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1.发明授权公开(公告)号：US08556610B2
公开(公告)日：2013-10-15
申请号：US13205464
申请日：2011-08-08
IPC分类号： B29B9/10
CPC分类号： B29B9/12 , B01J8/12 , B01J19/0066 , B01J19/20 , B01J2208/00176 , B01J2208/00221 , B01J2219/00779 , B01J2219/185 , B01J2219/1946 , B29B9/065 , B29B9/16 , B29B13/065 , B29B2009/165 , B29B2009/168 , B29K2067/00 , C08G63/90
摘要： The invention relates to a method and device for the direct production of polyester granulate from a highly viscous polyester melt with a polymerization degree of 132 to 165, as well as the granulates formed thereform. In the method, the highly viscous polyester melt is subjected to a pre-drying and drying/degassing after a hot cutting method. Hot cutting is implemented at water temperatures of 70° C. to 95° C. and with a liquid to solid ratio of 8 to 12:1.
摘要翻译： 本发明涉及从聚合度为132〜165的高粘度聚酯熔体以及由其形成的颗粒直接生产聚酯颗粒的方法和装置。 在该方法中，高粘度聚酯熔体在热切割方法之后进行预干燥和干燥/脱气。 热切割在70℃至95℃的水温和8至12:1的液体与固体比之间实施。
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2.发明授权公开(公告)号：US07993557B2
公开(公告)日：2011-08-09
申请号：US12195962
申请日：2008-08-21
IPC分类号： B29B9/10
CPC分类号： B29B9/12 , B01J8/12 , B01J19/0066 , B01J19/20 , B01J2208/00176 , B01J2208/00221 , B01J2219/00779 , B01J2219/185 , B01J2219/1946 , B29B9/065 , B29B9/16 , B29B13/065 , B29B2009/165 , B29B2009/168 , B29K2067/00 , C08G63/90
摘要： The invention relates to a method and device for the direct production of polyester granulate from a highly viscous polyester melt with a polymerization degree of 132 to 165, as well as the granulates formed thereform. In the method, the highly viscous polyester melt is subjected to a pre-drying and drying/degassing after a hot cutting method. Hot cutting is implemented at water temperatures of 70° C. to 95° C. and with a liquid to solid ratio of 8 to 12:1.
摘要翻译： 本发明涉及从聚合度为132〜165的高粘度聚酯熔体以及由其形成的颗粒直接生产聚酯颗粒的方法和装置。 在该方法中，高粘度聚酯熔体在热切割方法之后进行预干燥和干燥/脱气。 热切割在70℃至95℃的水温和8至12:1的液体与固体比之间实施。
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公开(公告)号：US20070066790A1
公开(公告)日：2007-03-22
申请号：US11373937
申请日：2006-03-13
IPC分类号： C08G63/02
CPC分类号： C08G63/785 , B01J19/1887 , B01J2219/00085 , B01J2219/00087 , B01J2219/0011 , B01J2219/00166 , C08G63/78
摘要： The invention relates to a method for producing high-molecular weight polyesters, such as e.g. polyethylene terephthalate (PET), polybutylene terephthalate (PBT), polynaphthalene terephthalate (PEN), polytrimethylene terephthalate (PTT) and/or polyesters of other dicarboxylic acids and diols including copolymers thereof. The invention relates likewise to a device for implementing this method. The latter concerns a single-stage tower reactor with which a method, comprising only two reactors, is made available for the total process.
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4.发明授权公开(公告)号：US08252888B2
公开(公告)日：2012-08-28
申请号：US13355938
申请日：2012-01-23
CPC分类号： B01J19/247 , B01J19/18 , B01J19/1862 , B01J19/20 , B01J2219/00006 , B01J2219/00081 , B01J2219/00083 , B01J2219/00085 , B01J2219/00087 , B01J2219/00092 , B01J2219/00094 , B01J2219/00103 , B01J2219/0011 , B01J2219/00159 , B01J2219/00768 , B01J2219/0077 , B01J2219/00779 , B01J2219/182 , B01J2219/185 , B01J2219/1943 , C08G63/78 , C08G63/785 , C08G63/83 , C08G63/85
摘要： The present invention relates to a method for the continuous production of high-molecular polyesters by esterification of dicarboxylic acids and/or transesterification of dicarboxylic acid esters with diols and/or mixtures thereof in the presence of catalysts with formation of a prepolymer in a tower reactor and polycondensation thereof to form a high-molecular polyester in a polycondensation reactor, a prepolymer with >40 to 70 repeat units (DP) being produced in the tower reactor and this prepolymer being polycondensed in only one further reactor to form a polyester with >150 to 205 DP.
