以回收清洁的催化剂。 在优选的实施方案中，浆料包括费 - 托固体催化剂; 浆料离开浆液泡沫反应器，或两者。 在一个实施方案中，溶剂包括石脑油; 残余烃包括蜡质烃; 并且其中一个分离步骤包括过滤。 在一个实施方案中，重复的溶剂添加和分离步骤是在串联操作的多个过滤器中进行的。