公开(公告)号：US20160168702A1

公开(公告)日：2016-06-16

申请号：US15051761

申请日：2016-02-24

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Christopher S. Lyons ,  Kent T. Engle ,  Steven R. Vanhoose ,  Terence D. Spawn ,  Joseph M. Pieper ,  Edward J. Anderson ,  Walter Stoss

IPC: C23C16/455 ,  B05D1/00 ,  B01D3/10 ,  C23C16/50

CPC classification number: C23C16/45561 ,  B01D3/10 ,  B05D1/60 ,  B05D2252/02 ,  C23C14/12 ,  C23C14/228 ,  C23C14/24 ,  C23C14/544 ,  C23C14/562 ,  C23C14/58 ,  C23C14/5806 ,  C23C14/582 ,  C23C16/50

Abstract: A system for processing vapor. The system includes a vapor source for producing a vapor and an outlet conduit coupled to the vapor source for carrying the vapor from the vapor source. Downstream of the vapor source the outlet conduit separates into a vapor bypass conduit and a vapor feed conduit. The system further includes a first vapor control valve disposed in the bypass conduit, a second vapor control valve disposed in the feed conduit, a first vacuum chamber connected to the bypass conduit, and a second vacuum chamber connected to the feed conduit.

Abstract translation: 蒸汽处理系统 该系统包括用于产生蒸汽的蒸汽源和与蒸汽源耦合的出口导管，用于承载来自蒸气源的蒸气。 在蒸汽源的下游，出口导管分离成蒸气旁路管道和蒸气供给导管。 该系统还包括设置在旁路管道中的第一蒸汽控制阀，设置在进料管道中的第二蒸汽控制阀，连接到旁路管道的第一真空室和连接到进料管道的第二真空室。

公开(公告)号：US20140178567A1

公开(公告)日：2014-06-26

申请号：US14232671

申请日：2012-08-01

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Christopher S. Lyons ,  Kent T. Engle ,  Steven R. Vanhoose ,  Terence D. Spawn ,  Joseph M. Pieper ,  Edward J. Anderson ,  Walter Stoss

IPC: B05D1/00

CPC classification number: C23C16/45561 ,  B01D3/10 ,  B05D1/60 ,  B05D2252/02 ,  C23C14/12 ,  C23C14/228 ,  C23C14/24 ,  C23C14/544 ,  C23C14/562 ,  C23C14/58 ,  C23C14/5806 ,  C23C14/582 ,  C23C16/50

Abstract: A system for processing vapor. The system includes a vapor source for producing a vapor and an outlet conduit coupled to the vapor source for carrying the vapor from the vapor source. Downstream of the vapor source the outlet conduit separates into a vapor bypass conduit and a vapor feed conduit. The system further includes a first vapor control valve disposed in the bypass conduit, a second vapor control valve disposed in the feed conduit, a first vacuum chamber connected fluidically coupled to the bypass conduit, and a second vacuum chamber connected fluidically coupled to the feed conduit.

Abstract translation: 蒸汽处理系统 该系统包括用于产生蒸汽的蒸汽源和与蒸汽源耦合的出口导管，用于承载来自蒸气源的蒸气。 在蒸汽源的下游，出口导管分离成蒸气旁路管道和蒸气供给导管。 该系统还包括设置在旁路管道中的第一蒸汽控制阀，设置在进料管道中的第二蒸汽控制阀，流体耦合到旁路管道的第一真空室，以及连接到进料管道 。

公开(公告)号：US09604902B2

公开(公告)日：2017-03-28

申请号：US14769875

申请日：2014-03-04

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Joshua L. Colby ,  Tabitha A. Clem ,  Terence D. Spawn ,  Aaron E. Hutt ,  Wade T. Teply

IPC: C07C67/08 ,  C09J133/08 ,  C08F220/18 ,  C07C57/02

CPC classification number: C07C67/08 ,  C07C57/02 ,  C08F220/18 ,  C09J133/08 ,  Y02P20/582 ,  C07C69/54 ,  C08F2220/1858 ,  C08F220/06

Abstract: A method of making 2-octyl acrylate comprising reacting 2-octanol with acrylic acid in the presence of an acid catalyst and added water is described. The 2-octanol may be derived from renewable resources, such as castor oil. The method is efficient and provides selectivity for 2-octyl acrylate.

