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    Oligomers And Polymers Containing Sulfinate Groups And Method For The Production Thereof
    1.
    发明申请
    Oligomers And Polymers Containing Sulfinate Groups And Method For The Production Thereof 有权
    含有亚磺酸盐的低聚物和聚合物及其制备方法

    公开(公告)号：US20090221759A1

    公开(公告)日：2009-09-03

    申请号：US12324320

    申请日：2008-11-26

    Applicant: Thomas Haring ,  Jochen Kerres ,  Wei Zhang

    Inventor： Thomas Haring ,  Jochen Kerres ,  Wei Zhang

    IPC: C08F126/06 ,  C08G16/00

    CPC classification number: H01M6/181 ,  C08C19/02 ,  C08F8/04 ,  C08J5/2243 ,  C08J2381/00 ,  H01M8/1023 ,  H01M8/1025 ,  H01M8/1027 ,  H01M8/103 ,  H01M8/1032 ,  H01M8/1039 ,  H01M8/1072 ,  Y02P70/56

    Abstract: The invention relates to novel polymers or oligomers containing at least sulfinate groups (P-(SO2)nX, X=1-(n=1), 2-(n=2) or 3-(n=3) valent metal cation or H+ or ammonium ion NR4+ where R=alkyl, aryl, H), which are obtained by completely or partially reducing polymers or oligomers containing at least SO2Y-groups (Y═F, Cl, Br, I, OR, NR2 (R=alkyl and/or aryl and/or H), N-imidazolyL N-pyrazolyl) by means of suitable reducing agents in a suspension or in a solution formPolymer and polymer(blend)membranes which are obtained by further reacting the received sulfinated polymers, especially by alkylation of the sulfinate groups with mono- di- or oligo functional electrophiles. The invention further relates to methods for producing the sulfinated polymers and for further reacting the sulfinated polymers with electrophiles by S-alkylation.

    Abstract translation: 本发明涉及至少含有亚磺酸基团（P-（SO 2）n X，X = 1-（n = 1），2-（n = 2）或3-（n = 3）价金属阳离子或 通过完全或部分还原含有至少SO 2 Y基团（YF，Cl，Br，I，OR，NR 2（R =烷基和/或烷基）的聚合物或低聚物）获得的H +或铵离子NR4 +，其中R =烷基，芳基，H） 或芳基和/或H），N-咪唑并吡唑基），通过合适的还原剂以悬浮液或溶液形式聚合物和聚合物（共混物）膜，其通过进一步使所接收的磺化聚合物反应而获得，特别是通过烷基化 的亚硫酸酯基团与单 - 或寡功能亲电试剂。 本发明还涉及用于生产硫化聚合物的方法，以及通过S-烷基化进一步使硫化聚合物与亲电体反应。

    Oligomers and polymers containing sulfonite groups and method for the production thereof
    3.
    发明授权
    Oligomers and polymers containing sulfonite groups and method for the production thereof 有权
    含有亚磺酸基团的低聚物和聚合物及其制备方法

    公开(公告)号：US07202327B2

    公开(公告)日：2007-04-10

    申请号：US10488420

    申请日：2002-09-02

    Applicant: Thomas Häring ,  Jochen Kerres ,  Wei Zhang

    Inventor： Thomas Häring ,  Jochen Kerres ,  Wei Zhang

    IPC: C08G75/00 ,  C08F28/02 ,  A61K7/06 ,  A61K7/11

    CPC classification number: H01M6/181 ,  C08C19/02 ,  C08F8/04 ,  C08J5/2243 ,  C08J2381/00 ,  H01M8/1023 ,  H01M8/1025 ,  H01M8/1027 ,  H01M8/103 ,  H01M8/1032 ,  H01M8/1039 ,  H01M8/1072 ,  Y02P70/56

    Abstract: The invention relates to novel polymers or oligomers containing at least sulfonite groups (P-(SO2)nX, X=1−(n=1), 2−(n=2) or 3−(n=3) valent metal cation or H+ or ammonium ion NR4+ wherein R=alkyl, aryl, H), which are obtained by completely or partially reducing polymers or oligomers containing at least SO2Y-groups (Y=F, Cl, Br, I, OR, NR2 (R=alkyl and/or aryl and/or H), N-imidazolyl, N-pyrazolyl) by means of suitable reducing agents in a suspension or in a solution form. The invention also relates to polymers and polymer(blend) membranes which are obtained by further reacting the obtained sulfinated polymers, especially by alkylation of the sulfinate groups with mono- di- or oligo functional electrophiles. The invention further relates to methods for producing the sulfinated polymers and for further reacting the sulfinated polymers with electrophiles by S-alkylation.