摘要翻译： 本发明涉及通过二羧酸酯化和/或二羧酸酯与二醇和/或其混合物的酯交换在催化剂存在下连续生产高分子聚酯的方法，在塔式反应器中形成预聚物 和缩聚反应在缩聚反应器中形成高分子聚酯，在塔式反应器中制备具有> 40至70个重复单元（DP）的预聚物，该预聚物仅在一个另外的反应器中缩聚形成> 150 至205 DP。
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5.发明申请公开(公告)号：US20120136132A1
公开(公告)日：2012-05-31
申请号：US13355938
申请日：2012-01-23
CPC分类号： B01J19/247 , B01J19/18 , B01J19/1862 , B01J19/20 , B01J2219/00006 , B01J2219/00081 , B01J2219/00083 , B01J2219/00085 , B01J2219/00087 , B01J2219/00092 , B01J2219/00094 , B01J2219/00103 , B01J2219/0011 , B01J2219/00159 , B01J2219/00768 , B01J2219/0077 , B01J2219/00779 , B01J2219/182 , B01J2219/185 , B01J2219/1943 , C08G63/78 , C08G63/785 , C08G63/83 , C08G63/85
摘要： The present invention relates to a method for the continuous production of high-molecular polyesters by esterification of dicarboxylic acids and/or transesterification of dicarboxylic acid esters with diols and/or mixtures thereof in the presence of catalysts with formation of a prepolymer in a tower reactor and polycondensation thereof to form a high-molecular polyester in a polycondensation reactor, a prepolymer with >40 to 70 repeat units (DP) being produced in the tower reactor and this prepolymer being polycondensed in only one further reactor to form a polyester with >150 to 205 DP.
摘要翻译： 本发明涉及通过二羧酸酯化和/或二羧酸酯与二醇和/或其混合物的酯交换在催化剂存在下连续生产高分子聚酯的方法，在塔式反应器中形成预聚物 和缩聚反应在缩聚反应器中形成高分子聚酯，在塔式反应器中制备具有> 40至70个重复单元（DP）的预聚物，该预聚物仅在一个另外的反应器中缩聚形成> 150 至205 DP。
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公开(公告)号：US5779986A
公开(公告)日：1998-07-14
申请号：US571137
申请日：1995-12-12
CPC分类号： C08G63/785 , B01F3/10 , B01F7/10 , B01J19/18 , C08G85/00 , B01F15/00883 , B01F7/00133 , B01J2219/00092 , B01J2219/00094 , B01J2219/00182 , B01J2219/00189 , B01J2219/182
摘要： The reactor device comprises a horizontally-disposed housing (1), at one end of which there is disposed an inlet (4) for supply of the medium, and at the other end of which there is an outlet (5) for the reaction products. Within the housing (1) of the reactor device a rotor (1) is rotatably mounted. The rotor (8) has a hollow cylinder (9), which is provided with openings (10) and annular members (12, 13) for moving and transporting the medium. The hollow cylinder (9) is partly immersed in the free-flowing medium, the openings (10) in the hollow cylinder (9) ensuring additional admixture of the medium.
摘要翻译： 反应器装置包括水平布置的壳体（1），其一端设置有用于供应介质的入口（4），并且其另一端具有用于反应产物的出口（5） 。 在反应器装置的壳体（1）内，转子（1）可旋转地安装。 转子（8）具有中空圆柱体（9），其设置有用于移动和传送介质的开口（10）和环形构件（12,13）。 中空圆筒（9）部分地浸没在自由流动的介质中，中空圆柱体（9）中的开口（10）确保介质的附加混合。
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公开(公告)号：US08110149B2
公开(公告)日：2012-02-07
申请号：US12302254
申请日：2007-05-31
CPC分类号： B01J19/247 , B01J19/18 , B01J19/1862 , B01J19/20 , B01J2219/00006 , B01J2219/00081 , B01J2219/00083 , B01J2219/00085 , B01J2219/00087 , B01J2219/00092 , B01J2219/00094 , B01J2219/00103 , B01J2219/0011 , B01J2219/00159 , B01J2219/00768 , B01J2219/0077 , B01J2219/00779 , B01J2219/182 , B01J2219/185 , B01J2219/1943 , C08G63/78 , C08G63/785 , C08G63/83 , C08G63/85
摘要： The present invention relates to a method for the continuous production of high-molecular polyesters by esterification of dicarboxylic acids and/or transesterification of dicarboxylic acid esters with diols and/or mixtures thereof in the presence of catalysts with formation of a prepolymer in a tower reactor and polycondensation thereof to form a high-molecular polyester in a polycondensation reactor, a prepolymer with >40 to 70 repeat units (DP) being produced in the tower reactor and this prepolymer being polycondensed in only one further reactor to form a polyester with >150 to 205 DP.
