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    Methods of fabricating plasticized, antiplasticized and crystalline conducting polymers and precursors thereof
    2.
    发明授权
    Methods of fabricating plasticized, antiplasticized and crystalline conducting polymers and precursors thereof 有权
    制造增塑的，抗增塑的和结晶的导电聚合物及其前体的方法

    公开(公告)号：US07902323B1

    公开(公告)日：2011-03-08

    申请号：US09346353

    申请日：1999-07-02

    申请人： Marie Angelopoulos ,  Yun-Hsin Liao ,  Ravi F. Saraf

    发明人： Marie Angelopoulos ,  Yun-Hsin Liao ,  Ravi F. Saraf

    IPC分类号： C08J3/11 ,  C08J3/18 ,  C08G73/00 ,  H01B1/12

    CPC分类号： H01B1/128 ,  C08G61/12

    摘要： Methods of forming materials containing precursors to electrically conductive polymers and electrically conductive polymers are described which have a high degree of crystallinity. The high degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. High levels of electrical conductivity are achieved in in the electrically conductive materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriented film which has isotropic electrical conductivity. In the preferred embodiment, additives are added to a solution containing a solvent and the precursor or electrically conductive polymer. The additives are preferably plasticizer of diluents. As the solvent is removed the material dries and contains a higher degree of crystallinity than in the absence of the additive.

    摘要翻译： 描述了形成具有高结晶度的导电聚合物和导电聚合物前体的材料的方法。 通过在允许它们彼此结合以形成结晶状态的聚合物分子提供高度迁移率的条件下制备材料来实现高结晶度。 在导电材料中实现高水平的导电性而不使材料拉伸定向。 与具有各向同性电导率的拉伸取向膜相比，增强的导电性是各向同性的。 在优选的实施方案中，将添加剂加入到含有溶剂和前体或导电聚合物的溶液中。 添加剂优选稀释剂的增塑剂。 当除去溶剂时，与没有添加剂相比，材料干燥并含有更高的结晶度。

    Polycrystalline conducting polymers and precursors thereof having adjustable morphology and properties
    3.
    发明授权
    Polycrystalline conducting polymers and precursors thereof having adjustable morphology and properties 有权
    具有可调节形态和性质的多晶导电聚合物及其前体

    公开(公告)号：US06210606B1

    公开(公告)日：2001-04-03

    申请号：US09268527

    申请日：1999-03-12

    申请人： Marie Angelopoulos ,  Yun-Hsin Liao ,  Ravi F. Saraf

    发明人： Marie Angelopoulos ,  Yun-Hsin Liao ,  Ravi F. Saraf

    IPC分类号： H01B112

    CPC分类号： C08G61/12 ,  H01B1/128 ,  Y10T428/249958

    摘要： Polycrystalline materials containing crystallites of precursors to electrically conductive polymers and electrically conductive polymers are described which have an adjustable high degree of crystallinity. The intersticial regions between the crystallites contains amorphous material containing precursors to electrically conductive polymers and/or electrically conductive polymers. The degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. This is preferable achieved by including additives, such as plasticizers and diluents, to the solution from which the polycrystalline material is formed. The morphology of the polycrystalline material is adjustable to modify the properties of the material such as the degree of crystallinity, crystal grain size, glass transition temperature, thermal coefficient of expansion and degree of electrical conductivity. High levels of electrical conductivity are achieved in the electrically conductive polycrystalline materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriented film which has isotropic electrical conductivity.

    摘要翻译： 描述了具有可调高结晶度的导电聚合物和导电聚合物的前体微晶的多晶材料。 微晶之间的区域包含含有导电聚合物和/或导电聚合物的前体的无定形材料。 通过在允许它们彼此结合以形成结晶状态的聚合物分子提供高度迁移率的条件下制备材料来实现结晶度。 优选通过将诸如增塑剂和稀释剂的添加剂添加到形成多晶材料的溶液中来实现。 可以调节多晶材料的形态，以改变材料的性质，例如结晶度，晶粒尺寸，玻璃化转变温度，热膨胀系数和电导率。 在导电多晶材料中实现高水平的导电性而不使材料拉伸取向。 与具有各向同性电导率的拉伸取向膜相比，增强的导电性是各向同性的。

