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公开(公告)号：US07691200B2
公开(公告)日：2010-04-06
申请号：US11909505
申请日：2006-03-24
CPC分类号： C30B29/16 , C23C14/081 , C30B11/003 , C30B23/066
摘要： Provided is a MgO single crystal for obtaining a magnesium oxide (MgO) single crystal deposition material which is prevented from splashing during the vapor deposition in, e.g., an electron beam deposition method without reducing the deposition rate, and for obtaining a MgO single crystal substrate which can form thereon, e.g., a superconductor thin film having excellent superconducting properties. A MgO single crystal having a calcium content of 150×10−6 to 1,000×10−6 kg/kg and a silicon content of 10×10−6 kg/kg or less, wherein the MgO single crystal has a variation of 30% or less in terms of a CV value in detected amounts of calcium fragment ions, as analyzed by TOF-SIMS with respect to the polished surface of the MgO single crystal. A MgO single crystal deposition material and a MgO single crystal substrate for forming a thin film obtained from the MgO single crystal.
摘要翻译： 本发明提供一种用于获得氧化镁（MgO）单晶沉积材料的MgO单晶，其在例如电子束沉积方法中在气相沉积期间防止溅射而不降低沉积速率，并且获得MgO单晶衬底 其可以在其上形成，例如具有优异超导性能的超导体薄膜。 钙含量为150×10 -6〜1,000×10 -6 kg / kg，硅含量为10×10 -6 kg / kg以下的MgO单晶，其中，MgO单晶的变化率为30％ 根据TOF-SIMS相对于MgO单晶的抛光表面的分析，检测到的钙碎片离子量的CV值以下。 一种MgO单晶沉积材料和用于形成由MgO单晶获得的薄膜的MgO单晶衬底。
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2.发明授权Phosphorus-containing coated magnesium oxide powder, method for producing same, and resin composition containing such powder 失效含磷的包覆氧化镁粉末，其制造方法和含有该粉末的树脂组合物公开(公告)号：US07393885B2
公开(公告)日：2008-07-01
申请号：US10597007
申请日：2005-12-01
CPC分类号： C01F5/02 , C01P2004/80 , C08K9/02 , C09C1/028 , H01L23/295 , H01L23/564 , H01L2924/0002 , H05K1/0373 , H05K2201/0209 , Y10T428/2991 , Y10T428/2993 , H01L2924/00
摘要： A phosphorus-containing coated magnesium oxide powdered material comprising a coated magnesium oxide powdered material having a surface coating layer comprised of a double oxide, wherein the phosphorus-containing coated magnesium oxide powdered material has a coating layer comprised of a magnesium phosphate compound in at least part of a surface of the coated magnesium oxide powdered material, wherein the content of the magnesium phosphate compound in the coated magnesium oxide powdered material is 0.1 to 10% by mass, in terms of phosphorus; a method for producing a phosphorus-containing coated magnesium oxide powdered material, wherein the method comprises treating a coated magnesium oxide powdered material having a surface coating layer comprised of a double oxide with a phosphorus compound, and then calcining the resultant powdered material at 300° C. or higher to form a magnesium phosphate compound in at least a part of a surface of the coated magnesium oxide powdered material; and a resin composition comprising the powder.
摘要翻译： 一种含磷涂覆的氧化镁粉末材料，其包含具有由双氧化物构成的表面被覆层的涂覆的氧化镁粉末材料，其中所述含磷涂覆的氧化镁粉末材料具有至少包含磷酸镁化合物的涂层 涂覆的氧化镁粉末材料的表面的一部分，其中涂覆的氧化镁粉末材料中的磷酸镁化合物的含量以磷为0.1〜10质量％ 含磷涂覆的氧化镁粉末材料的制造方法，其中，所述方法包括将具有由磷化合物构成的双氧化物的表面被覆层的被覆氧化镁粉末材料处理，然后在300℃下煅烧所得粉末材料 或更高，以在涂覆的氧化镁粉末材料的表面的至少一部分中形成磷酸镁化合物; 和包含该粉末的树脂组合物。
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3.发明申请公开(公告)号：US20080081767A1
公开(公告)日：2008-04-03
申请号：US11722921
申请日：2005-12-28
摘要： A magnesium oxide single crystal having controlled crystallinity comprising a subboundary, and ranges of variation of diffraction line positions, as measured for reciprocal lattice maps with respect to a region surrounded by the same subboundary, with the range of the variation of 1×10−3 to 2×10−2 degree of on Δω coordinates, and with the range of the variation of 4×10−4 to 5×10−3 degree on 2θ coordinates.