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8.发明授权Tower reactor and use thereof for the continuous production of high molecular weight polyesters 失效塔式反应器及其用于连续生产高分子量聚酯的用途公开(公告)号：US07608225B2
公开(公告)日：2009-10-27
申请号：US10573937
申请日：2004-10-29
CPC分类号： C08G63/785 , B01J19/1887 , B01J19/247 , B01J2219/00094 , B01J2219/00103 , B01J2219/0011 , B01J2219/00162 , B01J2219/00166 , B01J2219/00247
摘要： The invention relates to a tower reactor and the use thereof for producing high-molecular weight polyesters, such as e.g. polyethylene terephthalate (PET), polybutylene terephthalate (PBT), polynaphthalene terephthalate (PEN), polytrimethylene terephthalate (PTT) and/or polyesters of other dicarboxylic acids and diols including copolymers thereof. It thereby concerns a single-stage tower reactor.
摘要翻译： 本发明涉及塔式反应器及其用于生产高分子量聚酯的用途， 聚对苯二甲酸乙二醇酯（PET），聚对苯二甲酸丁二醇酯（PBT），聚萘二甲酸对苯二甲酸酯（PEN），聚对苯二甲酸丙二醇酯（PTT）和/或其他二羧酸和二醇的聚酯，包括它们的共聚物。 因此涉及单级塔式反应器。
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9.发明授权Method for increasing the molecular weight of a polyester granulate by using its residual heat 有权通过使用其余热来提高聚酯颗粒的分子量的方法公开(公告)号：US08877107B2
公开(公告)日：2014-11-04
申请号：US13246051
申请日：2011-09-27
CPC分类号： C08G63/80 , B01J19/1806 , B29B9/065 , B29B9/16 , B29B2009/165 , B29B2009/168 , F26B17/14
摘要： The present invention relates to increasing the molecular weight during a thermal treatment of polyester in combination with a latent heat granulation. With the newly-developed method, an SSP (Solid State Postcondensation) can be directly combined with an underwater granulation. The method differs from a conventional solid state postcondensation by an increase in the molecular weight being possible without additional heat input and hence only by using the residual heat and the crystallization heat present. A characterizing element is improved water separation and dehumidification during the granulation. Only in this way is an increase in viscosity possible even with a small granulate of an average particle weight less than 20 mg.
摘要翻译： 本发明涉及在热处理聚酯时与潜热造粒相结合的增加分子量。 采用新开发的方法，SSP（固态缩聚）可直接与水下造粒结合。 该方法不同于常规的固态缩合，通过在没有额外的热输入的情况下分子量的增加是可能的，因此仅通过使用存在的残余热和结晶热。 特征元素在造粒期间改善了水分离和除湿。 只有这样，即使使用平均颗粒重量小于20mg的小颗粒也可以增加粘度。
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10.发明申请METHOD FOR INCREASING THE MOLECULAR WEIGHT OF A POLYESTER GRANULATE BY USING ITS RESIDUAL HEAT 有权通过使用残留热量增加聚酯纤维素分子量的方法公开(公告)号：US20120077951A1
公开(公告)日：2012-03-29
申请号：US13246051
申请日：2011-09-27
IPC分类号： C08G63/88 , C08G63/183
CPC分类号： C08G63/80 , B01J19/1806 , B29B9/065 , B29B9/16 , B29B2009/165 , B29B2009/168 , F26B17/14
摘要： The present invention relates to increasing the molecular weight during a thermal treatment of polyester in combination with a latent heat granulation. With the newly-developed method, an SSP (Solid State Postcondensation) can be directly combined with an underwater granulation. The method differs from a conventional solid state postcondensation by an increase in the molecular weight being possible without additional heat input and hence only by using the residual heat and the crystallisation heat present. A characterising element is improved water separation and dehumidification during the granulation. Only in this way is an increase in viscosity possible even with a small granulate of an average particle weight less than 20 mg.
摘要翻译： 本发明涉及在热处理聚酯时与潜热造粒相结合的增加分子量。 采用新开发的方法，SSP（固态缩聚）可直接与水下造粒结合。 该方法不同于常规的固态缩合，通过增加分子量可以在没有额外的热量输入的情况下，因此仅通过使用剩余热量和存在的结晶热量。 特征元素在造粒期间改善了水分离和除湿。 只有这样，即使使用平均颗粒重量小于20mg的小颗粒也可以增加粘度。
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