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公开(公告)号：US09988759B2
公开(公告)日：2018-06-05
申请号：US13063809
申请日：2009-09-11
申请人： Shinichi Minami , Takashi Enomoto , Tetsuya Masutani , Masahiro Miyahara , Mitsuhiro Usugaya , Rumi Takeuchi , Ikuo Yamamoto , Peter Cheshire Hupfield
发明人： Shinichi Minami , Takashi Enomoto , Tetsuya Masutani , Masahiro Miyahara , Mitsuhiro Usugaya , Rumi Takeuchi , Ikuo Yamamoto , Peter Cheshire Hupfield
IPC分类号： B32B27/04 , D06M15/643 , C08F283/12 , C08F290/06 , D06M15/277 , D06M15/356
CPC分类号： D06M15/6436 , C08F283/122 , C08F290/068 , D06M15/277 , D06M15/3568 , Y10T442/2172 , C08F220/24 , C08F220/68
摘要： A surface treatment agent, which can impart the excellent water- and oil-repellency, soil resistance and feeling to the substrate, is obtained from a fluorine-containing polymer which contains: (A) a monomer which comprises; (A1) a fluorine-containing monomer of the formula: CH2═C(—X)—C(═O)—Y—Z—Rf wherein X is a hydrogen atom, a monovalent organic group, or a halogen atom, Y is —O— or —NH—, Z is a direct bond or a divalent organic group, and Rf is a fluoroalkyl group having 1 to 20 carbon atoms, and (A2) a (meth)acrylate monomer having a cyclic hydrocarbon group, and (B) at least one functional organopolysiloxane selected from the group consisting of a mercapto-functional organopolysiloxane, a vinyl-functional organopolysiloxane, a (meth)acrylamide-functional organopolysiloxane and a (meth)acrylate-functional group.
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2.发明授权公开(公告)号：US07973107B2
公开(公告)日：2011-07-05
申请号：US11913814
申请日：2006-05-08
IPC分类号： C08L83/06
CPC分类号： D06M15/277 , C08F283/122 , C08G77/26 , C08G77/28 , C08G77/442 , D06M15/6436 , D06M15/657 , D06M2200/11 , Y10T428/31663 , Y10T442/60 , C08F220/24 , C08F214/18
摘要： A fluorosilicone reaction product of a mercapto functional organopolysiloxane and a fluorine-containing monomer, and methods of preparing the fluorosilicone are disclosed. The fluorosilicone products are suitable for application to substrates such as textiles, particularly fabrics, to impart oil repellent properties to the textile. The fluorosilicone reaction product is prepared from (A) a fluorine-containing monomer of the formula CH2═C(X)COOYRf, and (B) a mercapto functional organopolysiloxane.
摘要翻译： 公开了巯基官能化有机聚硅氧烷和含氟单体的氟硅酮反应产物及氟硅氧烷的制备方法。 氟硅氧烷产品适用于纺织品，特别是织物等基材，以赋予纺织品防油性能。 氟代硅氧烷反应产物由（A）式CH 2 = C（X）COOYRf的含氟单体和（B）巯基官能的有机聚硅氧烷制备。
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3.发明申请公开(公告)号：US20110124803A1
公开(公告)日：2011-05-26
申请号：US12935344
申请日：2009-03-12
申请人： Ikuo Yamamoto , Tetsuya Masutani , Masahiro Miyahara , Takashi Enomoto , Shinichi Minami , Peter Cheshire Hupfield , Samantha Reed , Avril E. Surgenor
发明人： Ikuo Yamamoto , Tetsuya Masutani , Masahiro Miyahara , Takashi Enomoto , Shinichi Minami , Peter Cheshire Hupfield , Samantha Reed , Avril E. Surgenor
IPC分类号： C09D183/08 , C08L83/08
CPC分类号： C08F283/122 , C08F14/18 , C08F14/22 , C08F214/186 , C08F283/124 , C08J3/03 , C08J2383/10 , D06M15/277 , D06M15/3568 , D06M15/643 , D06M15/6436 , D06M15/657 , D06M2200/11 , D06M2200/12 , D06M2200/50 , C08F2/30
摘要： A fluorosilicone reaction product of a mercapto or vinyl functional organopolysiloxane and a fluorine-containing monomer, and methods of preparing the fluorosilicone are disclosed. The fluorosilicone products are suitable for application to substrates such as textiles, particularly fabrics, to impart oil repellent properties to the textile. The fluorosilicone reaction product is prepared from (A) a fluorine-containing monomer of the formula CH2═C(X)COOYRf, and (B) a mercapto or vinyl functional organopolysiloxane.
