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    Continuous process for the preparation of sodium titanate nanotubes
    1.
    发明授权
    Continuous process for the preparation of sodium titanate nanotubes 有权
    制备钛酸钠纳米管的连续工艺

    公开(公告)号：US08545795B2

    公开(公告)日：2013-10-01

    申请号：US12007970

    申请日：2008-01-17

    申请人： Edisson Morgado Junior ,  Marco Antonio Santos De Abreu ,  Gustavo Torres Moure

    发明人： Edisson Morgado Junior ,  Marco Antonio Santos De Abreu ,  Gustavo Torres Moure

    IPC分类号： C01G23/00

    CPC分类号： C01G23/005 ,  B82Y30/00 ,  C01P2002/72 ,  C01P2004/04 ,  C01P2004/13 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/12

    摘要： The invention relates to a process carried out continuously in one or more reactors connected in series for the preparation of sodium titanate nanotubes and their derivatives obtained by ion exchange and/or thermal treatment, by reacting titanium oxides with sodium hydroxide under suitable hydrothermal conditions to obtain or control the morphology of nanostructural titanates. The reaction mixture is introduced continuously into the reactor at a feed rate that is the same as the rate of discharge of the product. When more than one reactor is used, the material leaving the first reactor is used to feed the next reactor, and a differential of temperature is applied between the reactors in such a way as to obtain in the average, a temperature of between 60° C. and 180° C.

    摘要翻译： 本发明涉及在一个或多个反应器中连续进行的方法，该反应器串联连接制备钛酸钠纳米管及其通过离子交换和/或热处理获得的衍生物，通过在合适的水热条件下使二氧化钛与氢氧化钠反应以获得 或控制纳米结构钛酸盐的形态。 将反应混合物以与产物的排放速率相同的进料速率连续引入反应器。 当使用多于一个反应器时，离开第一反应器的材料用于进料下一个反应器，并且在反应器之间以这样的方式施加温度差，以平均获得温度在60℃ 和180℃

    Molecular sieves of faujasite structure
    4.
    发明授权
    Molecular sieves of faujasite structure 失效
    八面沸石结构分子筛

    公开(公告)号：US06756029B2

    公开(公告)日：2004-06-29

    申请号：US10164926

    申请日：2002-06-07

    申请人： Yiu Lau Lam ,  Alvaro Saavedra ,  Alexandre de Figueiredo Costa ,  Anselmo da Silva Santos ,  Gustavo Torres Moure ,  Rodolfo Eugenio Roncolatto ,  Dennis Stamires ,  Paul O'Connor

    发明人： Yiu Lau Lam ,  Alvaro Saavedra ,  Alexandre de Figueiredo Costa ,  Anselmo da Silva Santos ,  Gustavo Torres Moure ,  Rodolfo Eugenio Roncolatto ,  Dennis Stamires ,  Paul O'Connor

    IPC分类号： C01B3924

    CPC分类号： C10G11/05 ,  B01J29/084 ,  C01B39/24 ,  C10G49/08 ,  Y10S423/21

    摘要： A process for preparing molecular sieves of type Y faujasite structure is described, as well as pre-shaped bodies of faujasite structure type Y molecular sieves. The process comprises preparing a precursor gel from a source of silica-alumina or a source of alumina and a source of silica with a template agent at a SiO2/Al2O3 greater than 7 and suitable for forming a type Y zeolite, drying the precursor gel and contacting the dried precursor gel with steam, optionally followed by caustic washing, without the formation of crystalline phases other than type Y zeolite being observed. Advantageously, the pre-shaped bodies prepared with the precursor gel of Y zeolite, when subjected to the process of the invention, will have their outer surface covered by type Y zeolite crystals. The molecular sieves so obtained may be employed as catalysts or adsorbents in various processes of the chemical or oil industry.

    摘要翻译： 描述了制备Y型八面沸石结构的分子筛的方法，以及Y型分子筛的八面沸石结构体的预制体。 该方法包括从二氧化硅 - 氧化铝源或氧化铝源和二氧化硅源以二氧化硅/ Al 2 O 3大于7的模板剂制备前体凝胶并适于形成Y型沸石，干燥前体凝胶和 使干燥的前体凝胶与蒸汽接触，任选地随后进行苛性碱洗涤，而不形成除Y型沸石以外的结晶相。 有利的是，当用Y沸石的前体凝胶制备的预制体在进行本发明的方法时，其外表面将被Y型沸石晶体覆盖。 如此获得的分子筛可用作化学或石油工业的各种方法中的催化剂或吸附剂。

    Continuous process for the preparation of sodium titanate nanotubes
    6.
    发明申请
    Continuous process for the preparation of sodium titanate nanotubes 有权
    制备钛酸钠纳米管的连续工艺

    公开(公告)号：US20100284902A1

    公开(公告)日：2010-11-11

    申请号：US12007970

    申请日：2008-01-17

    申请人： Edisson Morgado Junior ,  Marco Antonio De Abreu ,  Gustavo Torres Moure

    发明人： Edisson Morgado Junior ,  Marco Antonio De Abreu ,  Gustavo Torres Moure

    IPC分类号： C01G23/04 ,  C01D1/02

    CPC分类号： C01G23/005 ,  B82Y30/00 ,  C01P2002/72 ,  C01P2004/04 ,  C01P2004/13 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/12

    摘要： The invention relates to a continuous process for the preparation of sodium titanate nanotubes and their derivatives obtained by ion exchange and/or thermal treatment, by reacting titanium oxides with sodium hydroxide under suitable hydrothermal conditions to obtain or control the morphology of nanostructural titanates.The method is carried out continuously in one or more reactors connected in series, where the reaction mixture is introduced continuously into the reactor at a feed rate that is the same as the rate of discharge of the product. When more than one reactor is used, the material leaving the first reactor is used to feed the next reactor, and preferably a temperature differential is applied between the reactors in such a way as to obtain a mean temperature of between 60 and 180° C., and the overall reaction time is short, being about 90 minutes or less.The nanostructures obtained can be later subjected to ion exchange and/or thermal treatment in an inert, oxidizing or reducing atmosphere in order to prepare adsorbents, catalysts, photocatalysts, electrocatalysts, or else electrodes for photovoltaic cells, lithium batteries, gas sensors and systems for the separation and storage of hydrogen.

    摘要翻译： 本发明涉及通过离子交换和/或热处理制备钛酸钠纳米管及其衍生物的连续方法，通过在合适的水热条件下使二氧化钛与氢氧化钠反应以获得或控制纳米结构的钛酸盐的形态。 该方法在连续串联的一个或多个反应器中连续进行，其中反应混合物以与产物的排放速率相同的进料速率连续引入反应器。 当使用多于一个反应器时，离开第一反应器的材料用于进料下一个反应器，并且优选地在反应器之间以这样的方式施加温差以获得在60和180℃之间的平均温度。 ，总反应时间短，为约90分钟以下。 所获得的纳米结构可以在惰性，氧化或还原气氛中进行离子交换和/或热处理，以制备吸附剂，催化剂，光催化剂，电催化剂，或用于光伏电池的电极，锂电池，气体传感器和用于 氢的分离和储存。