公开(公告)号：US20160009628A1

公开(公告)日：2016-01-14

申请号：US14769850

申请日：2014-03-13

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Joshua L. Colby ,  Aaron E. Hutt ,  Terence D. Spawn ,  Jason D. Clapper ,  Tabitha A. Clem

IPC: C07C67/04 ,  C07C1/24

CPC classification number: C07C67/04 ,  C07C1/24 ,  C07C2531/08 ,  C07C2531/10 ,  C08F220/18 ,  C09J133/08 ,  C07C69/54 ,  C07C11/02 ,  C08F2220/1825 ,  C08F220/06

Abstract: Polymers, particularly those used in pressure-sensitive adhesives, are prepared from a mixture of structural isomers of a secondary alkyl (meth)acrylate monomer. The mixture is made by dehydrating a biobased C2-C22 alcohol with a first acid catalyst using a continuous process to form a mixture of olefins, and reacting (meth)acrylic acid with at least some of the mixture of olefins in the presence of a second acid catalyst. The adhesives are characterized by exhibiting an overall balance of adhesive and cohesive characteristics, and containing biobased material.

Abstract translation: 聚合物，特别是用于压敏粘合剂的聚合物，由（甲基）丙烯酸仲烷基酯单体的结构异构体的混合物制备。 该混合物通过使用连续方法用第一种酸催化剂使生物基C2-C22醇脱水来形成烯烃的混合物，并在第二种存在下使（甲基）丙烯酸与至少一些烯烃混合物反应 酸催化剂。 粘合剂的特征在于显示粘合剂和内聚特性的总体平衡，并且包含生物基材料。

公开(公告)号：US20150259270A1

公开(公告)日：2015-09-17

申请号：US14434981

申请日：2013-10-09

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Steven J. Martin ,  Luke T. Dressel ,  Aaron E. Hutt ,  Eric A. Schotz ,  Terence D. Spawn ,  Miguel A. Guerra ,  Tatsuo Fukushi ,  Jeremy A. Miller ,  Christopher M. Geise ,  James A. McDonell

IPC: C07C45/58 ,  C07C17/26

CPC classification number: C07C45/58 ,  C07C17/00 ,  C07C17/093 ,  C07C17/26 ,  C07C19/16

Abstract: A method of making α,ω-diiodoperfluoroalkanes includes combining: diatomic iodine, at least one perfluoroalkylene oxide represented by the formula wherein Rf represents a perfluoroalkyl group; and at least one of: a) a first metallic compound comprising nickel, and a second metallic compound comprising molybdenum that is compositionally different from the first metallic compound; or b) a metallic alloy comprising from 50 to 70 percent by weight of nickel and from 20 to 40 percent by weight of molybdenum, based on the total weight of the metallic alloy, thereby producing at least one product represented by the formula I(CF2)nI, wherein n independently represents an integer in the range of from 1 to 11. The total weight of the at least one product wherein n is 3 or greater exceeds the total weight of the at least one product wherein n is 1 or 2 by a factor of at least 4.

Abstract translation: 制备α，ω-二碘全氟烷烃的方法包括组合：双原子碘，至少一种由下式表示的全氟氧化烯，其中Rf表示全氟烷基; 和至少一种：a）包含镍的第一金属化合物和包含与第一金属化合物成分不同的钼的第二金属化合物; 或b）金属合金，其包含基于金属合金的总重量的50-70重量％的镍和20至40重量％的钼，由此产生至少一种由式I表示的产物（CF 2 ）nI，其中n独立地表示1至11范围内的整数。其中n为3或更大的至少一种产物的总重量超过至少一种产物的总重量，其中n为1或2，其中n为1或2， 至少4的因素。

公开(公告)号：US09908837B2

公开(公告)日：2018-03-06

申请号：US14769850

申请日：2014-03-13

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Joshua L. Colby ,  Aaron E. Hutt ,  Terence D. Spawn ,  Jason D. Clapper ,  Tabitha A. Clem

