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    High yield dialysis-free process for producing organosoluble regenerated silk fibroin
    1.
    发明授权
    High yield dialysis-free process for producing organosoluble regenerated silk fibroin 有权
    用于生产有机溶剂的再生丝素蛋白的高产率透析工艺

    公开(公告)号：US08309689B2

    公开(公告)日：2012-11-13

    申请号：US12783818

    申请日：2010-05-20

    Applicant: Jen-Chang Yang ,  Sheng-Yang Lee ,  Chien Chung Chen ,  Yun-Ting Hsu ,  Hong-Da Wu ,  Dian-Yu Ji

    Inventor： Jen-Chang Yang ,  Sheng-Yang Lee ,  Chien Chung Chen ,  Yun-Ting Hsu ,  Hong-Da Wu ,  Dian-Yu Ji

    IPC: C07K1/30

    CPC classification number: C07K14/43586

    Abstract: The invention relates to a simple and high yield process for producing a regenerated silk fibroin which does not need dialysis. Particularly, a process of the invention is characterized in that the silk fibroin is precipitated by applying a shear stress and/or changing the solvent power of the fibroin solution. The process of the invention simplifies the process of producing silk fibroin and greatly shortens the process time to 1 to 2 hours, whereas the conventional dialysis process is complex and needs around 2 to 3 days. In addition to reducing the time needed, the process of the invention can increase productivity of silk fibroin by at least 8%.

    Abstract translation: 本发明涉及用于生产不需要透析的再生丝素蛋白的简单且高产率的方法。 特别地，本发明的方法的特征在于，通过施加剪切应力和/或改变丝心蛋白溶液的溶剂能力使丝素蛋白沉淀。 本发明的方法简化了生产丝素蛋白的过程，大大缩短了1至2小时的处理时间，而常规透析过程复杂，需要2至3天左右。 除了减少所需时间之外，本发明的方法可以将丝素蛋白的生产率提高至少8％。

    Novel amorphous metal salt for facilitating the handling property of portland cements and dental applications thereof
    3.
    发明申请
    Novel amorphous metal salt for facilitating the handling property of portland cements and dental applications thereof 有权
    新型无定形金属盐，用于促进波特兰水泥及其牙科应用的处理性能

    公开(公告)号：US20100139524A1

    公开(公告)日：2010-06-10

    申请号：US12591764

    申请日：2009-12-01

    Applicant: Jeng-Chang Yang ,  Pei-Ying Lee ,  Dain-Yu Ji ,  Nain-Chia Teng ,  Sung-Chih Hsieh ,  Sheng-Yang Lee

    Inventor： Jeng-Chang Yang ,  Pei-Ying Lee ,  Dain-Yu Ji ,  Nain-Chia Teng ,  Sung-Chih Hsieh ,  Sheng-Yang Lee

    IPC: C09K3/00 ,  C07C69/68 ,  C07C303/24

    CPC classification number: C04B24/06 ,  A61K6/0008 ,  A61K6/0215 ,  A61K6/023 ,  A61K6/0606 ,  A61K6/0625 ,  C04B28/04 ,  C04B2111/00198 ,  C04B2111/00836 ,  C04B14/366

    Abstract: A novel amorphous divalent metal ion salt for enhancing the manageability of a Portland cement and its application in dental field are disclosed. Typical formula (I), (II), or (III) of this amorphous metal ion salt are shown as following: M 2 +  A x -  B 2 - x - ( I ) M 2 +  A y 2 -  C ( 4 - y ) 4 2 - ( II ) M 2 +  A z 3 -  D ( 6 - z ) 9 3 - ( III ) wherein, M2+, A−, B−, C−2, D−3, x, y, and z are defined the same as the specification. A novel tooth filling material comprises: a Portland cement, a bone substitute substance, and an amorphous divalent metal ion salt with formula of (I), (II), or (III). In addition, a novel root canal filling material comprises: a Portland cement, a radiopaque substance, and an amorphous divalent metal ion salt with formula of (I), (II), or (III). This amorphous divalent metal ion salt in the filling material of the present invention can improve the sticking together and reduce the setting time, thus offering more convenient in dental applications.

