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    METHOD OF MAKING ALPHA, OMEGA-DIIODOPERFLUOROALKANES
    1.
    发明申请
    METHOD OF MAKING ALPHA, OMEGA-DIIODOPERFLUOROALKANES 有权
    制备ALPHA，OMEGA-DIIODOPERFLUOROKANES的方法

    公开(公告)号：US20150259270A1

    公开(公告)日：2015-09-17

    申请号：US14434981

    申请日：2013-10-09

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Steven J. Martin ,  Luke T. Dressel ,  Aaron E. Hutt ,  Eric A. Schotz ,  Terence D. Spawn ,  Miguel A. Guerra ,  Tatsuo Fukushi ,  Jeremy A. Miller ,  Christopher M. Geise ,  James A. McDonell

    IPC: C07C45/58 ,  C07C17/26

    CPC classification number: C07C45/58 ,  C07C17/00 ,  C07C17/093 ,  C07C17/26 ,  C07C19/16

    Abstract: A method of making α,ω-diiodoperfluoroalkanes includes combining: diatomic iodine, at least one perfluoroalkylene oxide represented by the formula wherein Rf represents a perfluoroalkyl group; and at least one of: a) a first metallic compound comprising nickel, and a second metallic compound comprising molybdenum that is compositionally different from the first metallic compound; or b) a metallic alloy comprising from 50 to 70 percent by weight of nickel and from 20 to 40 percent by weight of molybdenum, based on the total weight of the metallic alloy, thereby producing at least one product represented by the formula I(CF2)nI, wherein n independently represents an integer in the range of from 1 to 11. The total weight of the at least one product wherein n is 3 or greater exceeds the total weight of the at least one product wherein n is 1 or 2 by a factor of at least 4.

    Abstract translation: 制备α，ω-二碘全氟烷烃的方法包括组合：双原子碘，至少一种由下式表示的全氟氧化烯，其中Rf表示全氟烷基; 和至少一种：a）包含镍的第一金属化合物和包含与第一金属化合物成分不同的钼的第二金属化合物; 或b）金属合金，其包含基于金属合金的总重量的50-70重量％的镍和20至40重量％的钼，由此产生至少一种由式I表示的产物（CF 2 ）nI，其中n独立地表示1至11范围内的整数。其中n为3或更大的至少一种产物的总重量超过至少一种产物的总重量，其中n为1或2，其中n为1或2， 至少4的因素。

    Methods of Direct Addition of (Meth) Acrylic Acid to Bio-based oils
    2.
    发明申请
    Methods of Direct Addition of (Meth) Acrylic Acid to Bio-based oils 有权
    （甲基）丙烯酸直接添加到生物油中的方法

    公开(公告)号：US20160053200A1

    公开(公告)日：2016-02-25

    申请号：US14778644

    申请日：2014-05-01

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Joshua L. Colby ,  Lianzhou Chen ,  Kwame Owusu-Adom ,  Aaron E. Hutt

    IPC: C11C3/00 ,  C07C67/04

    CPC classification number: C07C67/04 ,  C07C67/31 ,  C07C69/54 ,  C11C3/00 ,  C07C69/73

    Abstract: (Meth)acrylates are prepared in a single-step method from a mixture of (meth)acrylic acid and at least one biobased oil and/or its derivative(s), including at least one unsaturation. The (meth)acrylates are made by directly adding the (meth)acrylic acid to the biobased oil by reacting in the presence of an acid catalyst, including an inorganic or organic acid having at least one oxygen atom present thereon and which possesses at least one acid functionality having an ionization constant in water which is not greater than 3.

    Abstract translation: （甲基）丙烯酸酯由（甲基）丙烯酸和至少一种生物基油和/或其衍生物的混合物（包括至少一种不饱和键）以单步法制备。 （甲基）丙烯酸酯通过在生物基油中直接加入（甲基）丙烯酸而制备，在酸催化剂存在下反应，所述酸催化剂包括其中存在至少一个氧原子的无机或有机酸，并且具有至少一个 在水中电离常数不大于3的酸官能团。

    METHOD FOR PREPARING (METH)ACRYLATES OF BIOBASED ALCOHOLS AND POLYMERS THEREOF
    4.
    发明申请
    METHOD FOR PREPARING (METH)ACRYLATES OF BIOBASED ALCOHOLS AND POLYMERS THEREOF 有权
    制备生物脂肪酸（甲基）丙烯酸酯及其聚合物的方法

    公开(公告)号：US20160009628A1

    公开(公告)日：2016-01-14

    申请号：US14769850

    申请日：2014-03-13

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Joshua L. Colby ,  Aaron E. Hutt ,  Terence D. Spawn ,  Jason D. Clapper ,  Tabitha A. Clem

    IPC: C07C67/04 ,  C07C1/24

    CPC classification number: C07C67/04 ,  C07C1/24 ,  C07C2531/08 ,  C07C2531/10 ,  C08F220/18 ,  C09J133/08 ,  C07C69/54 ,  C07C11/02 ,  C08F2220/1825 ,  C08F220/06

    Abstract: Polymers, particularly those used in pressure-sensitive adhesives, are prepared from a mixture of structural isomers of a secondary alkyl (meth)acrylate monomer. The mixture is made by dehydrating a biobased C2-C22 alcohol with a first acid catalyst using a continuous process to form a mixture of olefins, and reacting (meth)acrylic acid with at least some of the mixture of olefins in the presence of a second acid catalyst. The adhesives are characterized by exhibiting an overall balance of adhesive and cohesive characteristics, and containing biobased material.