摘要翻译： 具有包含亚边界的受控结晶度的氧化镁单晶以及衍射线位置的变化范围，如相对于由相同子边界包围的区域的互逆格子图所测量的，其变化范围为1×10 -6 3倍至2倍10倍的Deltaomega坐标，并且变化范围为4×10 -4至5×10 -3 -3 2度的坐标。
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4.发明申请Phosphorus-containing coated magnesium oxide powder, method for producing same, and resin composition containing such powder 失效含磷的包覆氧化镁粉末，其制造方法和含有该粉末的树脂组合物公开(公告)号：US20070184269A1
公开(公告)日：2007-08-09
申请号：US10597007
申请日：2005-12-01
CPC分类号： C01F5/02 , C01P2004/80 , C08K9/02 , C09C1/028 , H01L23/295 , H01L23/564 , H01L2924/0002 , H05K1/0373 , H05K2201/0209 , Y10T428/2991 , Y10T428/2993 , H01L2924/00
摘要： A phosphorus-containing coated magnesium oxide powdered material comprising a coated magnesium oxide powdered material having a surface coating layer comprised of a double oxide, wherein the phosphorus-containing coated magnesium oxide powdered material has a coating layer comprised of a magnesium phosphate compound in at least part of a surface of the coated magnesium oxide powdered material, wherein the content of the magnesium phosphate compound in the coated magnesium oxide powdered material is 0.1 to 10% by mass, in terms of phosphorus; a method for producing a phosphorus-containing coated magnesium oxide powdered material, wherein the method comprises treating a coated magnesium oxide powdered material having a surface coating layer comprised of a double oxide with a phosphorus compound, and then calcining the resultant powdered material at 300° C. or higher to form a magnesium phosphate compound in at least a part of a surface of the coated magnesium oxide powdered material; and a resin composition comprising the powder.
摘要翻译： 一种含磷涂覆的氧化镁粉末材料，其包含具有由双氧化物构成的表面被覆层的涂覆的氧化镁粉末材料，其中所述含磷涂覆的氧化镁粉末材料具有至少包含磷酸镁化合物的涂层 涂覆的氧化镁粉末材料的表面的一部分，其中涂覆的氧化镁粉末材料中的磷酸镁化合物的含量以磷为0.1〜10质量％ 一种含磷涂覆的氧化镁粉末材料的制造方法，其特征在于，将具有由磷化合物构成的双氧化物的表面被覆层的被覆氧化镁粉末材料进行处理，然后在300℃下煅烧所得粉末材料 或更高，以在涂覆的氧化镁粉末材料的表面的至少一部分中形成磷酸镁化合物; 和包含该粉末的树脂组合物。
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5.发明申请Spherical Coated Magnesium Oxide Powder, Method for Producing the Same and Resin Composition Comprising the Powder 审中-公开球形涂覆氧化镁粉末，其制造方法和包含粉末的树脂组合物公开(公告)号：US20060286295A1
公开(公告)日：2006-12-21
申请号：US10568607
申请日：2003-12-12
CPC分类号： C09C1/028 , C01F5/02 , C01P2004/32 , C01P2004/54 , C01P2004/84 , H05K1/0373 , H05K2201/0209 , Y10T428/2991
摘要： Provided is a sphere-shaped coated magnesium oxide powder having a surface coated with a double oxide and having an average shape factor of 1.25 or less, wherein the powder is advantageous not only in that it has excellent humidity resistance, but also in that it has excellent filling property and excellent flowability when being used as filler for a resin. In addition, provided is a method for producing a sphere-shaped coated magnesium oxide powder, wherein the method comprises allowing a compound of an element forming a double oxide to be present on the surface of magnesium oxide powder, and then fusing the resultant magnesium oxide powder at a high temperature so that the surface of the magnesium oxide powder is coated with the double oxide and the magnesium oxide powder is shaped into sphere. Further, provided are a resin composition comprising the sphere-shaped coated magnesium oxide powder and an electronic device using the resin composition.