摘要翻译： 公开了巯基或乙烯基官能的有机聚硅氧烷和含氟单体的氟硅酮反应产物，以及氟硅氧烷的制备方法。 氟硅氧烷产品适用于纺织品，特别是织物等基材，以赋予纺织品防油性能。 氟硅酮反应产物由（A）式为CH2 = C（X）COOYRf的含氟单体和（B）巯基或乙烯基官能的有机聚硅氧烷制备。
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公开(公告)号：US07776982B2
公开(公告)日：2010-08-17
申请号：US10559765
申请日：2004-06-07
申请人： Ikuo Yamamoto , Tetsuya Masutani
发明人： Ikuo Yamamoto , Tetsuya Masutani
IPC分类号： C08F30/08
CPC分类号： D06M15/3568 , C08L27/12 , C08L83/04 , C09D133/16 , C09D143/04 , D06M15/263 , D06M15/277 , D06M15/643 , D06M15/6433 , D06M15/6436 , D06M15/65 , D06M15/657 , D06M2200/11 , D06M2200/12 , D06M2200/50 , Y10T428/2962 , Y10T428/31663 , C08L83/00 , C08L2666/04
摘要： There is provided a surface treatment agent which comprises a fluoropolymer having repeating units derived from a fluorine-containing monomer of the formula: wherein (a) the fluoropolymer contains a silicon atom, and/or (b) the surface treatment agent contains a fluorine-free polymer which is different from the fluoropolymer and which is a silicon-containing polymer. The surface treatment agent imparts excellent water- and oil-repellency and soil resistance to textiles while retaining the feeling of the textiles, even if the surface treatment agent contains a fluorine-containing acrylate polymer substituted at its α-position by a fluorine atom, a chlorine atom or the like.
摘要翻译： 提供一种表面处理剂，其包含具有衍生自下式的含氟单体的重复单元的含氟聚合物：其中（a）含氟聚合物含有硅原子，和/或（b）表面处理剂含有氟 - 与氟聚合物不同的游离聚合物，它是含硅聚合物。 即使表面处理剂含有在其α-位被氟原子取代的含氟丙烯酸酯聚合物，也能保持纺织品的感觉，表面处理剂赋予纺织品优异的拒水拒油性和耐污性， 氯原子等。
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公开(公告)号：US20100168304A1
公开(公告)日：2010-07-01
申请号：US12523914
申请日：2008-01-18
申请人： Masaru Nagato , Masahiko Maeda , Tetsuya Masutani , Satoshi Onodera , Eiji Kitaura , Motoshi Sasaki , Peter Cheshire Hupfield
发明人： Masaru Nagato , Masahiko Maeda , Tetsuya Masutani , Satoshi Onodera , Eiji Kitaura , Motoshi Sasaki , Peter Cheshire Hupfield
IPC分类号： C08K5/5415
CPC分类号： C09D7/1233 , C08G77/24 , C08K5/5406 , C08L61/20 , C08L83/02 , C09D7/63 , C09D167/00 , C08L83/00 , C08L2666/02
摘要： There is provided a polyester coating composition having excellent action of preventing deposition of outdoor stain and stain caused by rainfall, being capable of extending a period of time (pot life) from the mixing to the coating, and comprising (A) a polyester resin, (B) one or more of fluorine-containing organosilicon compounds having a fluorine content of 5 to 30% by mass, (C) one or more of aliphatic hydrocarbon compounds having hydroxyl group and 1 to 10 carbon atoms, in which a part of hydrogen atoms bonded to carbon atom may be substituted by fluorine atoms and/or one or more of alkoxy compounds having 2 to 10 carbon atoms, in which a part of hydrogen atoms bonded to carbon atom may be substituted by fluorine atoms, and (D) an organic solvent.
摘要翻译： 提供一种具有防止室外污渍沉积和由降雨引起的污渍的能够延长从混合到涂层的时间（适用期）的聚酯涂料组合物，并且包含（A）聚酯树脂， （B）一种或多种氟含量为5〜30质量％的含氟有机硅化合物，（C）一种或多种具有羟基和1至10个碳原子的脂族烃化合物，其中一部分氢 与碳原子键合的原子可以被氟原子和/或一个或多个具有2-10个碳原子的烷氧基化合物取代，其中一部分与碳原子键合的氢原子可以被氟原子取代，和（D） 有机溶剂。
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公开(公告)号：US20070066780A1
公开(公告)日：2007-03-22
申请号：US10559810
申请日：2004-06-07
IPC分类号： C08F16/24
CPC分类号： C08F220/24 , C04B41/4842
摘要： A fluoropolymer for masonry treatment produced from (A) a fluoromonomer which has been substituted in the α-position by a X group and is represented by the formula (I): and (B) a monomer having a functional group reactive with active hydrogen. It imparts excellent water- and oil-repellency and unsusceptibility to fouling to masonries.
摘要翻译： （A）通过X基团在α位被X基团取代并由式（I）表示的（A）含氟单体制备的用于石工处理的含氟聚合物：和（B）具有与活性氢反应的官能团的单体。 它赋予了优异的拒水拒油性和对砖石结垢的不可接受性。
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公开(公告)号：US20060054053A1
公开(公告)日：2006-03-16
申请号：US10541451
申请日：2004-01-22
CPC分类号： C09D183/10 , C08G65/007 , C09D5/00
摘要： There is provided a coating composition which comprises (A) a synthetic resin having functional group, (B) a stain-proofing component which is a liquid polydialkylsiloxane having functional group or a liquid fluoropolyether having functional group and (C) a curing agent, and the composition is excellent in a stain-proofing property, particularly removability of oily stain, thereby enabling scribbling to be easily wiped off, and is suitable for outdoor coating being excellent in weather resistance and adhesion.