    Abstract translation: 聚合物，特别是用于压敏粘合剂的聚合物，由（甲基）丙烯酸仲烷基酯单体的结构异构体的混合物制备。 该混合物通过使用连续方法用第一种酸催化剂使生物基C2-C22醇脱水来形成烯烃的混合物，并在第二种存在下使（甲基）丙烯酸与至少一些烯烃混合物反应 酸催化剂。 粘合剂的特征在于显示粘合剂和内聚特性的总体平衡，并且包含生物基材料。

    Methods of direct addition of (meth) acrylic acid to bio-based oils
    6.
    发明授权
    Methods of direct addition of (meth) acrylic acid to bio-based oils 有权
    将（甲基）丙烯酸直接加入到生物基油中的方法

    公开(公告)号：US09533935B2

    公开(公告)日：2017-01-03

    申请号：US14778644

    申请日：2014-05-01

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Joshua L. Colby ,  Lianzhou Chen ,  Kwame Owusu-Adom ,  Aaron E. Hutt

    IPC: C07C67/04 ,  C07C69/54 ,  C07C67/31 ,  C11C3/00

    CPC classification number: C07C67/04 ,  C07C67/31 ,  C07C69/54 ,  C11C3/00 ,  C07C69/73

    Abstract: (Meth)acrylates are prepared in a single-step method from a mixture of (meth)acrylic acid and at least one biobased oil and/or its derivative(s), including at least one unsaturation. The (meth)acrylates are made by directly adding the (meth)acrylic acid to the biobased oil by reacting in the presence of an acid catalyst, including an inorganic or organic acid having at least one oxygen atom present thereon and which possesses at least one acid functionality having an ionization constant in water which is not greater than 3.

    Abstract translation: （甲基）丙烯酸酯由（甲基）丙烯酸和至少一种生物基油和/或其衍生物的混合物（包括至少一种不饱和键）以单步法制备。 （甲基）丙烯酸酯通过在生物基油中直接加入（甲基）丙烯酸而制备，在酸催化剂存在下反应，所述酸催化剂包括其中存在至少一个氧原子的无机或有机酸，并且具有至少一个 在水中电离常数不大于3的酸官能团。

    Method of making alpha, omega-diiodoperfluoroalkanes
    8.
    发明授权
    Method of making alpha, omega-diiodoperfluoroalkanes 有权
    制备α，ω-二碘全氟烷烃的方法

    公开(公告)号：US09212119B2

    公开(公告)日：2015-12-15

    申请号：US14434981

    申请日：2013-10-09

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Steven J. Martin ,  Luke T. Dressel ,  Aaron E. Hutt ,  Eric A. Schotz ,  Terence D. Spawn ,  Miguel A. Guerra ,  Tatsuo Fukushi ,  Jeremy A. Miller ,  Christopher M. Geise ,  James A. McDonell

    IPC: C07C21/18 ,  C07C45/58 ,  C07C17/26 ,  C07C17/093

    CPC classification number: C07C45/58 ,  C07C17/00 ,  C07C17/093 ,  C07C17/26 ,  C07C19/16

    Abstract: A method of making α,ω-diiodoperfluoroalkanes includes combining: diatomic iodine, at least one perfluoroalkylene oxide represented by the formula wherein Rf represents a perfluoroalkyl group; and at least one of: a) a first metallic compound comprising nickel, and a second metallic compound comprising molybdenum that is compositionally different from the first metallic compound; or b) a metallic alloy comprising from 50 to 70 percent by weight of nickel and from 20 to 40 percent by weight of molybdenum, based on the total weight of the metallic alloy, thereby producing at least one product represented by the formula I(CF2)nI, wherein n independently represents an integer in the range of from 1 to 11. The total weight of the at least one product wherein n is 3 or greater exceeds the total weight of the at least one product wherein n is 1 or 2 by a factor of at least 4.

    Abstract translation: 制备α，ω-二碘全氟烷烃的方法包括组合：双原子碘，至少一种由下式表示的全氟氧化烯，其中Rf表示全氟烷基; 和至少一种：a）包含镍的第一金属化合物和包含与第一金属化合物成分不同的钼的第二金属化合物; 或b）金属合金，其包含基于金属合金的总重量的50-70重量％的镍和20至40重量％的钼，由此产生至少一种由式I表示的产物（CF 2 ）nI，其中n独立地表示1至11范围内的整数。其中n为3或更大的至少一种产物的总重量超过至少一种产物的总重量，其中n为1或2，其中n为1或2， 至少4的因素。

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