    Abstract translation: 公开了一种用于提高波特兰水泥的可管理性的新型无定形二价金属离子盐及其在牙科领域的应用。 该无定形金属离子盐的典型式（I），（II）或（III）表示如下：M 2 + A X - B 2 - x - （I）M 2 + A y 2 - C（4-y）4 2 - （II）M 2 + A 3 Z 3 - D（6-z）9 3 - （III）其中，M2 +，A-，B-，C-2，D-3 ，x，y和z定义与说明书相同。 一种新型牙齿填充材料包括：波特兰水泥，骨替代物质和具有式（I），（II）或（III）的式的无定形二价金属离子盐。 此外，新颖的根管填充材料包括：波特兰水泥，不透射线的物质和具有式（I），（II）或（III）的式的无定形二价金属离子盐。 本发明的填充材料中的这种无定形二价金属离子盐可以改善粘合在一起并缩短凝固时间，从而在牙齿应用中提供更方便。

    Process for preparing alpha calcium sulfate hemihydrate
    4.
    发明授权
    Process for preparing alpha calcium sulfate hemihydrate 有权
    制备α硫酸钙半水合物的方法

    公开(公告)号：US07700066B1

    公开(公告)日：2010-04-20

    申请号：US12245644

    申请日：2008-10-03

    Applicant: Jen-Chang Yang ,  Hong-Da Wu ,  Nai-Chia Teng ,  Sheng-Yang Lee

    Inventor： Jen-Chang Yang ,  Hong-Da Wu ,  Nai-Chia Teng ,  Sheng-Yang Lee

    IPC: C01B17/96 ,  C01F11/46

    CPC classification number: C01F11/46

    Abstract: The invention provides a process for preparing α-calcium sulfate hemihydrate which comprises the following steps: adding aqueous solutions containing sulfate ions and calcium ions to calcium chloride solution with a range of concentration; reacting the mixture of a) at a range of temperature for an appropriate time; filtering and washing the reaction products of b) with a rising solvent to isolate the solid and liquid phases; and d) collecting and drying the solid phase to obtain α-calcium sulfate hemihydrate with high purity; wherein the relationship between the range of the concentration of calcium chloride (y) and the range of the reaction temperature (x) is shown as the following formula: −0.4x5+7.33x4−52.83x3+187.17x2−328.27x+316

    Abstract translation: 本发明提供了一种制备α-硫酸钙半水合物的方法，包括以下步骤：将含有硫酸根离子和钙离子的水溶液加入到浓度范围的氯化钙溶液中; 使a）的混合物在一定温度范围内反应适当的时间; 过滤和洗涤b）的反应产物与上升溶剂分离固相和液相; 和d）收集和干燥固相以获得高纯度的α-硫酸钙半水合物; 其中氯化钙浓度范围（y）与反应温度（x）的范围之间的关系如下式所示：-0.4x5 + 7.33x4-52.83x3 + 187.17x2-328.27x + 316 < y <1.2x5-22x4 + 158.5x3-561.5x2 + 984.8x-588（2

    Micro-implantable apparatus and method for the stability assessment of a two-stage dental implant
    6.
    发明申请
    Micro-implantable apparatus and method for the stability assessment of a two-stage dental implant 审中-公开
    用于两阶段牙科植入物的稳定性评估的微植入装置和方法

    公开(公告)号：US20050026113A1

    公开(公告)日：2005-02-03

    申请号：US10629574

    申请日：2003-07-30

    Applicant: Jiunn-Liang Chen ,  Sheng-Yang Lee ,  Hao-Ming Huang ,  Kuang-Yu Cheng

    Inventor： Jiunn-Liang Chen ,  Sheng-Yang Lee ,  Hao-Ming Huang ,  Kuang-Yu Cheng

    IPC: A61B5/07 ,  A61C8/00

    CPC classification number: A61C8/00 ,  A61B5/076 ,  A61B5/4547 ,  A61B5/682

    Abstract: A micro-implantable apparatus and method for the stability assessment of a two-stage dental implant during Osseo integration processes, whose detection device is based on a transmission of a pulse wave signal from an upper opening of an implant and a subsequent analysis of the reflection waves that measure the changes in mechanical interlock between the bone and the implant resulted from the wound healing processes happened at the gap between bone-implant interface. The incorporation of RF coils in the detection device provides a mean to transmit and to receive the detection waves, which makes it possible for such a device to be operated in a wireless setting. This device also includes an energy storage, which serve as a temporary power supply unit to effectively eliminate the need for signal wires and power cores, which in turn further increases the applicability and safety of such a device as a passive, implant able apparatus.

