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    Modified Natural Graphite Particles
    1.
    发明申请
    Modified Natural Graphite Particles 审中-公开
    改性天然石墨颗粒

    公开(公告)号：US20140093781A1

    公开(公告)日：2014-04-03

    申请号：US14110240

    申请日：2012-04-03

    申请人： Katsuhiro Nishihara ,  Hiroshi Yamamoto ,  Tatsuo Nagata ,  Noriyuki Negi ,  Tooru Fujiwara

    发明人： Katsuhiro Nishihara ,  Hiroshi Yamamoto ,  Tatsuo Nagata ,  Noriyuki Negi ,  Tooru Fujiwara

    IPC分类号： H01M4/587

    CPC分类号： H01M4/587 ,  C01B32/20 ,  C01P2006/10 ,  C01P2006/11 ,  C01P2006/19 ,  H01M4/133 ,  H01M4/366 ,  H01M10/052

    摘要： A modified natural graphite material which provides a negative plate having improved adhesion between a negative electrode mixture and a current collector has a circularity of at least 0.92 and at most 1.0 and an incident angle dependence S60/0 of the peak intensity ratio of at least 0.5 and at most 0.7 as determined by measurement of C K-edge X-ray absorption spectra using synchrotron radiation as an excitation source. It preferably satisfies at least one of the following conditions: an absolute specific gravity of at least 2.25 (g/cm3), a tap density of at least 1.0 g/cm3 and at most 1.4 g/cm3, and linseed oil absorption of at least 20 cm3/100 g and at most 50 cm3/100 g. A carbonaceous material may adhere to at least a portion of the surface of the graphite particles.

    摘要翻译： 提供具有改善的负极混合物和集电体之间粘附性的负极板的改性天然石墨材料具有至少0.92至多1.0的圆形度，峰强度比的入射角依赖性S60 / 0至少为0.5 并且通过使用同步加速器辐射作为激发源的C K边缘X射线吸收光谱的测量来确定最多为0.7。 它优选满足以下条件中的至少一个：绝对比重至少为2.25（g / cm 3），振实密度为至少1.0g / cm 3和至多1.4g / cm 3，并且亚麻籽油吸收至少 20cm 3 / 100g和至多50cm 3 / 100g。 碳质材料可以粘附到石墨颗粒的表面的至少一部分上。

    Titanium Oxide Base Photocatalyst, Process for Producing the Same and Use Thereof
    3.
    发明申请
    Titanium Oxide Base Photocatalyst, Process for Producing the Same and Use Thereof 审中-公开
    氧化钛基光催化剂，其生产方法及用途

    公开(公告)号：US20070248831A1

    公开(公告)日：2007-10-25

    申请号：US11578874

    申请日：2005-04-19

    申请人： Katsuhiro Nishihara ,  Yasuhiro Masaki ,  Tadashi Fukuda ,  Katsumi Okada ,  Shinji Shimosaki ,  Sadanobu Nagaoka ,  Hideaki Kanno ,  Kazuomi Azuma ,  Tadashi Ogasawara

    发明人： Katsuhiro Nishihara ,  Yasuhiro Masaki ,  Tadashi Fukuda ,  Katsumi Okada ,  Shinji Shimosaki ,  Sadanobu Nagaoka ,  Hideaki Kanno ,  Kazuomi Azuma ,  Tadashi Ogasawara

    IPC分类号： B01J35/02 ,  B32B9/00

    CPC分类号： C01G23/0536 ,  B01J21/063 ,  B01J35/002 ,  B01J35/004 ,  B01J37/031 ,  C01P2006/12 ,  Y10T428/31678

    摘要： A highly active titanium oxide photocatalyst of the type responsive to visible light is prepared by subjecting a titanium (hydr)oxide raw material obtained by neutralizing an acidic titanium compound in ammonia or an amine under conditions such that the final pH is 7 or below to heat treatment in an atmosphere containing a hydrolyzable compound followed by contact with water and additional heat treatment at a temperature of at least 350° C. The resulting titanium oxide photocatalyst comprises titanium oxide with a specific surface area of at most 120 m2/g and with the amount of surface hydroxyl groups being at least 600 μeq/g. Preferably the density of surface hydroxyl groups is at least 8 μeq/m2, and the ratio of the amount of terminal type hydroxyl groups (T) to the amount of bridge type hydroxyl groups (B) in the surface hydroxyl groups satisfies T/B≧0.20. This titanium oxide photocatalyst has an ESR spectrum having two types of triplet signal for which the g values of the main spectra are 1.993-2.003 and 2.003-2.011, respectively, and it is also identified by having ratios of the strengths of these signals before irradiation with visible light, under irradiation, and immediately after the stop of irradiation which are different from conventional products.