    Abstract translation: 本发明涉及至少含有亚磺酸基团的新型聚合物或低聚物（X-1-（n = 1），2-（ n = 2）或3-（n = 3）价金属阳离子或H +或铵离子NR 4 +其中R =烷基， 芳基，H），其通过完全或部分还原含有至少SO 2 Y-基团（Y = F，Cl，Br，I，OR，NR 2）的聚合物或低聚物而获得， （R =烷基和/或芳基和/或H），N-咪唑基，N-吡唑基），通过合适的还原剂以悬浮液或溶液形式存在。 本发明还涉及聚合物和聚合物（共混物）膜，其通过进一步使得到的硫化聚合物反应而获得，特别是通过亚磺酸基团与单 - 或寡官能亲电体的烷基化。 本发明还涉及用于生产硫化聚合物的方法，以及通过S-烷基化进一步使硫化聚合物与亲电体反应。

    Phosphonic acid-containing blends and phosphonic acid-containing polymers
    5.
    发明授权
    Phosphonic acid-containing blends and phosphonic acid-containing polymers 有权
    含膦酸的共混物和含膦酸的聚合物

    公开(公告)号：US08637174B2

    公开(公告)日：2014-01-28

    申请号：US12278245

    申请日：2007-02-05

    Applicant: Thomas Häring ,  Jochen Kerres ,  Frank Schönberger ,  Martin Hein

    Inventor： Thomas Häring ,  Jochen Kerres ,  Frank Schönberger ,  Martin Hein

    IPC: H01M8/10

    CPC classification number: H01M8/1034 ,  B01J39/20 ,  C08G61/02 ,  C08G61/122 ,  C08J5/2287 ,  C08J2341/00 ,  H01M8/1011 ,  H01M8/1023 ,  H01M8/1025 ,  H01M8/1027 ,  H01M8/103 ,  H01M8/1032 ,  H01M8/1039 ,  H01M8/1044 ,  H01M8/1048 ,  H01M8/1072 ,  H01M2008/1095 ,  H01M2300/0082 ,  Y02E60/522 ,  Y02E60/523 ,  Y02P70/56

    Abstract: Various blends and blend membranes from low-molecular hydroxymethylene-oligo-phosphonic acids R—C(PO3H2)x(OH)y and polymers, the group R representing any organic group, the polymers containing cation exchanger groups or their nonionic precursors of the type SO2X, X being a halogen, OH, OMe, NR1R2, OR1 with Me being any metal cation or ammonium cation, R1, R2 being H or any aryl- or alkyl group, PDX2, COX and/or basic groups such as primary, secondary or tertiary amino groups, imidazole groups, pyridine groups, pyrazole groups etc. and/or OH groups. Such membranes may also include polymers that are modified with the 1-hydroxymethylene-1,1-bisphosphonic acid group. The polymers may be formed by reacting polymers which contain carboxylic acid groups or carboxylic halide groups —COHal (Hal=F, Cl, Br, I) with phosphite compounds or by reacting polymeric aldehydes or polymeric keto compounds with phosphite esters while carrying out an amine catalysis, an oxidation of the intermediary hydroxyphosphonic acid with MnO2 or another oxidant.