    Cross-linked electrically conductive polymers, precursors thereof
    4.
    发明授权
    Cross-linked electrically conductive polymers, precursors thereof 失效
    交联导电聚合物及其前体

    公开(公告)号：US06193909B1

    公开(公告)日：2001-02-27

    申请号：US08595853

    申请日：1996-02-02

    申请人： Marie Angelopoulos ,  Jeffrey D. Gelorme ,  Yun Hsin Liao ,  Jane M. Shaw

    发明人： Marie Angelopoulos ,  Jeffrey D. Gelorme ,  Yun Hsin Liao ,  Jane M. Shaw

    IPC分类号： H01B112

    CPC分类号： C08G73/1071 ,  H01B1/128

    摘要： Cross-linked electrically conductive polymers, in particular electrically conductive, polyaniline are described. Dopants and substituents having pendant cross-linkable functionality are used which form a cross-linked conducting polymer network. The cross-linking functionality can be hydrogen-bonding as well as chemically polymerizable or cross-linkable. A conjugated path between chains can also be incorporated. The resulting cross-linked conducting polymers have enhanced thermal and environmental stability. The dopant cannot readily be washed out with solvents or diffuse out upon exposure to heat. In addition, the cross-linked polymers have enhanced electrical conductivity.

    摘要翻译： 描述了交联的导电聚合物，特别是导电的聚苯胺。 使用具有侧链可交联官能团的掺杂剂和取代基，其形成交联的导电聚合物网络。 交联官能团可以是氢键合以及化学上可聚合的或可交联的。 还可以并入链之间的共轭路径。 所得的交联导电聚合物具有增强的热和环境稳定性。 掺杂剂不容易用溶剂洗涤或在暴露于热量时扩散出来。 此外，交联聚合物具有增强的导电性。

    Foamed elastomers for wafer probing applications and interposer connectors
    5.
    发明授权
    Foamed elastomers for wafer probing applications and interposer connectors 失效
    用于晶圆探测应用和插入式连接器的发泡弹性体

    公开(公告)号：US6054651A

    公开(公告)日：2000-04-25

    申请号：US752469

    申请日：1996-11-19

    申请人： Keith Edward Fogel ,  James Lupton Hedrick ,  Paul Alfred Lauro ,  Yun-Hsin Liao ,  Da-Yuan Shih

    发明人： Keith Edward Fogel ,  James Lupton Hedrick ,  Paul Alfred Lauro ,  Yun-Hsin Liao ,  Da-Yuan Shih

    IPC分类号： H01B3/46 ,  H01B7/00

    CPC分类号： H01B3/46

    摘要： The present invention is directed to a new foamed elastomer composition including elastomer, hollow fillers, and reinforced fillers for supporting the conducting wires in the test probes for wafer level testing and burn in and interposer connector applications. The thermally stable elastomer resin is mixed with hollow fillers and reinforced fillers before filling into the probe or connector mold with an array of elongated conducting wires, then is crosslinked by a crosslinking agent and a catalyst. The use of compressible hollow fillers to foam the elastomer has been successful to enhance the compliance and resilience, and to reduce the thermal expansion, density, and dielectric constant of the elastomer.

    摘要翻译： 本发明涉及一种新的泡沫弹性体组合物，其包括弹性体，中空填料和增强填料，用于在用于晶片级测试和烧录和插入件连接器应用的测试探针中支撑导线。 将热稳定的弹性体树脂与中空填料和增强填料混合，然后用细长的导线阵列填充到探针或连接器模具中，然后通过交联剂和催化剂进行交联。 使用可压缩中空填料来弹性弹性体已经成功地提高了弹性体的顺应性和弹性，并降低了弹性体的热膨胀，密度和介电常数。

    Methods of fabricating plasticized, antiplasticized and crystalline conducting polymers and precursors thereof
    7.
    发明申请
    Methods of fabricating plasticized, antiplasticized and crystalline conducting polymers and precursors thereof 有权
    制造增塑的，抗增塑的和结晶的导电聚合物及其前体的方法