    摘要翻译： 通过使在最终pH为7以下的条件下将氨基或胺中的酸性钛化合物得到的钛（氢化物）氧化物原料进行加热，制备对可见光敏感的高活性氧化钛光催化剂 在含有可水解化合物的气氛中进行处理，然后与水接触，并在至少350℃的温度下进行额外的热处理。所得到的氧化钛光催化剂包括比表面积至多为120μm2的氧化钛， / SUP / g，表面羟基的量为至少600mueq / g。 优选地，表面羟基的密度为至少8mueq / m 2，并且末端型羟基（T）的量与桥型羟基的量的比例（B）在 表面羟基满足T / B> = 0.20。 该氧化钛光催化剂具有ESR谱，其具有两种类型的三重态信号，其主要光谱的g值分别为1.993-2.003和2.003-2.011，并且还通过在照射前具有这些信号的强度比来鉴定 具有可见光，照射下，以及在与常规产品不同的照射停止之后。

    TITANIUM OXIDE PHOTOCATALYST, METHOD FOR PRODUCING SAME AND USE THEREOF
    6.
    发明申请
    TITANIUM OXIDE PHOTOCATALYST, METHOD FOR PRODUCING SAME AND USE THEREOF 有权
    氧化钛光催化剂，其生产方法及其用途

    公开(公告)号：US20080268268A1

    公开(公告)日：2008-10-30

    申请号：US12057983

    申请日：2008-03-28

    申请人： Yasuhiro Masaki ,  Tadashi Fukuda ,  Katsuhiro Nishihara ,  Rie Katsui

    发明人： Yasuhiro Masaki ,  Tadashi Fukuda ,  Katsuhiro Nishihara ,  Rie Katsui

    IPC分类号： B32B15/04 ,  B01J23/00 ,  B01J21/00

    CPC分类号： B01J35/004 ,  B01D2255/20707 ,  B01D2255/802 ,  B01J21/06 ,  B01J21/063 ,  B01J21/066 ,  B01J23/18 ,  B01J35/002 ,  B01J37/033

    摘要： A titanium oxide-based photocatalyst which can exhibit excellent photocatalytic properties in response to visible light while maintaining its inherent activity in response to ultraviolet light and which is suitable for mass production contains bismuth as a first additional metal component and at least one metal element selected from silicon, zirconium, aluminum, and hafnium as a second additional metal component in titanium oxide. The Bi/Ti atomic ratio is preferably at least 0.0001 and at most 1.0, the atomic ratio of the second additional metal to Ti is preferably at least 0.0001 and at most 0.8, and a portion of bismuth is preferably present in the form of lower valence (Bi2+ or Bi0). The presence of lower valence bismuth can be ascertained by XPS analysis.

    摘要翻译： 可以在可见光下表现出优异的光催化性能，同时保持其响应于紫外线的固有活性并且适合于批量生产的二氧化钛基光催化剂包含铋作为第一附加金属组分和至少一种选自 硅，锆，铝和铪作为氧化钛中的第二另外的金属组分。 Bi / Ti原子比优选为0.0001以上且1.0以下，第二附加金属与Ti的原子比优选为0.0001以上且0.8以下，铋的一部分优选以低价存在 （Bi 2+ +或Bi 0）。 低价铋的存在可以通过XPS分析来确定。

    Titanium oxide photocatalyst, method for producing same and use thereof
    7.
    发明授权
    Titanium oxide photocatalyst, method for producing same and use thereof 有权
    氧化钛光催化剂及其制造方法及其用途

    公开(公告)号：US07858201B2

    公开(公告)日：2010-12-28

    申请号：US12057983

    申请日：2008-03-28

    申请人： Yasuhiro Masaki ,  Tadashi Fukuda ,  Katsuhiro Nishihara ,  Rie Katsui

    发明人： Yasuhiro Masaki ,  Tadashi Fukuda ,  Katsuhiro Nishihara ,  Rie Katsui

    IPC分类号： B32B15/04 ,  B01J23/00 ,  B01J21/00

    CPC分类号： B01J35/004 ,  B01D2255/20707 ,  B01D2255/802 ,  B01J21/06 ,  B01J21/063 ,  B01J21/066 ,  B01J23/18 ,  B01J35/002 ,  B01J37/033

    摘要： A titanium oxide-based photocatalyst which can exhibit excellent photocatalytic properties in response to visible light while maintaining its inherent activity in response to ultraviolet light and which is suitable for mass production contains bismuth as a first additional metal component and at least one metal element selected from silicon, zirconium, aluminum, and hafnium as a second additional metal component in titanium oxide. The Bi/Ti atomic ratio is preferably at least 0.0001 and at most 1.0, the atomic ratio of the second additional metal to Ti is preferably at least 0.0001 and at most 0.8, and a portion of bismuth is preferably present in the form of lower valence (Bi2+ or Bi0). The presence of lower valence bismuth can be ascertained by XPS analysis.

    摘要翻译： 可以在可见光下表现出优异的光催化性能，同时保持其响应于紫外线的固有活性并且适合于批量生产的二氧化钛基光催化剂包含铋作为第一附加金属组分和至少一种选自 硅，锆，铝和铪作为氧化钛中的第二另外的金属组分。 Bi / Ti原子比优选为0.0001以上且1.0以下，第二附加金属与Ti的原子比优选为0.0001以上且0.8以下，铋的一部分优选以低价存在 （Bi2 +或Bi0）。 低价铋的存在可以通过XPS分析来确定。