IPC: C07C1/24 ,  C07C11/02 ,  C07C67/04 ,  C07C69/54 ,  C08F220/06 ,  C08F220/18 ,  C09J133/08

CPC classification number: C07C67/04 ,  C07C1/24 ,  C07C2531/08 ,  C07C2531/10 ,  C08F220/18 ,  C09J133/08 ,  C07C69/54 ,  C07C11/02 ,  C08F2220/1825 ,  C08F220/06

Abstract: Polymers, particularly those used in pressure-sensitive adhesives, are prepared from a mixture of structural isomers of a secondary alkyl (meth)acrylate monomer. The mixture is made by dehydrating a biobased C2-C22 alcohol with a first acid catalyst using a continuous process to form a mixture of olefins, and reacting (meth)acrylic acid with at least some of the mixture of olefins in the presence of a second acid catalyst. The adhesives are characterized by exhibiting an overall balance of adhesive and cohesive characteristics, and containing biobased material.

公开(公告)号：US20160002140A1

公开(公告)日：2016-01-07

申请号：US14769875

申请日：2014-03-04

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Joshua L. Colby ,  Tabitha A. Clem ,  Terence D. Spawn ,  Aaron E. Hutt ,  Wade T. Teply

IPC: C07C67/08 ,  C07C57/02 ,  C09J133/08

CPC classification number: C07C67/08 ,  C07C57/02 ,  C08F220/18 ,  C09J133/08 ,  Y02P20/582 ,  C07C69/54 ,  C08F2220/1858 ,  C08F220/06

Abstract: A method of making 2-octyl acrylate comprising reacting 2-octanol with acrylic acid in the presence of an acid catalyst and added water is described. The 2-octanol may be derived from renewable resources, such as castor oil. The method is efficient and provides selectivity for 2-octyl acrylate.

Abstract translation: 描述了在酸催化剂和加入水的存在下，使2-辛醇与丙烯酸反应制备丙烯酸2-辛酯的方法。 2-辛醇可来自可再生资源，如蓖麻油。 该方法是有效的，并为丙烯酸2-辛酯提供选择性。

公开(公告)号：US09212119B2

公开(公告)日：2015-12-15

申请号：US14434981

申请日：2013-10-09

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Steven J. Martin ,  Luke T. Dressel ,  Aaron E. Hutt ,  Eric A. Schotz ,  Terence D. Spawn ,  Miguel A. Guerra ,  Tatsuo Fukushi ,  Jeremy A. Miller ,  Christopher M. Geise ,  James A. McDonell

IPC: C07C21/18 ,  C07C45/58 ,  C07C17/26 ,  C07C17/093

CPC classification number: C07C45/58 ,  C07C17/00 ,  C07C17/093 ,  C07C17/26 ,  C07C19/16

Abstract: A method of making α,ω-diiodoperfluoroalkanes includes combining: diatomic iodine, at least one perfluoroalkylene oxide represented by the formula wherein Rf represents a perfluoroalkyl group; and at least one of: a) a first metallic compound comprising nickel, and a second metallic compound comprising molybdenum that is compositionally different from the first metallic compound; or b) a metallic alloy comprising from 50 to 70 percent by weight of nickel and from 20 to 40 percent by weight of molybdenum, based on the total weight of the metallic alloy, thereby producing at least one product represented by the formula I(CF2)nI, wherein n independently represents an integer in the range of from 1 to 11. The total weight of the at least one product wherein n is 3 or greater exceeds the total weight of the at least one product wherein n is 1 or 2 by a factor of at least 4.

Abstract translation: 制备α，ω-二碘全氟烷烃的方法包括组合：双原子碘，至少一种由下式表示的全氟氧化烯，其中Rf表示全氟烷基; 和至少一种：a）包含镍的第一金属化合物和包含与第一金属化合物成分不同的钼的第二金属化合物; 或b）金属合金，其包含基于金属合金的总重量的50-70重量％的镍和20至40重量％的钼，由此产生至少一种由式I表示的产物（CF 2 ）nI，其中n独立地表示1至11范围内的整数。其中n为3或更大的至少一种产物的总重量超过至少一种产物的总重量，其中n为1或2，其中n为1或2， 至少4的因素。