摘要翻译： 提供一种涂料组合物，其包含（A）具有官能团的合成树脂，（B）具有官能团的液体聚二烷基硅氧烷或具有官能团的液体氟聚醚的防污组分和（C）固化剂，和 该组合物的防污性，特别是油性污渍的可除去性优异，从而可以容易地擦去涂布，适用于耐候性和粘合性优异的室外涂布。
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公开(公告)号：US06673948B2
公开(公告)日：2004-01-06
申请号：US10221193
申请日：2002-09-23
申请人： Tetsuya Masutani , Akinori Yamamoto
发明人： Tetsuya Masutani , Akinori Yamamoto
IPC分类号： C07D30506
CPC分类号： C07D305/06
摘要： A process for preparing compounds of formula (I) comprising radical addition of RfI to 3-(allyloxy)methyl-3-alkyloxetane (1) wherein R is C1-3 alkyl and Rf is C1-18 linear or branched fluoroalkyl. The compounds of formula (I) are useful as intermediates for preparing various fluorine-containing functional materials.
摘要翻译： 制备式（I）化合物的方法，其包括向3-（烯丙氧基）甲基-3-烷基氧杂环丁烷（1）中自由基加成，其中R是C 1-3烷基，R f是C 1-18直链或支链氟代烷基。 式（I）可用作制备各种含氟官能材料的中间体。
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9.发明授权Surface treatment composition, process for producing the same, and surface-treated article 有权表面处理组合物，其制备方法和表面处理制品公开(公告)号：US09523004B2
公开(公告)日：2016-12-20
申请号：US13508870
申请日：2010-11-10
申请人： Gregory Hervieu , Pierre-Jean Calba , Don Lee Kleyer , Masayuki Hayashi , Peter Cheshire Hupfield , Tomohiro Yoshida , Yasuo Itami , Masahiko Maeda , Tetsuya Masutani
发明人： Gregory Hervieu , Pierre-Jean Calba , Don Lee Kleyer , Masayuki Hayashi , Peter Cheshire Hupfield , Tomohiro Yoshida , Yasuo Itami , Masahiko Maeda , Tetsuya Masutani
CPC分类号： C09D5/006 , C09D5/1675 , Y10T428/31663
摘要： A surface treatment composition comprising (i) an organosilicon compound having an alkoxysilane functional group at the end of a fluorocontaining polyether chain and (ii) fluorocontaining polyether compound s, wherein a content of the fluorocontaining polyether compounds in the surface treatment composition is less than 25 mol % based on the surface treatment composition.
摘要翻译： 表面处理组合物，其包含（i）在含氟聚醚链末端具有烷氧基硅烷官能团的有机硅化合物和（ii）含氟聚醚化合物，其中表面处理组合物中含氟聚醚化合物的含量小于25 mol％，基于表面处理组成。
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公开(公告)号：US09175177B2
公开(公告)日：2015-11-03
申请号：US12523914
申请日：2008-01-18
申请人： Masaru Nagato , Masahiko Maeda , Tetsuya Masutani , Satoshi Onodera , Eiji Kitaura , Motoshi Sasaki , Peter Cheshire Hupfield
发明人： Masaru Nagato , Masahiko Maeda , Tetsuya Masutani , Satoshi Onodera , Eiji Kitaura , Motoshi Sasaki , Peter Cheshire Hupfield
CPC分类号： C09D7/1233 , C08G77/24 , C08K5/5406 , C08L61/20 , C08L83/02 , C09D7/63 , C09D167/00 , C08L83/00 , C08L2666/02
摘要： There is provided a polyester coating composition having excellent action of preventing deposition of outdoor stain and stain caused by rainfall, being capable of extending a period of time (pot life) from the mixing to the coating, and comprising (A) a polyester resin, (B) one or more of fluorine-containing organosilicon compounds having a fluorine content of 5 to 30% by mass, (C) one or more of aliphatic hydrocarbon compounds having hydroxyl group and 1 to 10 carbon atoms, in which a part of hydrogen atoms bonded to carbon atom may be substituted by fluorine atoms and/or one or more of alkoxy compounds having 2 to 10 carbon atoms, in which a part of hydrogen atoms bonded to carbon atom may be substituted by fluorine atoms, and (D) an organic solvent.
摘要翻译： 提供一种具有防止室外污渍沉积和由降雨引起的污渍的能够延长从混合到涂层的时间（适用期）的聚酯涂料组合物，并且包含（A）聚酯树脂， （B）一种或多种氟含量为5〜30质量％的含氟有机硅化合物，（C）一种或多种具有羟基和1至10个碳原子的脂族烃化合物，其中一部分氢 与碳原子键合的原子可以被氟原子和/或一个或多个具有2-10个碳原子的烷氧基化合物取代，其中一部分与碳原子键合的氢原子可以被氟原子取代，和（D） 有机溶剂。
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