    公开(公告)号：US20090304908A1

    公开(公告)日：2009-12-10

    申请号：US12583030

    申请日：2009-08-12

    申请人： Marie Angelopoulos ,  Yun-Hsin Liao ,  Ravi F. Saraf

    发明人： Marie Angelopoulos ,  Yun-Hsin Liao ,  Ravi F. Saraf

    IPC分类号： B05D5/12 ,  H01B1/12

    CPC分类号： H01B1/128

    摘要： Methods of forming materials containing precursors to electrically conductive polymers and electrically conductive polymers are described which have a high degree of crystallinity. The high degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. High levels of electrical conductivity are achieved in in the electrically conductive materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriented film which has isotropic electrical conductivity. In the preferred embodiment, additives are added to a solution containing a solvent and the precursor or electrically conductive polymer. The additives are preferably plasticizer of diluents. As the solvent is removed the material dries and contains a higher degree of crystallinity than in the absence of the additive.

    摘要翻译： 描述了形成具有高结晶度的导电聚合物和导电聚合物前体的材料的方法。 通过在允许它们彼此结合以形成结晶状态的聚合物分子提供高度迁移率的条件下制备材料来实现高结晶度。 在导电材料中实现高水平的导电性而不使材料拉伸定向。 与具有各向同性电导率的拉伸取向膜相比，增强的导电性是各向同性的。 在优选的实施方案中，将添加剂加入到含有溶剂和前体或导电聚合物的溶液中。 添加剂优选稀释剂的增塑剂。 当除去溶剂时，与没有添加剂相比，材料干燥并含有更高的结晶度。

    POLYCRYSTALLINE CONDUCTING POLYMERS AND PRECURSORS THEREOF HAVING ADJUSTABLE MORPHOLOGY AND PROPERTIES
    8.
    发明申请
    POLYCRYSTALLINE CONDUCTING POLYMERS AND PRECURSORS THEREOF HAVING ADJUSTABLE MORPHOLOGY AND PROPERTIES 审中-公开
    具有可调节形态和性质的多晶硅导电聚合物及其前驱体

    公开(公告)号：US20090032775A1

    公开(公告)日：2009-02-05

    申请号：US12137646

    申请日：2008-06-12

    申请人： Marie Angelopoulos ,  Yun-Hsin Liao ,  Ravi F. Saraf

    发明人： Marie Angelopoulos ,  Yun-Hsin Liao ,  Ravi F. Saraf

    IPC分类号： H01B1/12 ,  C08K5/09 ,  C08K5/10 ,  C08K5/5317

    CPC分类号： C08G61/12 ,  H01B1/128 ,  Y10T428/249958

    摘要： Polycrystalline materials containing crystallies of precursors to electrically conductive polymers and electrically conductive polymers are described which have an adjustable high degree of crystallinity. The intersticial regions between the crystallites contains amorphous material containing precursors to electrically conductive polymers and/or electrically conductive polymers. The degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. This is preferable achieved by including additives, such as plasticizers and diluents, to the solution from which the polycrystalline material is formed. The morphology of the polycrystalline material is adjustable to modify the properties of the material such as the degree of crystallinity, crystal grain size, glass transition temperature, thermal coefficient of expansion and degree of electrical conductivity. High levels of electrical conductivity are achieved in in the electrically conductive polycrystalline materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriented film which has isotropic electrical conductivity.

    摘要翻译： 描述了具有可调节高结晶度的导电聚合物和导电聚合物的前体结晶的多晶材料。 微晶之间的区域包含含有导电聚合物和/或导电聚合物的前体的无定形材料。 通过在允许它们彼此结合以形成结晶状态的聚合物分子提供高度迁移率的条件下制备材料来实现结晶度。 优选通过将诸如增塑剂和稀释剂的添加剂添加到形成多晶材料的溶液中来实现。 可以调节多晶材料的形态，以改变材料的性质，例如结晶度，晶粒尺寸，玻璃化转变温度，热膨胀系数和电导率。 在导电多晶材料中实现高水平的导电性，而不拉伸定向该材料。 与具有各向同性电导率的拉伸取向膜相比，增强的导电性是各向同性的。