    Abstract translation: 一种用于在Osseo积分过程期间两阶段牙科植入物的稳定性评估的微型植入式装置和方法，其检测装置基于来自植入物的上部开口的脉搏波信号的传输和随后的反射分析 用于测量骨骼和植入物之间的机械互锁变化的波形是由于创伤愈合过程发生在骨 - 植入物界面之间的间隙处。 RF线圈在检测装置中的并入提供了发送和接收检测波的平均值，这使得这种装置可以在无线设置中操作。 该装置还包括能量存储器，其用作临时电源单元，以有效地消除对信号线和功率核心的需要，这又进一步增加了诸如无源植入式装置的这种装置的适用性和安全性。

    Amorphous metal salt for facilitating the handling property of portland cements and dental applications thereof
    9.
    发明授权
    Amorphous metal salt for facilitating the handling property of portland cements and dental applications thereof 有权
    无定形金属盐，用于促进波特兰水泥及其牙科应用的处理性能

    公开(公告)号：US08298328B2

    公开(公告)日：2012-10-30

    申请号：US12591764

    申请日：2009-12-01

    Applicant: Jeng-Chang Yang ,  Pei-Ying Lee ,  Dian-Yu Ji ,  Nai-Chia Teng ,  Sung-Chih Hsieh ,  Sheng-Yang Lee

    Inventor： Jeng-Chang Yang ,  Pei-Ying Lee ,  Dian-Yu Ji ,  Nai-Chia Teng ,  Sung-Chih Hsieh ,  Sheng-Yang Lee

    IPC: A61K6/06

    CPC classification number: C04B24/06 ,  A61K6/0008 ,  A61K6/0215 ,  A61K6/023 ,  A61K6/0606 ,  A61K6/0625 ,  C04B28/04 ,  C04B2111/00198 ,  C04B2111/00836 ,  C04B14/366

    Abstract: A novel amorphous divalent metal ion salt for enhancing the manageability of a Portland cement and its application in dental field are disclosed. Typical formula (I), (II), or (III) of this amorphous metal ion salt are shown as following: M 2 + ⁢ A x - ⁢ B 2 - x - ( I ) M 2 + ⁢ A y 2 - ⁢ C ( 4 - y ) 4 2 - ( II ) M 2 + ⁢ A z 3 - ⁢ D ( 6 - z ) 9 3 - ( III ) wherein, M2+, A−, B−, C−2, D−3, x, y, and z are defined the same as the specification. A novel tooth filling material comprises: a Portland cement, a bone substitute substance, and an amorphous divalent metal ion salt with formula of (I), (II), or (III). In addition, a novel root canal filling material comprises: a Portland cement, a radiopaque substance, and an amorphous divalent metal ion salt with formula of (I), (II), or (III). This amorphous divalent metal ion salt in the filling material of the present invention can improve the sticking together and reduce the setting time, thus offering more convenient in dental applications.

    Abstract translation: 公开了一种用于提高波特兰水泥的可管理性的新型无定形二价金属离子盐及其在牙科领域的应用。 该非晶金属离子盐的典型的式（I），（II）或（III）表示如下：M 2 + A x -B 2-x - （I）M 2 + A y 2 - C（4-y）4 2 - （II）M 2 + A z 3 -D（6-z）9 3 - （III）其中，M2 +，A-，B-，C-2，D-3 ，x，y和z定义与说明书相同。 一种新型牙齿填充材料包括：波特兰水泥，骨替代物质和具有式（I），（II）或（III）的式的无定形二价金属离子盐。 此外，新颖的根管填充材料包括：波特兰水泥，不透射线的物质和具有式（I），（II）或（III）的式的无定形二价金属离子盐。 本发明的填充材料中的这种无定形二价金属离子盐可以改善粘合在一起并缩短凝固时间，从而在牙齿应用中提供更方便。

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