    Abstract translation: 来自低分子羟基亚甲基 - 寡聚膦酸RC（PO 3 H 2）x（OH）y和聚合物的各种共混物和共混膜，R代表任何有机基团，含有阳离子交换剂基团的聚合物或其SO 2 X型非离子前体， X是卤素，OH，OMe，NR1R2，OR1，其中Me是任何金属阳离子或铵阳离子，R1，R2是H或任何芳基或烷基，POX2，COX和/或碱性基团如伯，仲或叔 氨基，咪唑基，吡啶基，吡唑基等和/或OH基。 这样的膜还可以包括用1-羟基亚甲基-1,1-二膦酸基团改性的聚合物。 聚合物可以通过使含有羧酸基团或羧酸卤化物-COHal（Hal = F，Cl，Br，I）的聚合物与亚磷酸酯化合物或通过使聚合醛或聚合酮化合物与亚磷酸酯反应同时进行胺 催化，中间体羟基膦酸与MnO2或另一种氧化剂的氧化。

    Method for producing a proton-conducting, structured electrolyte membrane
    6.
    发明授权
    Method for producing a proton-conducting, structured electrolyte membrane 有权
    生产质子传导结构电解质膜的方法

    公开(公告)号：US08592091B2

    公开(公告)日：2013-11-26

    申请号：US12987772

    申请日：2011-01-10

    Applicant: Gilbert Erdler ,  Holger Reinecke ,  Mirko Frank ,  Claas Mueller ,  Jochen Kerres

    Inventor： Gilbert Erdler ,  Holger Reinecke ,  Mirko Frank ,  Claas Mueller ,  Jochen Kerres

    IPC: H01M8/00

    CPC classification number: C08J5/2256 ,  B01D67/0034 ,  B01D2323/30 ,  B01D2323/34 ,  B01D2325/26 ,  C08J2381/06 ,  C08J2479/06 ,  H01M8/1025 ,  H01M8/1076 ,  H01M2300/0082 ,  Y02P70/56

    Abstract: In a method for producing a proton-conductive, structured electrolyte membrane, particularly for a fuel cell, a coating, which comprises at least one ion-conductive cross-linking component having at least one acid group and at least one photoactive substances interacting therewith, is applied onto a solid body surface. The coating is optically masked in that at least one region of the coating, in which the electrolyte membrane is supposed to be, is exposed such that the cross-linking component cross-links with the photoactive substances to form a polymer and/or copolymer network adhering to the solid body surface. At least one unexposed region of the coating is removed in order to structure the electrolyte membrane.

    Abstract translation: 在制造质子传导性结构化电解质膜，特别是用于燃料电池的方法中，包括至少一种具有至少一个酸基的离子传导性交联组分和至少一种与其相互作用的光活性物质的涂层， 施加到固体表面上。 该涂层被光学掩模，因为其中假定电解质膜的涂层的至少一个区域被暴露，使得交联组分与光活性物质交联以形成聚合物和/或共聚物网络 坚固的身体表面。 为了构造电解质膜，去除了涂层的至少一个未曝光区域。

    Composites and Composite Membranes
    8.
    发明申请
    Composites and Composite Membranes 审中-公开
    复合材料和复合膜

    公开(公告)号：US20100151352A1

    公开(公告)日：2010-06-17

    申请号：US12636323

    申请日：2009-12-11

    Applicant: Thomas Haring ,  Vladimir Linkov ,  Jochen Kerres ,  Andreas Ullrich ,  Chy-Ming Tang ,  Martin Hein ,  Wei Zhang

    Inventor： Thomas Haring ,  Vladimir Linkov ,  Jochen Kerres ,  Andreas Ullrich ,  Chy-Ming Tang ,  Martin Hein ,  Wei Zhang

    IPC: H01M8/10 ,  C25C7/04 ,  B01D61/42 ,  C08J5/22 ,  B05D3/02 ,  B01D61/36 ,  C02F1/44 ,  B01D61/02 ,  B01D53/22 ,  H01M6/18

    CPC classification number: B01D67/0093 ,  B01D67/0006 ,  B01D67/0011 ,  B01D69/12 ,  B01D69/141 ,  B01D71/00 ,  B01D71/52 ,  B01D71/62 ,  B01D71/82 ,  B01D2323/30 ,  B01D2325/14 ,  C08J5/2275 ,  C08J2379/06 ,  C25B13/08 ,  H01B1/122 ,  H01M8/1025 ,  H01M8/1027 ,  H01M8/103 ,  H01M8/1032 ,  H01M8/1048 ,  H01M8/1051 ,  H01M8/1081 ,  H01M8/1088 ,  H01M10/05 ,  H01M10/0565 ,  Y02P70/56