摘要翻译： 本发明提供一种具有表面被双氧化物表面涂布的平均形状因子为1.25以下的球状涂覆氧化镁粉末，其特征在于，不仅具有优异的耐湿性，而且具有优异的耐湿性， 优异的填充性和用作树脂填料时的流动性优异。 此外，提供了一种球状涂覆氧化镁粉末的制造方法，其中，所述方法包括使形成双氧化物的元素的化合物存在于氧化镁粉末的表面上，然后将所得的氧化镁 在高温下粉碎，使得氧化镁粉末的表面被双氧化物涂覆，氧化镁粉末成形为球形。 此外，提供了包含球形涂覆的氧化镁粉末和使用该树脂组合物的电子器件的树脂组合物。
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公开(公告)号：US20090053131A1
公开(公告)日：2009-02-26
申请号：US11909505
申请日：2006-03-24
CPC分类号： C30B29/16 , C23C14/081 , C30B11/003 , C30B23/066
摘要： Provided is a MgO single crystal for obtaining a magnesium oxide (MgO) single crystal deposition material which is prevented from splashing during the vapor deposition in, e.g., an electron beam deposition method without reducing the deposition rate, and for obtaining a MgO single crystal substrate which can form thereon, e.g., a superconductor thin film having excellent superconducting properties. A MgO single crystal having a calcium content of 150×10−6 to 1,000×10−6 kg/kg and a silicon content of 10×10−6 kg/kg or less, wherein the MgO single crystal has a variation of 30% or less in terms of a CV value in detected amounts of calcium fragment ions, as analyzed by TOF-SIMS with respect to the polished surface of the MgO single crystal. A MgO single crystal deposition material and a MgO single crystal substrate for forming a thin film obtained from the MgO single crystal.
摘要翻译： 本发明提供一种用于获得氧化镁（MgO）单晶沉积材料的MgO单晶，其在例如电子束沉积方法中在气相沉积期间防止溅射而不降低沉积速率，并且获得MgO单晶衬底 其可以在其上形成，例如具有优异超导性能的超导体薄膜。 具有钙含量为150×10 -6〜1,000×10 -6 kg / kg，硅含量为10×10 -6 kg / kg以下的MgO单晶，其中MgO单晶的变化范围为30％以下， 通过TOF-SIMS相对于MgO单晶的抛光表面分析的钙碎片离子的检测量的CV值。 一种MgO单晶沉积材料和用于形成由MgO单晶获得的薄膜的MgO单晶衬底。
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7.发明授权公开(公告)号：US07544345B2
公开(公告)日：2009-06-09
申请号：US11722921
申请日：2005-12-28
摘要： A magnesium oxide single crystal having controlled crystallinity has a subboundary, and ranges of variation of diffraction line positions, as measured for reciprocal lattice maps with respect to a region surrounded by the same subboundary, with the range of the variation of 1×10−3 to 2×10−2 degree of on Δω coordinates, and with the range of the variation of 4×10−4 to 5×10−3 degree on 2θ coordinates.
摘要翻译： 具有可控结晶度的氧化镁单晶具有子边界，以及相对于由相同子边界包围的区域的互易格子图测量的衍射线位置的变化范围，其变化范围为1×10 -3至2×10 在Deltaomega坐标上为-2度，在2θ坐标上的变化范围为4x10-4至5x10-3度。
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