    Abstract: The invention relates to the following types of composite membranes; composites or composite membranes obtained by adding a metal salt, e.g. from ZrOCl2, to a solvent, especially DMSO, for dissolving one or more polymers in an organic solvent or in aqueous systems, in addition to the subsequent precipitation in the matrix of the thus produced composite-membrane by post-treatment thereof in an acid or in a salt solution, especially phosphoric acid. The invention also relates to composites or composite membranes obtained by subsequent ion exchange of finished polymer membranes with a suitable salt cation, especially ZrO2+, wherein the polymer membrane is, optionally, swollen with an organic solvent or a mixture of organic solvent with water prior to the ion exchange and the subsequent precipitation of a low soluble salt, e.g. from Zr3(PO4)4, in the membrane by post-treatment thereof in an acid or in a salt solution, especially phosphoric acid. The invention further relates to composites or composite membranes obtained by adding nano-scaled Zr3(PO4)4 powder to a polymer solution, composites and composite membranes obtained according to the above-mentioned methods, wherein additional heteropoly acids are also incorporated into the polymer or membrane morphology, in addition to methods for producing said inventive polymers and membranes.

    Abstract translation: 本发明涉及以下类型的复合膜; 复合材料或复合膜，通过加入金属盐， 从ZrOCl 2到溶剂，特别是DMSO中，用于将一种或多种聚合物溶解在有机溶剂或水性体系中，以及随后通过在酸中后处理由此制备的复合膜的基质中的沉淀，或 在盐溶液中，特别是磷酸。 本发明还涉及通过随后使用合适的盐阳离子，特别是ZrO 2 +离子交换成品聚合物膜而获得的复合材料或复合膜，其中聚合物膜任选地在有机溶剂或有机溶剂与水的混合物之前在水中溶胀 离子交换和随后的低溶解盐沉淀，例如 通过在酸或盐溶液，特别是磷酸中后处理，从Zr3（PO4）4中除去。 本发明还涉及通过将纳米级Zr 3（PO 4）4粉末加入到根据上述方法获得的聚合物溶液，复合材料和复合膜中而获得的复合材料或复合膜，其中另外的杂多酸也被引入聚合物或 膜形态，以及用于制备所述本发明聚合物和膜的方法。

    Cross-linking of modified engineering thermoplastics
    10.
    发明授权
    Cross-linking of modified engineering thermoplastics 失效
    改性工程热塑性塑料的交联

    公开(公告)号：US06552135B2

    公开(公告)日：2003-04-22

    申请号：US09760630

    申请日：2001-01-16

    Applicant: Werner Schnurnberger ,  Jochen Kerres ,  Wei Cui

    Inventor： Werner Schnurnberger ,  Jochen Kerres ,  Wei Cui

    IPC: C08F834

    CPC classification number: B01J39/20 ,  C08G75/00

    Abstract: The present invention pertains to a process for the cross-linking of modified engineering thermoplastics, in particular, of polymeric sulfinic acids or sulfinic acid salts. In particular, the invention pertains to a process for the preparation of cross-linked polymers, characterized in that solutions of polymeric sulfinic acids or sulfinic acid salts (—SO2Me), optionally in the presence of organic di- or oligohalogeno compounds [R(Hal)x], are freed from solvent and cross-linked to polymers, wherein Me stands for a monovalent or polyvalent metal cation; R stands for an optionally substituted alkyl or aryl residue containing from 1 to 20 carbon atoms; and Hal stands for F, Cl, Br or I.

    Abstract translation: 本发明涉及改性工程热塑性塑料，特别是聚合亚磺酸或亚磺酸盐交联的方法。特别地，本发明涉及制备交联聚合物的方法，其特征在于： 聚合亚磺酸或亚磺酸盐（-SO 2 Me）的溶液，任选在有机二卤代或低卤代化合物[R（Hal）x]存在下，不溶于溶剂并与聚合物交联，其中Me代表单价或 多价金属阳离子; R代表含有1至20个碳原子的任选取代的烷基或芳基; 而H代表F，Cl，Br或I.

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